CN105062308A - Heatproof corrosion-resistant aqueous epoxy resin coating for ships - Google Patents
Heatproof corrosion-resistant aqueous epoxy resin coating for ships Download PDFInfo
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- CN105062308A CN105062308A CN201510473837.2A CN201510473837A CN105062308A CN 105062308 A CN105062308 A CN 105062308A CN 201510473837 A CN201510473837 A CN 201510473837A CN 105062308 A CN105062308 A CN 105062308A
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Abstract
The invention discloses a heatproof corrosion-resistant aqueous epoxy resin coating for ships. The heatproof corrosion-resistant aqueous epoxy resin coating comprises an ingredient A and an ingredient B and a weight ratio of the ingredient A to the ingredient B is 100: 1-2. The ingredient A comprises, by weight, 5-15 parts of epoxy resin E-44, 30-40 parts of siloxane-modified epoxy resin, 20-40 parts of novolac epoxy, 1-2 parts of aliphatic acid, 10-18 parts of alumina silicate, 5-10 parts of polypyrrole hollow balls, 2-8 parts of barium sulfate, 2-6 parts of titanium dioxide microspheres, 2-5 parts of powdered steatile, 1-3 parts of lithium-based bentonite, 1-4 parts of zinc oxide, 2-8 parts of zinc phosphate, 1-3 parts of aluminum triphosphate, 10-20 parts of polyvinyl alcohol, 1-3 parts of a dispersant, 1-3 parts of an antifoaming agent, 1-3 parts of a wetting agent, 1-3 parts of a leveling agent, and 20-40 parts of deionized water. The ingredient B comprises, by weight, 5-15 parts of triethylene tetramine, 10-20 parts of m-xylylenediamine, 1-2 parts of propylene glycol monomethyl ether acetate, 1-3 parts of 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate and 10-20 parts of deionized water.
Description
Technical field
The present invention relates to marine finish technical field, particularly relate to a kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint.
Background technology
Along with the development of shipping industry, hull bottom, inner cabin of ship due to long-term submergence in the seawater, the original preservative coat of structure is wrecked, produces corrosion, and these structures are difficult to move to land and keep in repair.In order to extend the work-ing life of these boats and ships, ensure safety in production, need at employing marine surface coating anticorrosive coating, to prevent the corrosion of all kinds of water surrounding, the mechanical property of current marine finish, corrosion resistance nature and sticking power also do not reach demand.
Summary of the invention
The present invention proposes a kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, mechanical property is good, and erosion resistance and sticking power are very excellent.
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint that the present invention proposes, comprise component A and B component, the weight ratio of component A and B component is 100:1-2;
The raw material of component A comprises by weight: epoxy resin E-44 5-15 part, silicone-modified epoxy resin 30-40 part, novolac epoxy 20-40 part, lipid acid 1-2 part, pure aluminium silicate 10-18 part, polypyrrole hollow ball 5-10 part, barium sulfate 2-8 part, titanium dioxide microballoon sphere 2-6 part, talcum powder 2-5 part, lithium bentonite 1-3 part, zinc oxide 1-4 part, zinc phosphate 2-8 part, aluminium triphosphate 1-3 part, polyvinyl alcohol 10-20 part, dispersion agent 1-3 part, defoamer 1-3 part, wetting agent 1-3 part, flow agent 1-3 part, deionized water 20-40 part;
The raw material of B component comprises by weight: triethylene tetramine 5-15 part, m-xylene diamine 10-20 part, 1-Methoxy-2-propyl acetate 1-2 part, alcohol ester 12 1-3 part, deionized water 10-20 part.
Preferably, in silicone-modified epoxy resin, by weight by 50-80 part bisphenol-S diglycidyl ether, 5-10 part polysiloxane is sent in 100 parts of xylene solutions and is stirred, whipping temp is 40-60 DEG C, churning time is 40-50min, add 15-30 part polytetrahydrofuran polyol to continue to stir 5-15min, whipping temp is 68-74 DEG C, add 0.2-0.8 part propenyl triethoxyl silane, 0.1-0.2 part aminopropyl triethoxysilane continues to stir 10-20min, whipping temp is 80-92 DEG C, filter, send in vacuum drying oven and carry out drying, drying temperature is 120-140 DEG C, time of drying is 1-2h, pulverize, obtain silicone-modified epoxy resin.
