CN105055261B - A kind of antipollution skin-protection product and preparation method thereof - Google Patents
A kind of antipollution skin-protection product and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to a kind of antipollution skin-protection products and preparation method thereof.A kind of antipollution skin-protection product and preparation method thereof more particularly to antifouling composition and containing the antifouling composition.A variety of natural plant compositions such as the be added to wing seed Moringa seed extract of antipollution skin-protection product of the present invention, trehalose, tremella polysaccharides; it plays a protective role to skin; repel positively charged atmospheric dust and the harmful heavy metal of complexing; mitigate skin to injure caused by due to atmosphere pollution; and cell can be protected, dehydration, cold and hot variation injury caused by skin can be reduced.
Description
Technical field
The invention belongs to cosmetic fields, more particularly to a kind of antipollution skin-protection product and preparation method thereof.
Background technology
As production and economic express delivery increase, the continuous deterioration of environment, air pollution constantly aggravates, the pollution of the mankind
Source is constantly increasing.What is be hurt is the skin of the mankind first, is accumulated over a long period, and the health of skin is corroded, and accelerates the aging of skin,
Cause a series of skin problem, the skin care item with anti-pollution can resist the damage of physics and chemical factor to skin
The ability that epidermis resists pollution is reinforced in evil, corrosion, and improving cell viability just seems particularly urgent.
Excessive ozone reduces the content of vitamin C and vitamin E in skin in air so that lipid peroxidation increases；
Vehicle exhaust and polycyclic aromatic hydrocarbon increase oxidative stress and cellular damage；The pollutant floated in air, it is easy to enter pore,
The serious update cycle for destroying cuticula and speed cause a series of skin problem, performance as follows：Capillary seriously expands
, there is apparent red blood silk, cutaneous sensibility increases, and is very easy to allergic reaction occur, the colour of skin is obscure, and spot colors add
Deep, microgroove increases.
Cosmetics on the market are by film forming component or addition ultraviolet light attractant, the pollution of air-isolation mostly at present
And anti-ultraviolet injury is supported, effect is relatively simple, cannot comprehensively resist various pollution sources, and resistant to pollution effect is not notable.
So developing a skin care item with antipollution, protection cell just becomes urgent in the extreme.
Invention content
In order to solve the above-mentioned problems in the prior art, the present invention provides one kind to invade specifically for atmosphere pollution etc.
Harmful antifouling composition, the antifouling composition can repel positively charged atmospheric dust and the harmful heavy metal of complexing, mitigate
Skin injures caused by due to atmosphere pollution.
Used technical solution is as follows in order to achieve the above technical purposes：
A kind of antifouling composition includes following component raw material according to weight：
Wing seed Moringa seed extract 50~83%；
Trehalose 15~49%；
Tremella polysaccharides 1~5%.
As a preferred embodiment, including following component raw material according to weight：
Wing seed Moringa seed extract 65~83%；
Trehalose 30~49%；
Tremella polysaccharides 2~5%.
Another technical object of the present invention is to provide a kind of antipollution skin-protection product, the antipollution skin-protection product contains
Antifouling composition is stated, weight percentage of the antifouling composition in the antipollution skin-protection product is 1~5%.
It is highly preferred that weight percentage of the antifouling composition in the antipollution skin-protection product is in the present invention
1.5~3%.
Further, the antipollution skin-protection product further includes foundation emulsion, and the foundation emulsion is according to weight
Including following component raw material：
In the present invention, it is preferable that one kind in aluminium-magnesium silicate, xanthans, carragheen, carbomer of the suspending agent or
Two or more substances；The preservative is selected from one or more of ethohexadiol, Phenoxyethanol, methylisothiazolinone
Substance；The moisturizer is selected from the substance of one or more of butanediol, 1,3-PD, sorbierite, glycine betaine.
In the present invention, it is preferable that the whitening agent is selected from silicon processing titanium dioxide and/or alpha-arbutin；The emollient
Substance selected from one or more of isononyl isononanoate, cyclopentasiloxane, lanolin, C12-15 alcohol benzoic ethers；
The colorant is selected from one or more of silicon processing iron oxide yellow, silicon processing iron oxide red, silicon processing iron oxide black
Composition；Film forming agent object one or more kinds of in trimethyl silicane alkoxy esters of silicon acis, polyethylene, cellulose
Matter；Emulsifier one kind or two in sorbitan sesquioleate, cetearyl glucoside, spermaceti oleth -10
Kind or more substance；Solvent substance one or more kinds of in water, ethyl alcohol, PEG-8.
