CN105231482A - Gum base type smokeless tobacco product with anti-fatigue effect and preparing method of gum base type non-smoke-gas tobacco product - Google Patents
Gum base type smokeless tobacco product with anti-fatigue effect and preparing method of gum base type non-smoke-gas tobacco product Download PDFInfo
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Abstract
The invention belongs to the field of smokeless tobaccos, and particularly relates to a gum base type smokeless tobacco product with an anti-fatigue effect and a preparing method of the gum base type smokeless tobacco product. The tobacco product is prepared from raw materials including gum base, tobacco materials and a Maca composition. The gum base type smokeless tobacco product has the advantages that the Maca composition is added, so that the physiological intensity is proper; the mouthfeel is comfortable; the gum base type smokeless tobacco product can be used as a novel supplementary substitute product of conventional cigarettes for smokers in places such as public places in which no smoking is not recommended; the effects of nicotine dependence reduction, antifatigue and the like are also achieved; and the gum base type smokeless tobacco product is a smokeless tobacco product with good market application prospects.
Description
Technical field
The invention belongs to smokeless tobacco field, be specifically related to a kind of gum base type smoke-free tobacco product with antifatigue effect and its production and use.
Background technology
Smoker has dependence to smoking, mainly can produce satisfaction and joyful sense owing to burning and sucking tobacco, extends the visual cognitive ability time, pressure, the anxiety etc. of releiving unhealthy emotion.Smoke-free tobacco product is provide physiology satisfaction by compositions such as nicotine to consumer in essence, thus plays the effect of alternative smoking or minimizing smoking.Gum base type smoke-free tobacco product is blended in chewing gum base by compositions such as tobacco-containing materials, be made into the tobacco product being similar to chewing gum, easy to use, excitant is little, domestic consumer is more acceptant, is the promising Novel smokeless gas tobacco product in a kind of market at home.
The gum base type smoke-free tobacco product of external listing by adding nicotine composition in matrix, discharge nicotine during use to provide certain physiology satisfaction, discharge too fast, excitement is strong, as the supplementary substitute of traditional cigarette, but can not reduce the dependence feeling to nicotine.
Summary of the invention
The shortcoming of prior art in view of the above, the object of the present invention is to provide a kind of gum base type smoke-free tobacco product with antifatigue effect and preparation method thereof, for solving the problems of the prior art.
For achieving the above object and other relevant objects, first aspect present invention provides a kind of gum base type smokeless tobacco composition with antifatigue effect, and its raw material comprises matrix, tobacco-containing material and Ma Ka composition.
The present invention is surprised to find that, tobacco-containing material and agate card composition have synergistic function, and when the two is composite, antifatigue effect significantly promotes, especially the best results when the part by weight of described tobacco-containing material and described agate card composition is 0.5-15: 2-10.
Preferably, described in there is the gum base type smokeless tobacco composition of antifatigue effect, its raw material comprises matrix 20-55 part, tobacco-containing material 0.005-25 part and agate card composition 0.5-20 part with parts by weight.
Further preferably, described in there is the gum base type smokeless tobacco composition of antifatigue effect, its raw material comprises matrix 30-50 part, tobacco-containing material 0.5-15 part and agate card composition 2-6 part with parts by weight.
For improving the above-mentioned mouthfeel with the gum base type smokeless tobacco composition of antifatigue effect further, reduce its excitant, improve the comfort of product and the adaptability of crowd, the formula of the present invention to this tobacco compositions is optimized further.
The above-mentioned gum base type smokeless tobacco composition with antifatigue effect, its raw material comprises by weight:
Preferably, the above-mentioned gum base type smokeless tobacco composition with antifatigue effect, its raw material by weight, comprising:
Second aspect present invention provide above-mentioned there is the gum base type smokeless tobacco composition of antifatigue effect preparing the application in tobacco product.
Third aspect present invention provides containing the above-mentioned tobacco product with the gum base type smokeless tobacco composition of antifatigue effect; Preferably, described tobacco product also comprises the acceptable raw material of Field of Tobacco, such as emulsifying agent, softening agent, humectant, pH adjusting agent, filler, antioxidant, colouring agent etc.
Preferably, above-mentioned tobacco product, its raw material by weight, comprising:
There is gum base type smokeless tobacco composition 80-99.5 part of antifatigue effect;
Further preferably, above-mentioned tobacco product, its raw material by weight, comprising:
There is gum base type smokeless tobacco composition 90-97 part of antifatigue effect;
Preferably, described tobacco product outer surface is also coated with dressing, and described dressing raw material comprises the acceptable raw material of Field of Tobacco, such as sweetener, flavouring agent, natural plant gum, edible wax, filler etc.
Preferably, described matrix is selected from one or more the combination in natural plants matrix, chemical synthesis matrix.
Further preferably, described natural plants matrix is selected from tunny gum, natural rubber, Ba Lata glue, gutta-percha, gutta-percha, gelutong, one or more the combination come out in Europe glue, Gorgon euryale thatch palm glue, guayule rubber glue and other food natural gums.Described chemical synthesis matrix is selected from one or more the combination in polyvinyl acetate, polyisobutene, polyisoprene and other food synthesis matrix.
Described tobacco-containing material is one or more in tobacco powder, tobacco extract or tobacco extract composite fine powders.
Preferably, described tobacco is selected from one or more the combination in flue-cured tobacco, suncured tabacco, air-curing of tobacco leaves, burley tobaccos, Turkish tobaccos, Nicotiniana rustica; Specifically can use the position such as leaf, flower, stem, seed of tobacco.
Further preferably, described suncured tabacco is selected from one or more the combination in Dark sun-cured and Sun cured tobacco and other region suncured tabacco, and described air-curing of tobacco leaves is selected from one or more the combination in Maryland, cigar and other region air-curing of tobacco leaves.