Preferably, in bisphenol-S diglycidyl ether, epoxy equivalent (weight) is 280-300g/mol, and softening temperature is 93-96 DEG C.
Preferably, the weight ratio of bisphenol-S diglycidyl ether, polysiloxane, polytetrahydrofuran polyol, propenyl triethoxyl silane and aminopropyl triethoxysilane is 50-80:5-10:15-30:0.2-0.8:0.1-0.2.
Preferably, the weight ratio of epoxy resin E-44, silicone-modified epoxy resin and novolac epoxy is 10-13:26-28:30-36.
Preferably, the weight ratio of triethylene tetramine and m-xylene diamine is 10-13:14-16.
Preferably, in the raw material of component A, epoxy resin E-44 10-13 part, silicone-modified epoxy resin 26-28 part, novolac epoxy 30-36 part, lipid acid 1.2-1.5 part, pure aluminium silicate 14-16 part, polypyrrole hollow ball 7-9 part, barium sulfate 5-6 part, titanium dioxide microballoon sphere 4-5 part, talcum powder 4-4.6 part, lithium bentonite 2-2.5 part, aluminium triphosphate 2-2.4 part, zinc oxide 2-3 part, zinc phosphate 4-5 part, polyvinyl alcohol 16-18 part, dispersion agent 2-2.4 part, defoamer 2-2.6 part, wetting agent 2-2.5 part, flow agent 2-2.6 part, deionized water 30-36 part.
Preferably, in the raw material of B component, triethylene tetramine 10-13 part, m-xylene diamine 14-16 part, 1-Methoxy-2-propyl acetate 1.2-1.6 part, alcohol ester 12 1.5-2.5 part, deionized water 14-18 part.
In the present invention, the preparation process of component A is: epoxy resin E-44, silicone-modified epoxy resin, novolac epoxy, lipid acid, pure aluminium silicate, polypyrrole hollow ball, aluminium triphosphate, zinc oxide, zinc phosphate, polyvinyl alcohol, dispersion agent, defoamer, wetting agent, flow agent, deionized water are mixed in rear feeding three-roller and ground, extremely wherein solids particle diameter is 10-30 μm, add barium sulfate again, titanium dioxide microballoon sphere, talcum powder, lithium bentonite stir, add polypyrrole hollow ball to stir, filter, obtain component A;
The preparation process of B component is: triethylene tetramine, m-xylene diamine, 1-Methoxy-2-propyl acetate, alcohol ester 12, deionized water are mixed, obtain B component.
In the present invention, adopt epoxy resin E-44, silicone-modified epoxy resin and novolac epoxy are as major ingredient, and adopt triethylene tetramine, benzene dimethylamine synergy solidifying agent, the sticking power of goods and coated substrate is fabulous, excellent in mechanical performance, and corrosion resistance nature is better, add polypyrrole hollow ball, barium sulfate, titanium dioxide microballoon sphere, talcum powder and lithium bentonite are as filler, Mechanical Properties of Products is good, to coated substrate strong adhesion, and levelling property is better, wherein the cavity of polypyrrole hollow ball inner sealing has deformability, with epoxy resin E-44, silicone-modified epoxy resin and novolac epoxy synergy can obviously strengthen goods impact strength and toughness, mechanical property is better, and can not move in reproduced goods, mechanical property is lasting, act synergistically with titanium dioxide microballoon sphere, also coating and flow leveling can significantly be improved, lithium bentonite is laminate structure, with polypyrrole hollow ball, barium sulfate, titanium dioxide microballoon sphere, talcum powder acting in conjunction, lithium bentonite can make storeroom viscosity increase, and at epoxy resin E-44, the particle surface formation solvation film of silicone-modified epoxy resin and novolac epoxy and dimensional network structure are to support and to stop polypyrrole hollow ball, barium sulfate, titanium dioxide microballoon sphere, talcum powder sinks, not only can strengthen the bonding force of goods and coated substrate, and it is also very excellent at wet substrate surface sticking power, in silicone-modified epoxy resin, containing-SO in bisphenol-S diglycidyl ether
2-, its polarity is extremely strong, interacts with polysiloxane, and adopts consistency and the bonding force of both polytetrahydrofuran polyol, propenyl triethoxyl silane, aminopropyl triethoxysilane promotions, goods not only mechanical property are fabulous, and sticking power and antiseptic property strengthen further.