Preferably, the silicon processing is to wrap up last layer ring five dimethyl silicone polymer in material surface to be treated,
The compatibility that titanium dioxide and grease can be increased in this way, can also increase iron oxide yellow, iron oxide red, iron oxide black and other
The compatibility of substance.
It is highly preferred that the grain size of the silicon processing titanium dioxide is 20~40 microns.Grain size is too small to be not easy to cover face's flaw
Defect, grain size is too big to be not easy to adhere to skin again.
Another technical purpose of the present invention is to provide a kind of preparation method of antipollution skin-protection product, includes the following steps：
The preparation of antifouling composition：Wing seed Moringa seed extract, trehalose and tremella polysaccharides are proportionally added into emulsification pot
In, it stirs evenly, it is spare to obtain component C；
2) preparation of foundation emulsions：It is added in water phase pot after suspending agent is soaked with moisturizer, opens stirring, sequentially add
Preservative and solvent are warming up to 70~80 DEG C, and 10~15min of heat preservation obtains component A to being completely dissolved after homogeneous；By whitening agent, profit
Skin agent, colorant, film forming agent, emulsifier sequentially add in emulsification pot, are heated to 70~80 DEG C and obtain B component；Then by the component A
It is added into the B component, stirs simultaneously low speed 5~10min of homogeneous, be cooled to 40~50 DEG C；
3) the step 1) antifouling composition is added in the foundation emulsion obtained by step 2), stirs evenly, is cooled to 35
~40 DEG C discharge up to the antipollution skin-protection product.
In the present invention, it is preferable that the speed stirred in the step 2) is 25~30 turns/min, and the homogeneous speed is
2300~2600 revs/min.
In the present invention, it is preferable that B component is added to the component A and is added using vacuum suck or supercharging in the step 2)
Enter.
Wing seed moringa seeds (Moringa Pterygosperma) extract：Moringa is herbaceos perennial, originates in print
Northwestward Asia Himalayas is spent, is the tropical plants that there is unique economic to be worth, western scientist's praise is mystery
Tree.Moringa complete stool is precious, and leaf of Moringa, seed nutritional are extremely abundant, the cationic protein (6000- rich in vitamin, low molecular weight
13000 dalton) and the minerals such as calcium, iron, potassium, meanwhile, the active constituent of fabulous flocculating properties is contained in Moringa seed, kind
Sub- water extract can be substantially reduced bacterial content in the turbidity, hardness and mixed water of mixed water.It has lotus-effect, reduces pollutant
Adhere to skin surface；Cell, the murder by poisoning to preventing from heavy metal is protected to play a protective role skin.It is added in inventive formulation
Wing seed Moringa seed extract, for from commercial channel purchase obtain, be from BASF if not specified in specific embodiment
Company obtains, and name of product isPOE LS 9726。
Trehalose has excellent holding cell viability and the active characteristic of large biological molecule, its energy in the case of severe
Enough to form one layer of special protective film in cell surface, the mucus being precipitated from film not only moistens Skin Cell, and also having will
The function that external heat is radiate, to protect skin that will not be damaged.It is naturally occurring carbohydrate, energy in various plants
It is maintained under worst weather using life.It protects skin fibroblasts anti-by replacing the moisture in tissue
Anti-avulsion water, it injures caused by capable of reducing dehydration, cold and hot variation, to keep the natural structure of skin and hair, can protect
The injury that cell can suffer from by climate change.The trehalose added in inventive formulation, to be bought from commercial channel
It obtains, is to be obtained from Japanese Lin Yuan companies if not specified in specific embodiment, name of product TREHALOSE
100。
Tremella polysaccharides：It is a kind of acidity to obtain tremella polysaccharides (Tremellam) from white fungus (being commonly called as tremella) fructification
Heteroglycan, backbone structure are by the mannosan of α-(1 → 3) glucosides key connection, and branch is made of glucuronic acid and xylose.
A kind of revolutionary plant-derived efficient moisture-retention agent, there is the moistening effect for surmounting hyaluronic acid, it collect moisture retention, anti-aging,
Increase skin sense three zones, main active is different glycan protein nucleic acid compound.Added in inventive formulation
The tremella polysaccharides added obtain for the purchase from commercial channel, are from Shanghai brightness text biology if not specified in specific embodiment
Technology Co., Ltd. obtains, name of product WSK.