Still more preferably, described tobacco is the airing cigarette originating from Guizhou province, or the combination of this airing cigarette and other tobaccos.
Preferably, described tobacco is one or more the combination in conventional tobacco leaf and ecological organic tobacco leaf.
Preferably, described tobacco, after spontaneous fermentation, ageing, taking out stalk, cleaning, dehydration, needs carry out flavouring and/or reduce nicotine process before further use.Described flavouring process refers to spice liquid immersion or infiltrates tobacco-containing material, or is sprayed onto by spice liquid on tobacco powder or tobacco extract composite powder.Spice liquid decocts water by spices material or flavouring agent is formulated.
Preferably, reducing nicotine is treated to according to tobacco-containing material: tobacco-containing material is immersed deionized water by the ratio of water=1:10-50, adds the materials such as a certain amount of citric acid, citrate, soaks 10-60 minute under 30-90 DEG C of condition, then filtrate is removed, dry tobacco-containing material.
Preferably, described tobacco-containing material granularity is greater than 200 orders; More preferably, described tobacco-containing material granularity is 200-4000 order.
Described tobacco extract refers to that tobacco is after super-dry, pulverizing, screening, through extracting the tobacco extract obtained; More preferably, described extracting method is selected from one or more the combination in supercritical extract, extraction, ultrasound on extracting, microwave auxiliary extraction, distillation extraction etc.
Described tobacco extract compound fine powder be tobacco extract through means such as molecular clock, freeze drying, spraying dry, the tobacco extract compound fine powder made under the effect of excipient.
Described excipients comprises calcium carbonate, starch, phosphorylation PASELLI EASYGEL, sodium carboxymethyl starch, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethylcellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, HPMC, gelatin, Arabic gum, casein, chitin, chitosan, chitosan oligosaccharide and derivative, sodium alginate, propylene glycol alginate, tara gum, mannitol, D-sorbite, lactitol, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Sunset Abelmoschus Root glue, xanthans, cassia gum, peach gum, lac, bassora gum, carragheen, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, the combination of one or more in flaxseed gum and other food-grade excipients.
Described agate card composition is agate card.
Or described agate card composition comprises agate card, and Bee Pollen, Moringa extract, Herb Gynostemmae Pentaphylli extract, wolfberry fruit extract, inulin, A Sayi berry extract, card nurse berry extract, kola extract, Guarana extract, Sakyamuni extract, extractive of alfalfa, Noni extract, one or more combination in damiana extract.Preferably, in described agate card composition, the part by weight of agate card and other plant component is 0.1:1-5:1.
Preferably, described agate card comprises maca powder and/or agate card extract.
In order to improve pungent, the pained mouthfeel of agate card itself, and improve the service efficiency of agate card active ingredient, maca powder of the present invention adopts low-temperature airflow crushing technology to be prepared from, and particle diameter is less than 75 μm; Described agate card extract adopts two-stage compound collecting technology, and enrichment to the full extent concentrates the active ingredient in agate card, improves effect in the product; Agate card component and other plant composition are re-dubbed agate card composition, on the basis of mouthfeel of improving agate card component, the antifatigue effect of agate card composition can be improved further.
Described agate card (formal name used at school: LepidiummeyeniiWalp has another name called agate coffee), Spanish: Maca.
Preferably, the preparation method of described maca powder comprises:
1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%;
The temperature of preferably freeze drying is-20 ~-45 DEG C, and vacuum is 10-30Pa;
The temperature of preferred low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa;
2) described dried agate card is pulverized, sieved, obtain 20-100 object meal;
3) utilize low-temperature airflow micronizer that described agate card meal is carried out separating twice, screening obtains maca powder.
More preferably, the granularity of described maca powder is greater than 200 orders.
Further preferably, the granularity of described maca powder is greater than 2000 orders.
Preferably, the preparation method of described agate card extract comprises:
1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%; Dried agate card is pulverized, sieves, obtain 20-100 object meal;
2) utilize 70-95% ethanol as extractant, the part by weight of extractant and described agate card meal is 10:1-30:1, at 50-80 DEG C, extract 1-5 hour, is separated to obtain filtrate and filter residue, obtains agate card alcohol extract by concentrated for described filter vacuum;
3) by step 2) described filter residue adds 10-20 times of weight water, extracts 0.5-3 hour, be separated to obtain filtrate at 80-100 DEG C, obtains agate card water extract by concentrated for described filter vacuum;
4) be get Ma Ka extract after described agate card alcohol extract and Ma Ka water extract being mixed according to 1:1-5:1 part by weight.Powdery agate card extract can be prepared through further freeze drying or spraying dry.
Preferably, described cryodesiccated temperature is-20 ~-45 DEG C, and vacuum is 10-30Pa;
Preferably, the temperature of described low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa;
More preferably, the order of alcohol extraction process and extraction process by water can exchange, or adds other treatment process arbitrary operation is forward and backward.
Preferred, described extracting method comprises one or more the combination in extraction, ultrasound on extracting, microwave auxiliary extraction, distillation extraction etc.
Preferably, in described agate card composition except agate card other extract components be through drying, pulverizing, extraction, the concentrated paste that obtains or powdered extract.
Described agate card composition can technology be prepared from routinely.
Preferably, described sweetener is selected from fructose, glucose (slurry), HFCS, sucrose, maltose, hydrogenated starch hydrolysate, corn syrup, Maple Syrup, honey, steviol glycoside, mogroside, xylitol, lactitol, maltitol (slurry), D-sorbite (slurry), mannose, D-mannital, isomaltoketose, isomalt, isomalto-oligosaccharide, antierythrite, milk ketose, gossypose, soyabean oligosaccharides, lactosucrose, xylo-oligosaccharide, galactooligosaccharide, FOS, inulooligosaccharide, lactose, protein sugar, licorice powder, glycyrrhetate, Africa arrowroot glucin, acesulfame potassium, knob is sweet, Aspartame, saccharin sodium, honey element, calcium cyclamate, Sucralose, alitame, Sucralose, glycyrrhizin, NHDC, curculin, miracle fruit thaumatin T, potato root of fangji glucin, two sweet, one or more combination in Arabinose and other food carbohydrates and/or non-sugar sweetener.