Rotproofness of the present invention, sticking power and mechanical property are fabulous, and levelling property is excellent, and smooth coating is smooth, has good protection effect to applied material surface.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, comprise component A and B component, the weight ratio of component A and B component is 100:1;
The raw material of component A comprises by weight: epoxy resin E-44 15 parts, silicone-modified epoxy resin 30 parts, novolac epoxy 40 parts, 1 part, lipid acid, pure aluminium silicate 18 parts, polypyrrole hollow ball 5 parts, 8 parts, barium sulfate, titanium dioxide microballoon sphere 2 parts, talcum powder 5 parts, lithium bentonite 1 part, 4 parts, zinc oxide, zinc phosphate 2 parts, aluminium triphosphate 3 parts, polyvinyl alcohol 10 parts, dispersion agent 3 parts, defoamer 1 part, wetting agent 3 parts, flow agent 1 part, deionized water 40 parts;
The raw material of B component comprises by weight: triethylene tetramine 5 parts, m-xylene diamine 20 parts, 1-Methoxy-2-propyl acetate 1 part, alcohol ester 12 parts, deionized water 10 parts.
Embodiment 2
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, comprise component A and B component, the weight ratio of component A and B component is 100:2;
The raw material of component A comprises by weight: epoxy resin E-44 5 parts, silicone-modified epoxy resin 40 parts, novolac epoxy 20 parts, 2 parts, lipid acid, pure aluminium silicate 10 parts, polypyrrole hollow ball 10 parts, 2 parts, barium sulfate, titanium dioxide microballoon sphere 6 parts, talcum powder 2 parts, lithium bentonite 3 parts, 1 part, zinc oxide, zinc phosphate 8 parts, aluminium triphosphate 1 part, polyvinyl alcohol 20 parts, dispersion agent 1 part, defoamer 3 parts, wetting agent 1 part, flow agent 3 parts, deionized water 20 parts;
The raw material of B component comprises by weight: triethylene tetramine 15 parts, m-xylene diamine 10 parts, 1-Methoxy-2-propyl acetate 2 parts, alcohol ester 12 parts, deionized water 20 parts.
Embodiment 3
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, comprise component A and B component, the weight ratio of component A and B component is 100:1.2;
The raw material of component A comprises by weight: epoxy resin E-44 13 parts, silicone-modified epoxy resin 26 parts, novolac epoxy 36 parts, 1.2 parts, lipid acid, pure aluminium silicate 16 parts, polypyrrole hollow ball 7 parts, 6 parts, barium sulfate, titanium dioxide microballoon sphere 4 parts, talcum powder 4.6 parts, lithium bentonite 2 parts, aluminium triphosphate 2.4 parts, 2 parts, zinc oxide, zinc phosphate 5 parts, polyvinyl alcohol 16 parts, dispersion agent 2.4 parts, defoamer 2 parts, wetting agent 2.5 parts, flow agent 2 parts, deionized water 36 parts;
The raw material of B component comprises by weight: triethylene tetramine 10 parts, m-xylene diamine 16 parts, 1-Methoxy-2-propyl acetate 1.2 parts, alcohol ester 12 parts, deionized water 14 parts.
