CN105133048B - A kind of cocoon cooking reeling agent and its application suitable for infra-red drying silk piece - Google Patents
A kind of cocoon cooking reeling agent and its application suitable for infra-red drying silk piece Download PDFInfo
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- CN105133048B CN105133048B CN201510655434.XA CN201510655434A CN105133048B CN 105133048 B CN105133048 B CN 105133048B CN 201510655434 A CN201510655434 A CN 201510655434A CN 105133048 B CN105133048 B CN 105133048B
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- Prior art keywords
- cocoon
- silk
- reeling agent
- reeling
- agent
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- 238000010411 cooking Methods 0.000 title claims abstract description 25
- 238000007603 infrared drying Methods 0.000 title claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 37
- 238000001764 infiltration Methods 0.000 claims abstract description 18
- 230000008595 infiltration Effects 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 18
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- -1 acids salt Chemical class 0.000 claims abstract description 6
- 239000002253 acid Substances 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 125000000129 anionic group Chemical group 0.000 claims description 3
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- 229910052731 fluorine Inorganic materials 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 238000009738 saturating Methods 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 8
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 description 8
- 229920001451 polypropylene glycol Polymers 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 150000001349 alkyl fluorides Chemical class 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Polyurethanes Or Polyureas (AREA)
- Woven Fabrics (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
The invention discloses a kind of cocoon cooking reeling agent suitable for infra-red drying silk piece and its application, the reeling agent can use in the vacuum infiltration process of the cocoon cooking for the raw material cocoon that reelability percentage is 35%~65%.The composition of reeling agent includes：50~200ppm fluoroalkylsulfonic acids salt, 200~500ppm alkyl polyoxyethylene ether and 10~150ppm PPG.Above-mentioned application is：By the vacuum infiltration process of cocoon cooking, reeling agent is drawn into silk cocoon, obtains the vacuum infiltration silk cocoon containing reeling agent.And technique progress cocoon cooking that can be same with the vacuum infiltration cocoon without reeling agent and filature.Using the silk cocoon filature containing reeling agent, the reelability percentage of silk cocoon can be made to improve 5%~10%.Be not in that feel is hardened and clean the problem of declining during with infrared drying silk piece.Preparation technology of the present invention is simple, and agents useful for same is nontoxic and content is extremely low, has fabulous effect to the silk cocoon for improving reelability percentage difference.
Description
Technical field
The present invention relates to the auxiliary agent in a kind of fiber tow production technical field, is that one kind is applied to infra-red drying specifically
The cocoon cooking reeling agent of silk piece and its application.
Background technology
Skein silk drying is indispensable link in Primary Processing.It is small in either conventional filature, it is bigSilk piece, also
It is big in the short route filature that filature rereeling is combined into oneSilk piece or boil reel silk from cocoons unification filature in silk piece, have to pass through
Subsequent production could be carried out after certain drying.At present, conventional silk piece heat drying is heated using traditional steam pipe mostly
Form.Its technological process is：--- steam transmitting pipe, heating tube --- vehicle cabin air --- dry silk piece to steam (thermal source).This
Kind drying principles mainly by " conduction ", the heat transfer form of " convection current ", transfer thermal energy to a piece, reach drying purpose,
But the problems such as thermal efficiency is relatively low, energy consumption is big, workshop temperature is high be present.Steaming is produced to overcome existing skein silk drying to rely on boiler fired coal
The drawbacks of vapour is to dry present in a piece, recently, the new technology for thering is enterprise to begin to use infrared drying silk piece, greatly reduce
Energy consumption.For the silk cocoon of routine, the cocoon cooking process in infra-red drying Si Pianduiqian roads does not require particularly.But for a small number of unwinding
The particularly poor silk cocoon needed with cocoon cooking reeling agent, using the salt such as cocoon cooking such as sodium carbonate, sodium phosphate, sodium metasilicate for commonly using alkalescence
After helping reeling agent, when using the infrared drying silk blade technolgy of radiant heating, tend to make the feel of the silk piece of drying inclined
Firmly, or even there is the phenomenon of isstudied decline, and do not have to reeling agent, often influence normal production.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of cocoon cooking solution suitable for infra-red drying silk piece
Easypro agent and its application.
The purpose of the present invention is achieved through the following technical solutions：A kind of cocoon cooking suitable for infra-red drying silk piece is unwinding
Agent, by 50~200ppm fluoroalkylsulfonic acids salt, 200~500ppm alkyl polyoxyethylene ether and 10~150ppm polyethers
Polyalcohol is dissolved in vacuum infiltration with being obtained after water.
Further, the fluoroalkylsulfonic acids salt can be anionic or nonionic.
The application of above-mentioned reeling agent is：By the vacuum infiltration process of cocoon cooking, reeling agent is drawn into reelability percentage as 30%
In~65% raw material cocoon, the reelability percentage of silk cocoon is improved.
The beneficial effects of the present invention are：Reeling agent provided by the present invention is nontoxic and various constituent contents are extremely low, can make
The reelability percentage of silk cocoon improves 5%~10%, makes it normally to produce, and using after reeling agent, does not influence to give birth in infra-red drying
The feel and isstudied of silk, be not in that feel is hardened and clean the problem of declining.
