CN105153874A - High-adhesion wear-resistant waterborne electrostatic conducted anticorrosive coating - Google Patents
High-adhesion wear-resistant waterborne electrostatic conducted anticorrosive coating Download PDFInfo
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Abstract
The invention discloses high-adhesion wear-resistant waterborne electrostatic conducted anticorrosive coating, which comprises the following raw materials in weight percentage: 620 to 70 percent of component A and 30 to 40 percent of component B; the component A comprises 38 to 42 parts of waterborne epoxy resin emulsion, 12 to 15 parts of styrene-acrylic emulsion, 7 to 10 parts of modified graphene reinforced silicon magnesium gel, 9 to 11 parts of attapulgite, 6 to 8 parts of mica powder, 1.8 to 2.2 parts of silane coupling agent a-172, 1.3 to 1.6 parts of defoamer, 0.8 to 1.3 parts of emulsifier, 1.2 to 1.5 parts of flexibilizer, 0.8 to 1.2 parts of smoothing agent, 0.2 to 0.4 parts of smoothing assistant, 0.5 to 0.8 parts of mildew preventive, 0.6 to 0.9 parts of corrosion inhibitor, 0.3 to 0.7 parts of electrostatic conducted assistant and 2.5 to 2.8 parts of mixed pigment in parts by weight; the component B comprises 0.8 to 1.2 parts of polyether amine, 3 to 5 parts of propanediol butyl ether and 6 to 9 parts of deionized water in parts by weight.
Description
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint.
Background technology
Water-based static conductive corrosion-resistant epoxy paint, compared with solvent based coating, has significant ecological, environmental protective advantage and price advantage, and especially in energy-saving and emission-reduction, it is nontoxic, nonirritant taste, pollution-free, non-volatile objectionable impurities; Do not fire not quick-fried, construction safety is convenient, and workmen washes one's hands with chemical cleaning project instrument without the need to using solvent-borne type thinner, and water-based static conductive corrosion-resistant epoxy paint improves resistance performance, the workability of water-borne coatings further.And along with universe's energy-saving and emission-reduction, protection home consciousness strengthen gradually, water-based static conductive corrosion-resistant epoxy paint more and more comes into one's own in heavy-duty coating technical field.Therefore, solve inferior position in some performances of water-based static conductive corrosion-resistant epoxy paint (as poor in sticking power, wear resisting property), solid basis more can be laid for its further genralrlization.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint, there is high adhesive force and excellent wear resisting property, and electrostatic conductive performance, antiseptic property are good, are a kind of water-based electrostatic conductive anticorrosion paints of good performance.
A kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint that the present invention proposes, its raw materials by weight comprises: component first 60-70%, component second 30-40%;
Component first comprises by weight: aqueous epoxy emulsion 38-42 part, benzene emulsion 12-15 part, and modified graphene strengthens silicon magnesium glue 7-10 part, attapulgite 9-11 part, mica powder 6-8 part, silane coupling A-1721.8-2.2 part, defoamer 1.3-1.6 part, emulsifying agent 0.8-1.3 part, toughner 1.2-1.5 part, advection agent 0.8-1.2 part, flow assistants 0.2-0.4 part, mould inhibitor 0.5-0.8 part, inhibiter 0.6-0.9 part, static conductive auxiliary agent 0.3-0.7 part, hybrid pigment 2.5-2.8 part;
Component second comprises by weight: polyetheramine 0.8-1.2 part, propandiol butyl ether 3-5 part, deionized water 6-9 part.
Preferably, in component first, the weight ratio of aqueous epoxy emulsion, benzene emulsion, modified graphene enhancing silicon magnesium glue, attapulgite, mica powder is 39-41:13-14:8-9:9.5-10:6.5-7.
Preferably, its raw materials by weight comprises: component first 63-68%, component second 32-37%;
Component first comprises by weight: aqueous epoxy emulsion 39-41 part, benzene emulsion 13-14 part, and modified graphene strengthens silicon magnesium glue 8-9 part, attapulgite 9.5-10 part, mica powder 6.5-7 part, silane coupling A-1721.9-2.1 part, defoamer 1.4-1.5 part, emulsifying agent 0.9-1.2 part, toughner 1.3-1.4 part, advection agent 0.9-1.1 part, flow assistants 0.3-0.4 part, mould inhibitor 0.6-0.7 part, inhibiter 0.7-0.8 part, static conductive auxiliary agent 0.4-0.5 part, hybrid pigment 2.6-2.7 part;
Component second comprises by weight: polyetheramine 0.9-1 part, propandiol butyl ether 3.5-4 part, deionized water 7-8 part.