In silicone-modified epoxy resin, by weight by 80 parts of bisphenol-S diglycidyl ethers, 5 parts of polysiloxane are sent in 100 parts of xylene solutions and are stirred, whipping temp is 60 DEG C, churning time is 40min, add 30 parts of polytetrahydrofuran polyol to continue to stir 5min, whipping temp is 74 DEG C, add 0.2 part of propenyl triethoxyl silane, 0.2 part of aminopropyl triethoxysilane continues to stir 10min, whipping temp is 92 DEG C, filter, send in vacuum drying oven and carry out drying, drying temperature is 120 DEG C, time of drying is 2h, pulverize, obtain silicone-modified epoxy resin.
In bisphenol-S diglycidyl ether, epoxy equivalent (weight) is 280g/mol, and softening temperature is 96 DEG C.
Embodiment 4
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, comprise component A and B component, the weight ratio of component A and B component is 100:1.8;
The raw material of component A comprises by weight: epoxy resin E-44 12 parts, silicone-modified epoxy resin 27 parts, novolac epoxy 33 parts, 1.4 parts, lipid acid, pure aluminium silicate 15 parts, polypyrrole hollow ball 8 parts, 5.6 parts, barium sulfate, titanium dioxide microballoon sphere 4.5 parts, talcum powder 4.3 parts, lithium bentonite 2.3 parts, aluminium triphosphate 2.2 parts, 2.3 parts, zinc oxide, zinc phosphate 4.5 parts, polyvinyl alcohol 17 parts, dispersion agent 2.2 parts, defoamer 2.3 parts, wetting agent 2.4 parts, flow agent 2.3 parts, deionized water 33 parts;
The raw material of B component comprises by weight: triethylene tetramine 12 parts, m-xylene diamine 15 parts, 1-Methoxy-2-propyl acetate 1.3 parts, alcohol ester 12 parts, deionized water 16 parts.
In silicone-modified epoxy resin, by weight by 60 parts of bisphenol-S diglycidyl ethers, 8 parts of polysiloxane are sent in 100 parts of xylene solutions and are stirred, whipping temp is 50 DEG C, churning time is 45min, add 20 parts of polytetrahydrofuran polyol to continue to stir 10min, whipping temp is 70 DEG C, add 0.5 part of propenyl triethoxyl silane, 0.12 part of aminopropyl triethoxysilane continues to stir 15min, whipping temp is 88 DEG C, filter, send in vacuum drying oven and carry out drying, drying temperature is 130 DEG C, time of drying is 1.2h, pulverize, obtain silicone-modified epoxy resin.
In bisphenol-S diglycidyl ether, epoxy equivalent (weight) is 290g/mol, and softening temperature is 95 DEG C.
Embodiment 5
A kind of boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, comprise component A and B component, the weight ratio of component A and B component is 100:1.5;
The raw material of component A comprises by weight: epoxy resin E-44 10 parts, silicone-modified epoxy resin 28 parts, novolac epoxy 30 parts, 1.5 parts, lipid acid, pure aluminium silicate 14 parts, polypyrrole hollow ball 9 parts, 5 parts, barium sulfate, titanium dioxide microballoon sphere 5 parts, talcum powder 4 parts, lithium bentonite 2.5 parts, aluminium triphosphate 2 parts, 3 parts, zinc oxide, zinc phosphate 4 parts, polyvinyl alcohol 18 parts, dispersion agent 2 parts, defoamer 2.6 parts, wetting agent 2 parts, flow agent 2.6 parts, deionized water 30 parts;
The raw material of B component comprises by weight: triethylene tetramine 13 parts, m-xylene diamine 14 parts, 1-Methoxy-2-propyl acetate 1.6 parts, alcohol ester 12 parts, deionized water 18 parts.
In silicone-modified epoxy resin, by weight by 50 parts of bisphenol-S diglycidyl ethers, 10 parts of polysiloxane are sent in 100 parts of xylene solutions and are stirred, whipping temp is 40 DEG C, churning time is 50min, add 15 parts of polytetrahydrofuran polyol to continue to stir 15min, whipping temp is 68 DEG C, add 0.8 part of propenyl triethoxyl silane, 0.1 part of aminopropyl triethoxysilane continues to stir 20min, whipping temp is 80 DEG C, filter, send in vacuum drying oven and carry out drying, drying temperature is 140 DEG C, time of drying is 1h, pulverize, obtain silicone-modified epoxy resin.