Preferably, described acid is selected from one or more the combination in citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid and other food acid taste agent.
Preferably, described flavouring agent is selected from one or more the combination in licorice powder, ground coffee, plum powder, red date powder, cocoa power, green tea powder, fruit extract, aloe extract, Honegsukle flower P.E, arhat fruit tincture, hawthorn fruit tincture, red date tincture, faenum graecum tincture, hop tincture, cocoa tincture, dark plum tincture, black tea tincture, green tea tincture, hergamot oil, lemon oil, caffeol, buchu leaves oil, clove leaf oil, basil, orange oil, natural cognac, Michelia oil, peppermint oil, grapefruit oil, FLOS CHRYSANTHEMI ALBA from Haizhou of China oil, Rum and other food flavouring agents.
Preferably, described emulsifying agent is selected from one or more the combination in single, double, triglyceride, lecithin, soybean lecithin, degreased cocoa powder, acetylation list bis-fatty acid glyceride, sucrose fatty ester and other food emulsifying agents.
More preferably, described triglyceride refers to Glycerin, mixed triester with caprylic acid capric acid and glyceryl triacetate etc.
Preferably, described softening agent is selected from one or more the combination in propane diols, glycerine, pectin, alginic acid, sodium alginate, ammonium alginate, Chitosan-phospholipid complex, chitosan oligosaccharide and derivative thereof, gelatin, xanthans, peach gum, Arabic gum, lac, hydrogenated vegetable oil, Brazil wax, beeswax, paraffin, microcrystalline wax, candelila wax, pulullan polysaccharide and other food softening agents.
Preferably, described humectant is selected from one or more the combination in propane diols, glycerine, water-soluble plant polysaccharide, honey, polydextrose, maltitol pulp, sorbitol syrup and other food humectants.
Preferably, described pH adjusting agent is selected from one or more the combination in sodium carbonate, potash, sodium acid carbonate, saleratus, sodium pyrophosphate, dipotassium hydrogen phosphate, sodium hydrogen phosphate, calcium monohydrogen phosphate, tripotassium phosphate, tertiary sodium phosphate, potassium metapbosphate, natrium citricum, potassium citrate, gluconic acid sodium salt, diammonium hydrogen phosphate and other food pH adjusting agents.
Preferably, described freshener is selected from menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-to one or more the combination in benzene acetonitrile base peppermint alkyl formamides, N-(2-(pyridine-2-base) ethyl) peppermint alkyl formamides, menthalactone and other mint extracts or derivative.
Preferably, described antioxidant selects one or more the combination in Tea Polyphenols, butylated hydroxy anisole, Sodium Benzoate, dibutyl hydroxy toluene, n-propyl gallate, sorbic acid and sylvite thereof, dl-alpha-tocopherol, d-alpha-tocopherol, vitamin C, Calcium Ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt, carnosic acid, Licorice root antioxidant, AOB, ginkgo biloba extract, tea extract and grape seed extract and other food antioxidants.
Preferably, described colouring agent is selected from erythrosine, light blue, monascus yellow pigment, tea uranidin, Tea Green Pigment, Ipomoea batatas(L.)Lam, β-A Piao-8 '-carotenal, copper chlorophyll, indigo, Pasania cuspidata palm fibre, titanium dioxide, lycopene, citrus is yellow, black soya bean is red, blackcurrant is red, safflower yellow, red rice is red, Monascus color, turmeric, burnt sugar coloring, fruit of Cherokee rose palm fibre, coreopsis yellow extract, cacao pigment, chilli orange, radish red, the certain herbaceous plants with big flowers that falls is red, roselle is red, close illiteracy is yellow, Grape Skin is red, mulberries are red, wild jujube look, natural amaranth, alkermes, red bayberry is red, lutein, algae is blue, one or more combination in beta carotene and other food coloring.
Preferably, described filler is selected from one or more the combination in titanium dioxide, calcium lactate, talcum powder, calcium monohydrogen phosphate, calcium carbonate, magnesium carbonate, calcirm-fluoride and other food fillers.
Fourth aspect present invention provides the above-mentioned preparation method with the gum base type smokeless tobacco composition of antifatigue effect, comprises the steps:
1) needed raw material is got by formula;
2), after described matrix is softening, add other raw materials by formula, stir; Part material can add suitable quantity of water if desired;
3) by step 2) gained material is pressed into sheet, cuts, sizing.
Fifth aspect present invention provides the preparation method of above-mentioned tobacco product, comprise the steps: to described have in the gum base type smokeless tobacco composition of antifatigue effect add other raw material.
The preparation method of above-mentioned tobacco product also comprises and carries out dressing, polishing, waxing, packaging and other steps.
Preferably, after overaging, low tempertaure storage, polishing waxing is carried out again after dressing.
During described polishing waxing, available polishing agent includes but not limited to one or more the combination in stearic acid, calcium stearate, dolomol, odium stearate, potassium stearate, Brazil wax, beeswax, Tissuemat E, polyethylene glycol, paraffin, petroleum paraffin, microcrystalline wax, candelila wax etc.
Preferably, described polishing agent consumption is the 0.05%-0.5% of described tobacco product weight.
Weight portion of the present invention can be the unit of weights well known in the art such as μ g, mg, g, kg, also can be its multiple, as 1/10,1/100,10 times, 100 times etc.