Preferably, in the aqueous epoxy emulsion of component first, the oxirane value of epoxy resin is 0.15-0.2.
Preferably, in component first, antirust hybrid pigment is mixed by weight 3-5:1-2 by zinc oxide, composite iron-titanium powder.
Preferably, modified graphene strengthens silicon magnesium glue by following technique preparation: graphite, saltpetre are dropped in sulphuric acid soln, add potassium permanganate after stirring, leave standstill and obtain solution A; Solution A and superoxol are added in deionized water and leave standstill, washing, spraying dry obtains graphene oxide; After graphene oxide, carbon nanotube are put into silica tube, heat up, after insulation, cooling obtains modified graphene; After water glass is added magnesium chloride solution, heat up, leave standstill and obtain solution B; In solution B, drop into modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Preferably, modified graphene strengthens silicon magnesium glue to be prepared by following technique: be in the sulphuric acid soln of 25-30wt% by graphite, saltpetre input massfraction, and add potassium permanganate after stirring, standing 8-10h obtains solution A; The superoxol being 35-38wt% by solution A and massfraction adds in deionized water, after leaving standstill 2-3h, and washing, spraying dry obtains graphene oxide; After graphene oxide, carbon nanotube are put into silica tube, be warming up to 1150-1180 DEG C, after insulation 3-5min, cooling obtains modified graphene; Water glass being added 30-33 part massfraction is after the magnesium chloride solution of 7-10wt%, then put into temperature be 70-80 DEG C thermostatic equipment leave standstill 10-12h obtain solution B; In solution B, drop into modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Preferably, modified graphene strengthens silicon magnesium glue to be prepared by following technique: be in the sulphuric acid soln of 25-30wt% by 5-8 part graphite, 5-8 part saltpetre input 15-18 part massfraction by weight, add 7-9 part potassium permanganate after stirring, standing 8-10h obtains solution A; The superoxol being 35-38wt% by solution A and 12-15 part massfraction adds in 55-60 part deionized water, after leaving standstill 2-3h, and washing, spraying dry obtains graphene oxide; After 15-18 part graphene oxide, 2-3 part carbon nanotube are put into silica tube, be warming up to 1150-1180 DEG C, after insulation 3-5min, cooling obtains modified graphene; 12-15 part water glass being added 30-33 part massfraction is after the magnesium chloride solution of 7-10wt%, then put into temperature be 70-80 DEG C thermostatic equipment leave standstill 10-12h obtain solution B; In solution B, drop into 5-8 part modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Preferably, modified graphene strengthens in the preparation process of silicon magnesium glue, and dry temperature is 95-98 DEG C, and the dry time is 7-8h.
The present invention adopts the aqueous epoxy emulsion of specific oxirane value in preparation process, benzene emulsion coordinates as filmogen, substantially increases sticking power of the present invention, wear resisting property and antiseptic property; The auxiliary modified graphene added strengthens silicon magnesium glue can be compatible admirably with unclassified stores of the present invention, further enhancing wear resisting property of the present invention, intensity, shock resistance and anti-corrosive and static conductive performance simultaneously, in its preparation process, graphite is placed in certain concentration saltpetre and sulphuric acid soln, can by graphite flake layer phased separation, then the potassium permanganate added can aggravate this process as catalyzer, thus forms even, smooth graphene sheet layer; The certain concentration superoxol oxidation capacity of then adding is extremely strong, can enter among Graphene by great amount of hydroxy group cuttage; And in ensuing washing, water molecules can insert in graphene sheet layer gradually, thus obtain homodisperse graphene oxide water solution, then when the graphene oxide that obtains of spraying dry and carbon nanotube are put into silica tube and heat, the rapid spatial expansion dilatation of graphene oxide powder, can be compatible with unclassified stores better; And carbon nanotube is after pyroprocessing, the unstable carbon bonds cuttage of part enters in Graphene; The silicon magnesium glue that the magnesium chloride solution of water glass and certain concentration is mixed with in specific proportions had splendid adsorptive power, after adding modified graphene, further increase shock resistance and wear resisting property, simultaneously, the carbon bond formed through