In bisphenol-S diglycidyl ether, epoxy equivalent (weight) is 300g/mol, and softening temperature is 93 DEG C.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (8)
1. a boats and ships heat-and corrosion-resistant aqueous epoxide resin paint, is characterized in that, comprises component A and B component, and the weight ratio of component A and B component is 100:1-2;
The raw material of component A comprises by weight: epoxy resin E-44 5-15 part, silicone-modified epoxy resin 30-40 part, novolac epoxy 20-40 part, lipid acid 1-2 part, pure aluminium silicate 10-18 part, polypyrrole hollow ball 5-10 part, barium sulfate 2-8 part, titanium dioxide microballoon sphere 2-6 part, talcum powder 2-5 part, lithium bentonite 1-3 part, zinc oxide 1-4 part, zinc phosphate 2-8 part, aluminium triphosphate 1-3 part, polyvinyl alcohol 10-20 part, dispersion agent 1-3 part, defoamer 1-3 part, wetting agent 1-3 part, flow agent 1-3 part, deionized water 20-40 part;
The raw material of B component comprises by weight: triethylene tetramine 5-15 part, m-xylene diamine 10-20 part, 1-Methoxy-2-propyl acetate 1-2 part, alcohol ester 12 1-3 part, deionized water 10-20 part.
2. boats and ships heat-and corrosion-resistant aqueous epoxide resin paint according to claim 1, it is characterized in that, in silicone-modified epoxy resin, by weight by 50-80 part bisphenol-S diglycidyl ether, 5-10 part polysiloxane is sent in 100 parts of xylene solutions and is stirred, whipping temp is 40-60 DEG C, churning time is 40-50min, add 15-30 part polytetrahydrofuran polyol to continue to stir 5-15min, whipping temp is 68-74 DEG C, add 0.2-0.8 part propenyl triethoxyl silane, 0.1-0.2 part aminopropyl triethoxysilane continues to stir 10-20min, whipping temp is 80-92 DEG C, filter, send in vacuum drying oven and carry out drying, drying temperature is 120-140 DEG C, time of drying is 1-2h, pulverize, obtain silicone-modified epoxy resin.
3. boats and ships heat-and corrosion-resistant aqueous epoxide resin paint according to claim 2, is characterized in that, in bisphenol-S diglycidyl ether, epoxy equivalent (weight) is 280-300g/mol, and softening temperature is 93-96 DEG C.
4. boats and ships heat-and corrosion-resistant aqueous epoxide resin paint according to claim 2, it is characterized in that, the weight ratio of bisphenol-S diglycidyl ether, polysiloxane, polytetrahydrofuran polyol, propenyl triethoxyl silane and aminopropyl triethoxysilane is 50-80:5-10:15-30:0.2-0.8:0.1-0.2.
5. the heat-and corrosion-resistant aqueous epoxide resin paint of the boats and ships according to any one of claim 1-4, is characterized in that, the weight ratio of epoxy resin E-44, silicone-modified epoxy resin and novolac epoxy is 10-13:26-28:30-36.
6. the heat-and corrosion-resistant aqueous epoxide resin paint of the boats and ships according to any one of claim 1-5, is characterized in that, the weight ratio of triethylene tetramine and m-xylene diamine is 10-13:14-16.
7. the heat-and corrosion-resistant aqueous epoxide resin paint of the boats and ships according to any one of claim 1-6, it is characterized in that, in the raw material of component A, epoxy resin E-44 10-13 part, silicone-modified epoxy resin 26-28 part, novolac epoxy 30-36 part, lipid acid 1.2-1.5 part, pure aluminium silicate 14-16 part, polypyrrole hollow ball 7-9 part, barium sulfate 5-6 part, titanium dioxide microballoon sphere 4-5 part, talcum powder 4-4.6 part, lithium bentonite 2-2.5 part, aluminium triphosphate 2-2.4 part, zinc oxide 2-3 part, zinc phosphate 4-5 part, polyvinyl alcohol 16-18 part, dispersion agent 2-2.4 part, defoamer 2-2.6 part, wetting agent 2-2.5 part, flow agent 2-2.6 part, deionized water 30-36 part.