The gum base type smoke-free tobacco product with antifatigue effect of the present invention, use as chewing, breath freshening can be kept, consumer obtains suitable physiology satisfaction while chewing, and a large amount of harmful components not having cigarette burning to produce, it also avoid the environmental tobacco smoke that traditional cigarette causes to pollute, can wait in public places and the place of smoking should not be used as the supplementary substitute products of traditional cigarette for smoker; In the matrix of gum base type smoke-free tobacco product, mix the spices volatility of joining greatly reduce, the time of preserving fragrance is more lasting, can slowly release flavor component, bring joyful sense to consumer in the process of chewing; The agate card composition added, agate blocking is become Ultramicro-powder or extract form, and optimize with other plant extract and compositely make agate card composition, not only improve the mouthfeel quality of agate card composition, also improve its action effect, there is the effects such as certain antifatigue, renitency, reduce the dependence feeling to nicotine, play certain health-care effect.
Detailed description of the invention
The agate card component obtained through special process process and other preferred plant components are optimized and compositely obtain agate card composition by inventor, agate card composition is with the addition of in gum base type smoke-free tobacco product formula, the gum base type smoke-free tobacco product obtained not only can be supplied to the suitable physiology impression of consumer by slow releasing nicotine, also there is the effect such as antifatigue, renitency, reduce the dependence to nicotine, play certain health-care effect.Effect, completes the present invention on this basis.
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Notice, in the following example, the concrete process equipment that indicates or device all adopt conventional equipment in this area or device.
In addition should be understood that the one or more method steps mentioned in the present invention do not repel and can also to there is additive method step or can also insert additive method step before and after described combination step between these steps clearly mentioned, except as otherwise noted; Will also be understood that, the relation that is connected between the one or more equipment/devices mentioned in the present invention is not repelled and can also to be there are other equipment/devices or can also insert other equipment/devices before and after described unit equipment/device between these two equipment/devices clearly mentioned, except as otherwise noted.And, except as otherwise noted, the numbering of various method steps is only the convenient tool differentiating various method steps, but not be ordering or the enforceable scope of restriction the present invention of restriction various method steps, the change of its relativeness or adjustment, when changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1
The present embodiment provides a kind of gum base type smoke-free tobacco product with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 60 parts, Bee Pollen 10 parts, Moringa extract 10 parts, A Sayi berry extract 10 parts, card nurse berry extract 10 parts.
The preparation method in the present embodiment with the gum base type smoke-free tobacco product of antifatigue effect comprises the following steps:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carried out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to airing cigarette: flue-cured tobacco: the weight ratio mixing of Turkish tobaccos=6:3:1, to pulverize, solvent extraction method or supercritical extraction is utilized to obtain smoking mixture extract.
By tobacco extract: Arabic gum: by weight dispersion in deionized water, strong stirring is emulsion uniformly for beta-schardinger dextrin-=1:2:3, and spraying dry forms tobacco extract compound.
(2) batch mixing
By plant matrix, soften 1 hour at 55 DEG C, kneading 5 minutes in kneading machine; Add glucose, xylitol, mix 10 minutes; Then add tobacco extract compound, agate card composition, glucose syrup, Arabic gum, caffeol, soybean lecithin, glycerine, menthol, potassium sorbate, sodium carbonate etc., stir 30 minutes to 1 hour, material is fully mixed.
(3) compressing tablet sizing
The gum base type smoke-free tobacco product material stirred is loaded after extruding in extruder, then be pressed into certain thickness plate by multi-section roller type machine, and then be cut into suitable sheet with cutting machine.Sheet gum base type smoke-free tobacco product material is put into modular system according to the specification of 1.0g/ sheet grain regular cut, embossing, sizing, spill one deck Icing Sugar simultaneously, in case gum base type smoke-free tobacco product sclerosis.Gum base type smoke-free tobacco product after sizing temperature 2-7 DEG C, relative humidity carries out under being 45-50% cooling, storing 48-72 hour.
(4) dressing is aging
The compound material of maltitol, guar gum, menthol, titanium dioxide is utilized to carry out outer coatings to stereotyped gum base type smoke-free tobacco product, then aging 8-24 hour at 2-7 DEG C.Utilize the polishing agent being main component with food grade Brazil wax, after gum base type smoke-free tobacco product being carried out surface finish process by rotation glossing, packaging.
Embodiment 2
The present embodiment provides a kind of gum base type smoke-free tobacco product with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 40 parts, kola extract 20 parts, Guarana extract 20 parts, Sakyamuni extract 10 parts, inulin 10 parts.
The preparation method in the present embodiment with the gum base type smoke-free tobacco product of antifatigue effect comprises the following steps:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, carry out taking out stalk, cleaning, processed.According to Radix Glycyrrhizae: the ratio of water=1:10-20 was by Radix Glycyrrhizae at 90-100 DEG C fried 1 hour, and cooling, after filtration, adding weight ratio in filtrate is that 5% honey is mixed with spice liquid, with spice liquid, airing cigarette is infiltrated 24-72 hour, carries out flavouring process.After airing cigarette is taken out, dry under 120-140 DEG C of condition to moisture and be less than 3wt%.Pulverized by dried tobacco-containing material, screening obtains 200-500 object airing tobacco powder end.
(2) batch mixing
Plant matrix is softened 3 hours at 50 DEG C, kneading 5 minutes in kneading machine; Add xylitol, D-sorbite, mix 5 minutes; Then add tobacco powder, agate card composition, mogroside, lac, Cranberry extract, lemon oil, lecithin, citric acid, vitamin C, menthol, titanium dioxide successively, stir 45 minutes, material is fully mixed.