Embodiment
A kind of cocoon cooking reeling agent suitable for infra-red drying silk piece of the invention, it can be 30%~65% in reelability percentage
Used in the vacuum infiltration process of the cocoon cooking of raw material cocoon.First, by 50~200ppm fluoroalkylsulfonic acids salt, 200~500ppm
The concentration of alkyl polyoxyethylene ether and 10~150ppm PPGs is dissolved in the water of vacuum infiltration, and preparation obtains unwinding
Agent；Secondly, by the vacuum infiltration process of cocoon cooking, the reeling agent prepared is drawn into silk cocoon, obtained containing reeling agent
Vacuum infiltration silk cocoon.And technique progress cocoon cooking that can be same with the vacuum infiltration cocoon without reeling agent and filature.Using containing
There is the silk cocoon filature of reeling agent, the reelability percentage of silk cocoon can be made to improve 5%~10%.During with infrared drying silk piece, it will not go out
Existing feel is hardened the problem of declining with isstudied.Preparation technology of the present invention is simple, and agents useful for same is nontoxic and content is extremely low, to changing
The silk cocoon of kind reelability percentage difference has fabulous effect.
The present invention is specifically described below according to embodiment.
Embodiment 1
The raw material of selection is that reelability percentage is 40%, and isstudied is 95 points of spring cocoon in 2014, by anionic alkyl fluoride
Base sulfonate, alkyl polyoxyethylene ether and PPG are that 200ppm, 500ppm and 150ppm are separately added into cocoon cooking by concentration
In the vacuum water of vacuum process, stir after, using routine vacuum technology make silk cocoon suck the water containing reeling agent, and
Silk cocoon after vacuum infiltration is subjected to cocoon cooking and filature by the technique same with the vacuum infiltration cocoon without reeling agent.Filature and multiple
Shake process and use infrared drying silk piece.Determined by 400 reelability percentages, reelability percentage the improving than cocoon quality identification of silk cocoon
15%, isstudied improves 1 point, is 96 points, and soft, determined through hard and soft, Stiffness 2.5%.
Embodiment 2
The raw material of selection is that reelability percentage is 65%, and isstudied is 96.5 points of autumn cocoon in 2014, and anionic is fluorinated
Alkylsulfonate, alkyl polyoxyethylene ether and PPG are that 50ppm, 200ppm and 10ppm are separately added into cocoon cooking by concentration
In the vacuum water of vacuum process, stir after, using routine vacuum technology make silk cocoon suck the water containing reeling agent, and
Silk cocoon after vacuum infiltration is subjected to cocoon cooking and filature by the technique same with the vacuum infiltration cocoon without reeling agent.Using filature
The two-in-one new technology filature of rereeling, silk piece are dried with infra-red drying method.Determined by 400 reelability percentages, silk cocoon it is unwinding
Rate improves 5% than cocoon quality identification, and isstudied maintains an equal level, and is 96.5 points, and soft, is surveyed through hard and soft, Stiffness
1.1%.
Embodiment 3
The raw material of selection is that reelability percentage is 52%, and isstudied is 96 points of autumn cocoon in 2014, by nonionic alkyl fluoride
Base sulfonate, alkyl polyoxyethylene ether and PPG are that 100ppm, 300ppm and 100ppm are separately added into cocoon cooking by concentration
In the vacuum water of vacuum process, stir after, using routine vacuum technology make silk cocoon suck the water containing reeling agent, and
Silk cocoon after vacuum infiltration is subjected to cocoon cooking and filature by the technique same with the vacuum infiltration cocoon without reeling agent.Silk piece is with red
Outer drying means is dried.Determined by 400 reelability percentages, the reelability percentage of silk cocoon improves 10% than cocoon quality identification, it is clean into
Achievement maintains an equal level, and is 96.5 points, and soft, surveyed through hard and soft, Stiffness 2.3%.
Claims (3)
- A kind of 1. cocoon cooking reeling agent suitable for infra-red drying silk piece, it is characterised in that the reeling agent by 50 ~ 200ppm fluorine Change alkylsulfonate, 200 ~ 500 ppm alkyl polyoxyethylene ether and 10 ~ 150 ppm PPG and be dissolved in vacuum infiltration With being obtained after water.
- 2. reeling agent according to claim 1, it is characterised in that the fluoroalkylsulfonic acids salt be anionic or it is non-from Subtype.
- 3. the application of the reeling agent described in a kind of claim 1, it is characterised in that the application is：Oozed by the vacuum of cocoon cooking Saturating process, reeling agent is drawn into raw material cocoon of the reelability percentage for the % of 30 % ~ 65, improves the reelability percentage of silk cocoon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510655434.XA CN105133048B (en) | 2015-10-12 | 2015-10-12 | A kind of cocoon cooking reeling agent and its application suitable for infra-red drying silk piece |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510655434.XA CN105133048B (en) | 2015-10-12 | 2015-10-12 | A kind of cocoon cooking reeling agent and its application suitable for infra-red drying silk piece |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105133048A CN105133048A (en) | 2015-12-09 |
| CN105133048B true CN105133048B (en) | 2018-02-16 |
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| CN201510655434.XA Active CN105133048B (en) | 2015-10-12 | 2015-10-12 | A kind of cocoon cooking reeling agent and its application suitable for infra-red drying silk piece |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105546938A (en) * | 2015-12-31 | 2016-05-04 | 浙江理工大学 | Method for preventing raw silk damage through infrared drying |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103225112B (en) * | 2013-05-17 | 2016-05-11 | 安徽绩溪县花神丝绸有限公司 | A kind of silk cocoon cocoons-boiling method cleaning |
| CN103882533B (en) * | 2014-03-18 | 2016-05-18 | 上林县中兴丝业有限公司 | A kind of method that improves raw silk reelability percentage |
| CN104480536B (en) * | 2014-11-14 | 2016-10-26 | 安徽省广德新丰丝绸有限公司 | A kind of automatic silk reeling production and application reeling agent |
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| CN105133048A (en) | 2015-12-09 |
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