pyroprocessing by carbon nanotube due to cuttage in modified graphene, make modified graphene strengthen silicon magnesium glue and have splendid snappiness and ductility, being convenient to pulverizes and sieve forms modified graphene enhancing silicon magnesium glue finished product; And the interpolation of attapulgite, mica powder improves volume of the present invention, reduce cost, can, under the effect of silane coupling A-172, be evenly distributed in filmogen simultaneously, improve wear resisting property of the present invention further; The interpolation of static conductive auxiliary agent, makes filmogen of the present invention have excellent electrostatic conductive performance; Specified proportion zinc oxide, composite iron-titanium powder add as antirust hybrid pigment, not only increase antiseptic and rustproof property of the present invention, can also make pure color of the present invention, be convenient to use.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
A kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint that the present invention proposes, its raw materials by weight comprises: component first 60%, component second 40%;
Component first comprises by weight: aqueous epoxy emulsion 42 parts, benzene emulsion 12 parts, and modified graphene strengthens 10 parts, silicon magnesium glue, attapulgite 9 parts, mica powder 8 parts, silane coupling A-1721.8 parts, defoamer 1.6 parts, emulsifying agent 0.8 part, toughner 1.5 parts, advection agent 0.8 part, flow assistants 0.4 part, mould inhibitor 0.5 part, inhibiter 0.9 part, static conductive auxiliary agent 0.3 part, hybrid pigment 2.8 parts; Wherein, in aqueous epoxy emulsion, the oxirane value of epoxy resin is 0.15; Antirust hybrid pigment is mixed by weight 5:1 by zinc oxide, composite iron-titanium powder;
Component second comprises by weight: polyetheramine 1.2 parts, propandiol butyl ether 3 parts, deionized water 9 parts;
Modified graphene strengthens silicon magnesium glue to be prepared by following technique: by weight 5 parts of graphite, 8 parts of saltpetre being dropped into 15 parts of massfractions is in the sulphuric acid soln of 30wt%, and add 7 parts of potassium permanganate after stirring, standing 10h obtains solution A; The superoxol being 38wt% by solution A and 12 parts of massfractions adds in 55 parts of deionized waters, after leaving standstill 3h, and washing, spraying dry obtains graphene oxide; After 15 parts of graphene oxides, 3 parts of carbon nanotubes are put into silica tube, be warming up to 1150 DEG C, after insulation 5min, cooling obtains modified graphene; 12 parts of water glass being added 33 parts of massfractions is after the magnesium chloride solution of 7wt%, then put into temperature be 80 DEG C thermostatic equipment leave standstill 10h obtain solution B; In solution B, drop into 8 parts of modified graphenes, after stirring, 95 DEG C of dry 8h, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Embodiment 2
A kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint that the present invention proposes, its raw materials by weight comprises: component first 70%, component second 30%;
Component first comprises by weight: aqueous epoxy emulsion 38 parts, benzene emulsion 15 parts, and modified graphene strengthens 7 parts, silicon magnesium glue, attapulgite 11 parts, mica powder 6 parts, silane coupling A-1722.2 parts, defoamer 1.3 parts, emulsifying agent 1.3 parts, toughner 1.2 parts, advection agent 1.2 parts, flow assistants 0.2 part, mould inhibitor 0.8 part, inhibiter 0.6 part, static conductive auxiliary agent 0.7 part, hybrid pigment 2.5 parts; Wherein, in aqueous epoxy emulsion, the oxirane value of epoxy resin is 0.2; Antirust hybrid pigment is mixed by weight 3:2 by zinc oxide, composite iron-titanium powder;
Component second comprises by weight: polyetheramine 0.8 part, propandiol butyl ether 5 parts, deionized water 6 parts;
Modified graphene strengthens silicon magnesium glue to be prepared by following technique: by weight 8 parts of graphite, 5 parts of saltpetre being dropped into 18 parts of massfractions is in the sulphuric acid soln of 25wt%, and add 9 parts of potassium permanganate after stirring, standing 8h obtains solution A; The superoxol being 35wt% by solution A and 15 parts of massfractions adds in 60 parts of deionized waters, after leaving standstill 2h, and washing, spraying dry obtains graphene oxide; After 18 parts of graphene oxides, 2 parts of carbon nanotubes are put into silica tube, be warming up to 1180 DEG C, after insulation 3min, cooling obtains modified graphene; 15 parts of water glass being added 30 parts of massfractions is after the magnesium chloride solution of 10wt%, then put into temperature be 70 DEG C thermostatic equipment leave standstill 12h obtain solution B; In solution B, drop into 5 parts of modified graphenes, after stirring, 98 DEG C of dry 7h, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Embodiment 3
A kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint that the present invention proposes, its raw materials by weight comprises: component first 63%, component second 37%;
Component first comprises by weight: aqueous epoxy emulsion 41 parts, benzene emulsion 13 parts, and modified graphene strengthens 9 parts, silicon magnesium glue, attapulgite 9.5 parts, mica powder 7 parts, silane coupling A-1721.9 parts, defoamer 1.5 parts, emulsifying agent 0.9 part, toughner 1.4 parts, advection agent 0.9 part, flow assistants 0.4 part, mould inhibitor 0.6 part, inhibiter 0.8 part, static conductive auxiliary agent 0.4 part, hybrid pigment 2.7 parts;
Component second comprises by weight: polyetheramine 0.9 part, propandiol butyl ether 4 parts, deionized water 7 parts;
Modified graphene strengthens silicon magnesium glue to be prepared by following technique: by weight 6 parts of graphite, 7 parts of saltpetre being dropped into 16 parts of massfractions is in the sulphuric acid soln of 28wt%, and add 7.8 parts of potassium permanganate after stirring, standing 9.5h obtains solution A; The superoxol being 37wt% by solution A and 13 parts of massfractions adds in 56 parts of deionized waters, after leaving standstill 2.6h, and washing, spraying dry obtains graphene oxide; After 16 parts of graphene oxides, 2.8 parts of carbon nanotubes are put into silica tube, be warming up to 1160 DEG C, after insulation 4.5min, cooling obtains modified graphene; 13 parts of water glass being added 32 parts of massfractions is after the magnesium chloride solution of 8wt%, then put into temperature be 76 DEG C thermostatic equipment leave standstill 10.8h obtain solution B; In solution B, drop into 7 parts of modified graphenes, after stirring, 96 DEG C of dry 7.7h, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
Embodiment 4
A kind of high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint that the present invention proposes, its raw materials by weight comprises: component first 68%, component second 32%;
Component first comprises by weight: aqueous epoxy emulsion 39 parts, benzene emulsion 14 parts, and modified graphene strengthens 8 parts, silicon magnesium glue, attapulgite 10 parts, mica powder 6.5 parts, silane coupling A-1722.1 parts, defoamer 1.4 parts, emulsifying agent 1.2 parts, toughner 1.3 parts, advection agent 1.1 parts, flow assistants 0.3 part, mould inhibitor 0.7 part, inhibiter 0.7 part, static conductive auxiliary agent 0.5 part, hybrid pigment 2.6 parts;
Component second comprises by weight: polyetheramine 1 part, propandiol butyl ether 3.5 parts, deionized water 8 parts;
Modified graphene strengthens silicon magnesium glue to be prepared by following technique: by weight 7 parts of graphite, 6 parts of saltpetre being dropped into 17 parts of massfractions is in the sulphuric acid soln of 26wt%, and add 8.6 parts of potassium permanganate after stirring, standing 8.5h obtains solution A; The superoxol being 36wt% by solution A and 14 parts of massfractions adds in 58 parts of deionized waters, after leaving standstill 2.2h, and washing, spraying dry obtains graphene oxide; After 17 parts of graphene oxides, 2.4 parts of carbon nanotubes are put into silica tube, be warming up to 1170 DEG C, after insulation 3.5min, cooling obtains modified graphene; 14 parts of water glass being added 31 parts of massfractions is after the magnesium chloride solution of 9wt%, then put into temperature be 74 DEG C thermostatic equipment leave standstill 11.2h obtain solution B; In solution B, drop into 6 parts of modified graphenes, after stirring, 97 DEG C of dry 7.3h, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (9)
1. a high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint, is characterized in that, its raw materials by weight comprises: component first 60-70%, component second 30-40%;
Component first comprises by weight: aqueous epoxy emulsion 38-42 part, benzene emulsion 12-15 part, and modified graphene strengthens silicon magnesium glue 7-10 part, attapulgite 9-11 part, mica powder 6-8 part, silane coupling A-1721.8-2.2 part, defoamer 1.3-1.6 part, emulsifying agent 0.8-1.3 part, toughner 1.2-1.5 part, advection agent 0.8-1.2 part, flow assistants 0.2-0.4 part, mould inhibitor 0.5-0.8 part, inhibiter 0.6-0.9 part, static conductive auxiliary agent 0.3-0.7 part, hybrid pigment 2.5-2.8 part;
Component second comprises by weight: polyetheramine 0.8-1.2 part, propandiol butyl ether 3-5 part, deionized water 6-9 part.
2. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to claim 1, it is characterized in that, in component first, the weight ratio of aqueous epoxy emulsion, benzene emulsion, modified graphene enhancing silicon magnesium glue, attapulgite, mica powder is 39-41:13-14:8-9:9.5-10:6.5-7.
3. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to claim 1 or 2, it is characterized in that, its raw materials by weight comprises: component first 63-68%, component second 32-37%;
Component first comprises by weight: aqueous epoxy emulsion 39-41 part, benzene emulsion 13-14 part, and modified graphene strengthens silicon magnesium glue 8-9 part, attapulgite 9.5-10 part, mica powder 6.5-7 part, silane coupling A-1721.9-2.1 part, defoamer 1.4-1.5 part, emulsifying agent 0.9-1.2 part, toughner 1.3-1.4 part, advection agent 0.9-1.1 part, flow assistants 0.3-0.4 part, mould inhibitor 0.6-0.7 part, inhibiter 0.7-0.8 part, static conductive auxiliary agent 0.4-0.5 part, hybrid pigment 2.6-2.7 part;
Component second comprises by weight: polyetheramine 0.9-1 part, propandiol butyl ether 3.5-4 part, deionized water 7-8 part.
4. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-3, is characterized in that, in the aqueous epoxy emulsion of component first, the oxirane value of epoxy resin is 0.15-0.2.
5. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-4, is characterized in that, in component first, antirust hybrid pigment is mixed by weight 3-5:1-2 by zinc oxide, composite iron-titanium powder.
6. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-5, it is characterized in that, modified graphene strengthens silicon magnesium glue by following technique preparation: graphite, saltpetre are dropped in sulphuric acid soln, add potassium permanganate after stirring, leave standstill and obtain solution A; Solution A and superoxol are added in deionized water and leave standstill, washing, spraying dry obtains graphene oxide; After graphene oxide, carbon nanotube are put into silica tube, heat up, after insulation, cooling obtains modified graphene; After water glass is added magnesium chloride solution, heat up, leave standstill and obtain solution B; In solution B, drop into modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
7. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-6, it is characterized in that, modified graphene strengthens silicon magnesium glue to be prepared by following technique: be in the sulphuric acid soln of 25-30wt% by graphite, saltpetre input massfraction, add potassium permanganate after stirring, standing 8-10h obtains solution A; The superoxol being 35-38wt% by solution A and massfraction adds in deionized water, after leaving standstill 2-3h, and washing, spraying dry obtains graphene oxide; After graphene oxide, carbon nanotube are put into silica tube, be warming up to 1150-1180 DEG C, after insulation 3-5min, cooling obtains modified graphene; Water glass being added 30-33 part massfraction is after the magnesium chloride solution of 7-10wt%, then put into temperature be 70-80 DEG C thermostatic equipment leave standstill 10-12h obtain solution B; In solution B, drop into modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
8. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-7, it is characterized in that, modified graphene strengthens silicon magnesium glue to be prepared by following technique: be in the sulphuric acid soln of 25-30wt% by 5-8 part graphite, 5-8 part saltpetre input 15-18 part massfraction by weight, add 7-9 part potassium permanganate after stirring, standing 8-10h obtains solution A; The superoxol being 35-38wt% by solution A and 12-15 part massfraction adds in 55-60 part deionized water, after leaving standstill 2-3h, and washing, spraying dry obtains graphene oxide; After 15-18 part graphene oxide, 2-3 part carbon nanotube are put into silica tube, be warming up to 1150-1180 DEG C, after insulation 3-5min, cooling obtains modified graphene; 12-15 part water glass being added 30-33 part massfraction is after the magnesium chloride solution of 7-10wt%, then put into temperature be 70-80 DEG C thermostatic equipment leave standstill 10-12h obtain solution B; In solution B, drop into 5-8 part modified graphene, after stirring, dry, cooling, pulverizes, and sieves and obtains modified graphene enhancing silicon magnesium glue.
9. high adhesive force abrasion-resistance water electrostatic conductive anticorrosion paint according to any one of claim 1-8, is characterized in that, modified graphene strengthens in the preparation process of silicon magnesium glue, and dry temperature is 95-98 DEG C, and the dry time is 7-8h.
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