(3) compressing tablet sizing
The gum base type smoke-free tobacco product material stirred is loaded after extruding in extruder, then be pressed into certain thickness plate by multi-section roller type machine, and then be cut into suitable sheet with cutting machine.Sheet gum base type smoke-free tobacco product material is put into modular system according to the specification of 1.0g/ sheet grain regular cut, embossing, sizing, spill one deck Icing Sugar simultaneously, in case gum base type smoke-free tobacco product sclerosis.Gum base type smoke-free tobacco product after sizing temperature 2-7 DEG C, relative humidity carries out under being 45-50% cooling, storing 24-48 hour.
(4) dressing is aging
The compound material of antierythrite, maltodextrin, locust bean gum, magnesium carbonate, orange oil is utilized to carry out outer coatings stereotyped gum base type smoke-free tobacco product, then aging 8-24 hour at 2-7 DEG C.Utilizing the polishing agent being main component with food grade beeswax, by rotating glossing, gum base type smoke-free tobacco product being carried out in surface finish after Lasaxing Oilfield, packaging.
Embodiment 3
The present embodiment provides a kind of gum base type smoke-free tobacco product with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 50 parts, Bee Pollen 30 parts, Herb Gynostemmae Pentaphylli extract 10 parts, Noni extract 10 parts.
The preparation method in the present embodiment with the gum base type smoke-free tobacco product of antifatigue effect comprises the following steps:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carried out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to airing cigarette: flue-cured tobacco: the weight ratio mixing of Turkish tobaccos=6:3:1, to pulverize, solvent extraction method or supercritical extraction is utilized to obtain tobacco extract.
(2) batch mixing
Softened 1 hour at 60 DEG C by plant matrix, in kneading machine, kneading 5 minutes, adds D-sorbite fine powder, mixes 10 minutes; Then add HFCS, tobacco extract, agate card composition, jujube tincture, Glycerin, mixed triester with caprylic acid capric acid, Arabic gum, sodium alginate, glycerine, sodium acid carbonate, menthol, vitamin E, calcium carbonate etc. successively, stir 1 hour, material is fully mixed.
(3) compressing tablet sizing
The gum base type smoke-free tobacco product material stirred is loaded after extruding in extruder, then be pressed into certain thickness plate by multi-section roller type machine, and then be cut into suitable sheet with cutting machine.Sheet gum base type smoke-free tobacco product material is put into modular system according to the specification of 1.5g/ sheet grain regular cut, embossing, sizing, spill one deck Icing Sugar simultaneously, in case gum base type smoke-free tobacco product sclerosis.Gum base type smoke-free tobacco product after sizing temperature 2-7 DEG C, relative humidity carries out under being 45-50% cooling, storing 48-72 hour.
(4) dressing is aging
The compound material of maltitol, gelatin, calcirm-fluoride, menthol is utilized to carry out outer coatings stereotyped gum base type smoke-free tobacco product, then aging 8-24 hour at 2-7 DEG C.Utilizing the polishing agent being main component with candelila wax and Brazil wax, by rotating glossing, gum base type smoke-free tobacco product being carried out in surface finish after Lasaxing Oilfield, packaging.
Embodiment 4
The present embodiment provides a kind of gum base type smoke-free tobacco product with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 40 parts, Sakyamuni extract 20 parts, extractive of alfalfa 10 parts, Noni extract 10 parts, wolfberry fruit extract 10 parts, damiana extract 10 parts.
The preparation method in the present embodiment with the gum base type smoke-free tobacco product of antifatigue effect comprises the following steps:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carried out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to airing cigarette: flue-cured tobacco: the weight ratio mixing of Turkish tobaccos=6:3:1, to pulverize, solvent extraction method or supercritical extraction is utilized to obtain tobacco extract.
(2) batch mixing
Plant matrix is softened 2 hours at 55 DEG C, kneading 5 minutes in kneading machine; Add D-sorbite fine powder, xylitol fine powder, mix 10 minutes; Then add tobacco extract, agate card composition, sodium alginate, maltodextrin, green tea powder, green tea tincture, peppermint oil, glyceryl triacetate, malic acid, glycerine, potassium sorbate, tea uranidin etc. successively, stir 1 hour, material is fully mixed.
(3) compressing tablet sizing
The gum base type smoke-free tobacco product material stirred is loaded after extruding in extruder, then be pressed into certain thickness plate by multi-section roller type machine, and then be cut into suitable sheet with cutting machine.Sheet gum base type smoke-free tobacco product material is put into modular system according to the specification of 1.5g/ sheet grain regular cut, embossing, sizing, spill one deck Icing Sugar simultaneously, in case gum base type smoke-free tobacco product sclerosis.Gum base type smoke-free tobacco product after sizing temperature 2-7 DEG C, relative humidity carries out under being 45-50% cooling, storing 48 hours.
(4) dressing is aging
The compound material of isomaltoketose, corn syrup, menthol, pulullan polysaccharide is utilized to carry out outer coatings stereotyped gum base type smoke-free tobacco product, then aging 8-12 hour at 2-7 DEG C.Utilizing the polishing agent being main component with polyethylene glycol, beeswax, by rotating glossing, gum base type smoke-free tobacco product being carried out in surface finish after Lasaxing Oilfield, packaging.
Embodiment 5
The present embodiment provides a kind of gum base type smokeless tobacco composition with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 60 parts, Bee Pollen 10 parts, Moringa extract 10 parts, A Sayi berry extract 10 parts, card nurse berry extract 10 parts.
The present embodiment has the gum base type smokeless tobacco composition of antifatigue effect, and its preparation method comprises the steps:
1) needed raw material is got by formula;
2), after described matrix is softening, add other raw materials by formula, stir; Part material can add suitable quantity of water if desired;
3) by step 2) gained material is pressed into sheet, cuts, sizing.
Embodiment 6
The present embodiment provides a kind of gum base type smokeless tobacco composition with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 40 parts, kola extract 20 parts, Guarana extract 20 parts, Sakyamuni extract 10 parts, inulin 10 parts.