8. the heat-and corrosion-resistant aqueous epoxide resin paint of the boats and ships according to any one of claim 1-7, it is characterized in that, in the raw material of B component, triethylene tetramine 10-13 part, m-xylene diamine 14-16 part, 1-Methoxy-2-propyl acetate 1.2-1.6 part, alcohol ester 12 1.5-2.5 part, deionized water 14-18 part.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510473837.2A CN105062308A (en) | 2015-08-05 | 2015-08-05 | Heatproof corrosion-resistant aqueous epoxy resin coating for ships |
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| CN201510473837.2A CN105062308A (en) | 2015-08-05 | 2015-08-05 | Heatproof corrosion-resistant aqueous epoxy resin coating for ships |
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Cited By (7)
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| CN105385342A (en) * | 2015-11-24 | 2016-03-09 | 安徽省金盾涂料有限责任公司 | Aqueous weather-resisting polysiloxane coating |
| CN106349888A (en) * | 2016-08-27 | 2017-01-25 | 安徽省金盾涂料有限责任公司 | Anticorrosive epoxy coating resistant to high and low temperatures |
| CN109575746A (en) * | 2018-10-31 | 2019-04-05 | 安徽开林新材料股份有限公司 | A kind of marine water coating that surface is smooth |
| CN109608980A (en) * | 2018-10-31 | 2019-04-12 | 安徽开林新材料股份有限公司 | A kind of ship acid and alkali-resistance waterborne epoxy coatings preparation method |
| CN110294992A (en) * | 2019-06-21 | 2019-10-01 | 中国船舶重工集团公司第七一九研究所 | A kind of corrosion-resistant and high-temperature resistant coating peculiar to vessel and preparation method thereof |
| WO2021035905A1 (en) * | 2019-08-27 | 2021-03-04 | 中国船舶重工集团公司第七二五研究所 | Anti-rust weather-resistant functional gradient type bottom-face integrated coating, and method for preparing coating layer |
| CN116606581A (en) * | 2023-04-27 | 2023-08-18 | 厦门双瑞船舶涂料有限公司 | Lightweight high-solid epoxy heavy-duty anticorrosive paint and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105385342A (en) * | 2015-11-24 | 2016-03-09 | 安徽省金盾涂料有限责任公司 | Aqueous weather-resisting polysiloxane coating |
| CN106349888A (en) * | 2016-08-27 | 2017-01-25 | 安徽省金盾涂料有限责任公司 | Anticorrosive epoxy coating resistant to high and low temperatures |
| CN109575746A (en) * | 2018-10-31 | 2019-04-05 | 安徽开林新材料股份有限公司 | A kind of marine water coating that surface is smooth |
| CN109608980A (en) * | 2018-10-31 | 2019-04-12 | 安徽开林新材料股份有限公司 | A kind of ship acid and alkali-resistance waterborne epoxy coatings preparation method |
| CN110294992A (en) * | 2019-06-21 | 2019-10-01 | 中国船舶重工集团公司第七一九研究所 | A kind of corrosion-resistant and high-temperature resistant coating peculiar to vessel and preparation method thereof |
| WO2021035905A1 (en) * | 2019-08-27 | 2021-03-04 | 中国船舶重工集团公司第七二五研究所 | Anti-rust weather-resistant functional gradient type bottom-face integrated coating, and method for preparing coating layer |
| CN116606581A (en) * | 2023-04-27 | 2023-08-18 | 厦门双瑞船舶涂料有限公司 | Lightweight high-solid epoxy heavy-duty anticorrosive paint and preparation method thereof |
| CN116606581B (en) * | 2023-04-27 | 2024-03-01 | 厦门双瑞船舶涂料有限公司 | Lightweight high-solid epoxy heavy-duty anticorrosive paint and preparation method thereof |
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