The present embodiment has the preparation method of the gum base type smokeless tobacco composition of antifatigue effect with embodiment 5.
Embodiment 7
The present embodiment provides a kind of gum base type smokeless tobacco composition with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 50 parts, Bee Pollen 30 parts, Herb Gynostemmae Pentaphylli extract 10 parts, Noni extract 10 parts.
The present embodiment has the preparation method of the gum base type smokeless tobacco composition of antifatigue effect with embodiment 5.
Embodiment 8
The present embodiment provides a kind of gum base type smokeless tobacco composition with antifatigue effect, and its raw material comprises:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 40 parts, Sakyamuni extract 20 parts, extractive of alfalfa 10 parts, Noni extract 10 parts, wolfberry fruit extract 10 parts, damiana extract 10 parts.
The present embodiment has the preparation method of the gum base type smokeless tobacco composition of antifatigue effect with embodiment 5.
Embodiment 9
The preparation method of maca powder: after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilizes freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%.Cryodesiccated temperature is-20 ~-45 DEG C, and vacuum is 10-30Pa.The temperature of low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa.Dried agate card section is pulverized, sieved, obtains 20-100 object meal.Utilize low-temperature airflow micronizer that agate card meal is carried out separating twice, screening obtains agate card Ultramicro-powder.Preferred, the granularity of described maca powder is greater than 200 orders.Preferred further, the granularity of described maca powder is for being greater than 2000 orders.
Comparative example 1
One tobacco articles, its raw material comprises:
| Composition | Title | kg |
| Matrix | Plant matrix | 40.00 |
| Tobacco-containing material | Flue-cured tobacco powder | 15.00 |
| Sweetener | Xylitol | 20.00 |
| Sweetener | D-sorbite | 15.00 |
| Sweetener | Mogroside | 0.10 |
| Acid | Citric acid | 0.10 |
| Flavouring agent | Cranberry extract | 4.00 |
| Flavouring agent | Lemon oil | 1.00 |
| Emulsifying agent | Lecithin | 1.00 |
| Softening agent | Lac | 3.20 |
| Antioxidant | Vitamin C | 0.10 |
| Filler | Titanium dioxide | 0.50 |
Dried at 40-60 DEG C by flue-cured tobacco, pulverizing, screening obtain 200-300 object tobacco powder.Adding weight ratio is in deionized water 1% cocoa tincture, 0.5% sorbitan monooleate, 5% beta-schardinger dextrin-, 2% microcrystalline cellulose, strong stirring, after mixing, is evenly sprayed in tobacco powder, be as the criterion not lump, after equilibrium water conten, namely obtain flue-cured tobacco powder.
In this comparative example, tobacco product tobacco-containing material is flue-cured tobacco powder, does not add agate card composition, and its preparation method is with reference to embodiment 2.
Comparative example 2
One tobacco articles, its raw material comprises:
| Composition | Title | kg |
| Matrix | Plant matrix | 36.00 |
| Tobacco-containing material | Tobacco extract | 2.00 |
| Agate card composition | Maca powder | 25.00 |
| Sweetener | Xylitol | 20.00 |
| Sweetener | Glucose | 10.00 |
| Softening agent | Arabic gum | 2.00 |
| Softening agent | Sodium alginate | 1.00 |
| Humectant | Glycerine | 1.90 |
| PH conditioning agent | Sodium acid carbonate | 1.00 |
| Antioxidant | Vitamin E | 0.10 |
| Filler | Calcium carbonate | 1.00 |
The agate card composition that in this comparative example, tobacco product adds is pure maca powder, does not add flavouring agent, and its preparation method is with reference to embodiment 3.
Comparative example 3
One tobacco articles, its raw material comprises:
| Composition | Title | kg |
| Matrix | Plant matrix | 40.00 |
| Tobacco-containing material | Tobacco extract compound | 20.00 |
| Sweetener | Xylitol | 15.00 |
| Sweetener | Glucose syrup | 10.00 |
| Sweetener | Powdered glucose | 10.00 |
| Emulsifying agent | Soybean lecithin | 0.80 |
| Softening agent | Arabic gum | 1.50 |
| Humectant | Glycerine | 1.00 |
| PH adjusting agent | Sodium carbonate | 1.00 |
| Antioxidant | Potassium sorbate | 0.10 |
In this comparative example, tobacco product does not add agate card composition, does not add flavouring agent, and its preparation method is with reference to embodiment 1.
Comparative example 4
One tobacco articles, its raw material comprises:
Wherein, in the formula of plant agate card composition, the weight ratio of each component is as follows: Sakyamuni extract 20 parts, extractive of alfalfa 20 parts, Noni extract 20 parts, wolfberry fruit extract 20 parts, damiana extract 20 parts.
In this comparative example, tobacco product does not add tobacco-containing material, and not containing agate card component in vegetable composition, its preparation method is with reference to embodiment 4.
Comparative example 5
One tobacco articles, the difference of its raw material and embodiment 1 is only not containing agate card composition.
Comparative example 6
One tobacco articles, the difference of its raw material and embodiment 2 is only not containing agate card composition.
Comparative example 7
One tobacco articles, the difference of its raw material and embodiment 3 is only not containing agate card composition.
Comparative example 8
One tobacco articles, the difference of its raw material and embodiment 4 is only not containing agate card composition.
Experimental example
The gum base type smoke-free tobacco product with antifatigue effect prepared by embodiment 1-4 and comparative example 1-4 is carried out sensory evaluation test, sensory quality assessment method, specific as follows:
Sensory quality assessment index
This sensory quality assessment method arranges 9 evaluation indexes altogether, comprise entrance mouthfeel, physiological strength, feature be fragrant, tobacco is fragrant, excitement, comfort, release uniformity, release persistence and oral cavity pleasant impression.After described entrance mouthfeel refers to that smoke-free tobacco product puts into oral cavity, the initial synthetic impressions such as the sense of smell of user, the sense of taste and sense of touch.Described physiological strength refers in use, the physiology satisfaction that user experiences, i.e. strength.Described feature perfume (or spice) refers in use, the amount of the characteristic perfume that user experiences and matter.Described tobacco perfume (or spice) refers in use, the amount of this perfume (or spice) of tobacco that user experiences and matter.Described excitement refers in use, and the positions such as user oral cavity, nasal cavity, throat, esophagus are experienced the discomfort such as pungent, dry and are subject to.Described comfort refers in use, smell coordination that user experiences, soft and moist sense, without the impression of the fragrance such as residue foreign body sensation.Described release uniformity refers in use, user experience the release stability in time such as fragrance, physiological strength.Described release persistence refers to that in use, user experiences the duration such as fragrance, physiological strength length.Described oral cavity pleasant impression refers to after use procedure, the comprehensive impression of the remaining sense of smell in user oral cavity, the sense of taste and sense of touch.
Sensory quality assessment scoring rule
Described sensory quality assessment scoring rule adopts hundred-mark system point system.Described hundred-mark system point system refers to according to every sensory quality assessment index the influence degree of smoke-free tobacco product aesthetic quality, give the weight that each sensory quality assessment index is different, i.e. different score value, 9 sensory quality assessment indexs are marked by 5 points, 10 points or twenty point system respectively, and the highest score value of 9 sensory quality assessment indexs adds and be a percentage.
The scoring rule of described 9 sensory quality assessment indexs is as follows: described sensory quality assessment index is divided into 6 grades, and every shared weight, scoring scale and scoring are interval as shown in table 1, and minimum score unit is 0.5 point.
Described sensory quality assessment index weights refers to this sensory quality assessment index the highest getable score value in sensory quality assessment process.Described sensory quality assessment index score is interval refers to that the score value of this sensory quality assessment index in sensory quality assessment process corresponding to a certain evaluation scale is interval, and wherein comparatively high score is included in this section of score, and lower point is not included in this section of score.
Described sensory quality assessment index " excitement " impression is stronger, and score is lower; Described sensory quality assessment index " entrance mouthfeel ", " oral cavity pleasant impression " experience better, and score is higher; Described sensory quality assessment index " physiological strength ", " feature is fragrant ", " tobacco is fragrant ", " comfort ", " release uniformity ", " release persistence " experience stronger, and score is higher;
Described sensory quality assessment total score is added by the arithmetic of each subitem sensory quality assessment index score and is obtained.Total score score is higher, then represent that the sensory quality assessment effect of this smoke-free tobacco product is better.
Table 1 smoke-free tobacco product sensory quality assessment scoring rule
Sensory quality assessment implementation method
Valuation officer is arranged
Preferably, the evaluation team comprising 9 valuation officers is set.
Evaluation operation process
A collection of smoke-free tobacco product sample to be evaluated is carried out blind mark (if sample number is greater than 999, then digital code can be upgraded to 4, the rest may be inferred) with 3 digit numerical code, and by sampfe order random process; Carry out sensory quality assessment according to the sampfe order after process, before each sample starts evaluation, be distributed to and evaluate everyone a smoke-free tobacco product sensory quality assessment record sheet of team, sensory evaluation is carried out to smoke-free tobacco product; According to weight, evaluation scale and the interval of scoring of 9 sensory quality assessment indexs in table 1, valuation officer tackles every evaluation index and carries out sensory quality assessment, and in sensory evaluation record sheet records appraisal result, then all sensory quality assessments evaluating team are aggregated in monocyte sample sensory quality assessment summary sheet, and carry out evaluation result statistical disposition; After completing the sensory quality assessment of all samples successively, the sensory quality assessment of all samples is aggregated in batch sample sensory quality assessment summary sheet.
Evaluation result statistical analysis
Preferably, the computational methods of individual event sensory quality assessment index score are: 9 participate in the valuation officer of sensory quality assessments to all scorings of this sensory quality assessment index in remove one minimum point and a best result, remain 7 scorings for effective score, the arithmetic mean of instantaneous value of effective score is this sensory quality assessment index score, and result retains two-decimal;
The arithmetic mean of instantaneous value of each individual event sensory quality assessment index score adds and is the sensory quality assessment total score of smoke-free tobacco product, and result retains two-decimal.Total score score value is higher, then represent that the sensory evaluation effect of this smoke-free tobacco product is better.Concrete outcome is as shown in table 2:
Table 2 has the sensory quality assessment statistical form of the gum base type smoke-free tobacco product of antifatigue effect
From table 2, with Guizhou province airing cigarette be main tobacco material, add prepare the gum base type smoke-free tobacco product with antifatigue effect have that physiological strength is moderate, excitant is little containing the agate card composition of agate card component, the feature such as comfortable taste, release are stable, good after-taste.
Evaluate after tobacco product prepared by embodiment 1-4 (adding agate card composition) and comparative example 5-8 (not adding agate card composition) is met at personage's use of smoking habit respectively.Participation number is totally 100 people, and the age is between 25-55.The personnel participating in in-service evaluation are divided into two groups, and age and the years of smoking of often organizing personnel are suitable, and use the gum base type smoke-free tobacco product adding and do not add agate card composition respectively, service time is 3 months; Then one week, one month, trimestral time point fills in use sense respectively by evaluation table, summarized results lists table 3 in.
The use sense of table 3 gum base type smoke-free tobacco product is by evaluation table
Can be found by table 3 result, compared with not adding the gum base type smoke-free tobacco product of agate card composition, the gum base type smoke-free tobacco product adding agate card composition has the effect of more effective minimizing Nicotine Dependence sense, and along with the prolongation of service time, more evaluation personnel also experience fatigue-relieving, strengthen the effects such as muscle power; Without obvious oral cavity sense of discomfort, respiratory tract sense of discomfort, alimentary canal sense of discomfort or other bad impressions after the gum base type smoke-free tobacco product use of interpolation agate card composition, human tolerance is good.
In sum, the gum base type smoke-free tobacco product of interpolation agate card composition of the present invention can improve enough physiology satisfactions, and excitant is little, comfortable taste is high; Agate card is carried out specially treated, and carries out composite with other plant composition, effectively reduce the pungent pained mouthfeel of agate card itself, and be added in smoke-free tobacco product, longer-term uses to play alleviates smoking desire, fatigue-resisting function.The present invention effectively overcomes various shortcoming of the prior art and tool high industrial utilization.
In sum, the present invention effectively overcomes various shortcoming of the prior art and tool high industrial utilization.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. have a gum base type smokeless tobacco composition for antifatigue effect, its raw material comprises matrix, tobacco-containing material and Ma Ka composition.
2. the gum base type smokeless tobacco composition with antifatigue effect according to claim 1, is characterized in that, the part by weight of described tobacco-containing material and described agate card composition is 0.5-15: 2-10.
3. the gum base type smokeless tobacco composition with antifatigue effect according to claim 1, is characterized in that, its raw material comprises matrix 20-55 part, tobacco-containing material 0.005-25 part and agate card composition 0.5-20 part by weight;
Preferably, its raw material comprises matrix 30-50 part, tobacco-containing material 0.5-15 part and agate card composition 2-6 part by weight.
4. the gum base type smokeless tobacco composition with antifatigue effect according to claim 1, its raw material comprises by weight:
Preferably, its raw material by weight, comprising:
5. the gum base type smokeless tobacco composition with antifatigue effect according to any one of claim 1-4, is characterized in that,
Described tobacco-containing material is one or more in tobacco powder, tobacco extract or tobacco extract composite fine powders;
Preferably, described tobacco-containing material granularity is greater than 200 orders; More preferably, the granularity of described tobacco-containing material is 200-4000 order.
6. the gum base type smokeless tobacco composition with antifatigue effect according to any one of claim 1-5, is characterized in that, described agate card composition is agate card; Or described agate card composition comprises agate card, and Bee Pollen, Moringa extract, Herb Gynostemmae Pentaphylli extract, wolfberry fruit extract, inulin, A Sayi berry extract, card nurse berry extract, kola extract, Guarana extract, Sakyamuni extract, extractive of alfalfa, Noni extract, one or more combination in damiana extract; Preferably, in described agate card composition, the part by weight of agate card and other plant component is 0.1:1-5:1;
Preferably, described agate card comprises maca powder and/or agate card extract;
Preferably, the granularity of described maca powder is greater than 200 orders; Further preferably, the granularity of described maca powder is greater than 2000 orders;
Preferably, the preparation method of described maca powder comprises:
1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%;
The temperature of preferably freeze drying is-20 ~-45 DEG C, and vacuum is 10-30Pa;
The temperature of preferred low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa;
2) described dried agate card is pulverized, sieved, obtain 20-100 object meal;
3) utilize low-temperature airflow micronizer that described agate card meal is carried out separating twice, screening obtains maca powder;
Preferably, the preparation method of described agate card extract comprises:
1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%; Dried agate card is pulverized, sieves, obtain 20-100 object meal; Preferred described cryodesiccated temperature is-20 ~-45 DEG C, and vacuum is 10-30Pa; The temperature of preferred described low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa;
2) utilize 70-95% ethanol as extractant, the part by weight of extractant and described agate card meal is 10:1-30:1, at 50-80 DEG C, extract 1-5 hour, is separated to obtain filtrate and filter residue, obtains agate card alcohol extract by concentrated for described filter vacuum;
3) by step 2) described filter residue adds 10-20 times of weight water, extracts 0.5-3 hour, be separated to obtain filtrate at 80-100 DEG C, obtains agate card water extract by concentrated for described filter vacuum;
4) be get Ma Ka extract after described agate card alcohol extract and Ma Ka water extract being mixed according to 1:1-5:1 part by weight.
7. the preparation method with the gum base type smokeless tobacco composition of antifatigue effect described in any one of claim 1-6, comprises the following steps:
1) needed raw material is got by formula;
2), after described matrix is softening, add other raw materials by formula, stir; Part material can add suitable quantity of water if desired;
3) by step 2) gained material is pressed into sheet, cuts, sizing.
8. there is described in any one of claim 1-6 the gum base type smokeless tobacco composition with antifatigue effect that described in the gum base type smokeless tobacco composition of antifatigue effect or claim 7 prepared by method and preparing the application on tobacco product.
9. containing the tobacco product described in any one of claim 1-6 with the gum base type smokeless tobacco composition of antifatigue effect; Or containing the tobacco product with the gum base type smokeless tobacco composition of antifatigue effect prepared by method described in claim 7;
Preferably, described tobacco product, its raw material by weight, comprising:
Further preferably, described tobacco product, its raw material by weight, comprising:
10. the preparation method of tobacco product described in claim 9, is characterized in that, comprises the following steps: to described have in the gum base type smokeless tobacco composition of antifatigue effect add other raw material;
Preferably, described preparation method also comprises and carries out dressing, polishing, waxing, packaging step;
Preferably, after overaging, low tempertaure storage, polishing waxing is carried out again after dressing;
Preferably, during described polishing waxing, available polishing agent includes but not limited to one or more the combination in stearic acid, calcium stearate, dolomol, odium stearate, potassium stearate, Brazil wax, beeswax, Tissuemat E, polyethylene glycol, paraffin, petroleum paraffin, microcrystalline wax, candelila wax etc.;
Preferably, described polishing agent consumption is the 0.05%-0.5% of described tobacco product weight.
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