Beneficial effects of the present invention：
Compared with prior art, antipollution skin-protection product of the invention has advantageous effect：
The be added to wing seed Moringa seed extract of antipollution skin-protection product of the present invention, trehalose, tremella polysaccharides etc.
A variety of natural plant compositions, play a protective role to skin, repel positively charged atmospheric dust and the harmful heavy metal of complexing,
Mitigate skin to injure caused by due to atmosphere pollution, and cell can be protected, dehydration, cold and hot variation wound caused by skin can be reduced
Evil.
Description of the drawings
Fig. 1 is design sketch after road assists the hand skin of diligent personnel to amplify 10 times.Left hand view skin is only coated with the present invention
The foundation emulsion of embodiment 6, right part of flg dermal application have the antipollution skin-protection product of the embodiment of the present invention 6.
Fig. 2A is 20 minutes purifying water effect figures of standing of antipollution skin-protection product of the present invention, and left figure is ink,
Right figure is the mixture added with ink Yu the antipollution skin-protection product of embodiment 6.
Fig. 2 B are 40 minutes purifying water effect figures of standing of antipollution skin-protection product of the present invention, and left figure is ink,
Right figure is the mixture added with ink Yu the antipollution skin-protection product of embodiment 6.
Fig. 2 C are 120 minutes purifying water effect figures of standing of antipollution skin-protection product of the present invention, and left figure is ink,
Right figure is the mixture added with ink Yu the antipollution skin-protection product of embodiment 6.
Fig. 3 is the cell viability test chart of the present invention.
Specific implementation mode
In order to make the object, technical solutions and advantages of the present invention definitely, below to the preferred embodiment of the present invention into
The detailed description of row.
Embodiment 1-6
The preparation method of antifouling composition and antipollution skin-protection product is introduced below.
1, prepared by antifouling composition
The preparation method of antifouling composition described in embodiment 1-3 is as follows：By wing seed Moringa seed extract, trehalose, white fungus
Polysaccharide is added sequentially in the ratio of table 1 in emulsification pot, is then stirred, until mixing is complete, it is then spare.
2. the preparation of antipollution skin-protection product
Embodiment 3~6 weighs each component substance according to the formula of table 2, prepares the preparation side of the antipollution skin-protection product
Method, its step are as follows：
1) aluminum magnesium silicate, xanthans are soaked with butanediol, are then added in water phase pot, stirring is opened, sequentially adds it
Its remaining component A is warming up to 80 DEG C, 10 minutes is kept the temperature, until being completely dissolved.
2), the raw material of B component is sequentially added in emulsification pot, 80 DEG C is heated to, component A is then passed through into vacuum suck institute
It states in emulsification pot, opens stirring, with 2500 revs/min of speed homogeneous 10 minutes, and be cooled to 45 DEG C up to foundation emulsions；
3), component C is added in emulsification pot, is stirred evenly, antipollution composition is selected from embodiment 1 at this time；
4) it discharges when, stirring is down to 38 DEG C.
5) it is qualified, to examine, and discharging is filling.
1 antipollution composition each component raw material proportioning of table (the sum of each raw material weight percentage composition meter is 100%)
| Raw material | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Wing seed Moringa seed extract | 83.00 | 50.00 | 65.00 |
| Trehalose | 15.00 | 49.00 | 30.00 |
| Tremella polysaccharides | 2.00 | 1.00 | 5.0 |
The each component raw material proportioning of 2 antipollution skin-protection product of table (the sum of each raw material weight percentage composition meter is 100%)
Effect example
One, Pollution protection object attachment test
Test method：
1, antipollution composition (embodiment 1).
2, foundation emulsion (embodiment 6).
3, antipollution skin-protection product (embodiment 6)：The antipollution composition of the addition 3% in foundation emulsion (embodiment 6) is (real
Apply example 1), it stirs evenly.
4,5 diligent personnel of road association are selected, both hands are cleaned up with hand cleanser, are dried with paper handkerchief.
5, in the place of left hand the back of the hand, 0.3 gram of foundation emulsion (embodiment 6) is coated on about 2 square centimeters of area；
In the place of its right hand the back of the hand, 0.3 gram of the powder containing 3% antipollution composition is coated on about 2 square centimeters of area
Bottom liquid (embodiment 6).
6, their 2 hours on duty on road side are allowed, then observation is coated with foundation emulsion (in fact in the case where amplifying 10 times
Apply example 6) position contaminated situation.
7, according to the amount of pollutants for the attachment for being coated with product position and degree come judge its Pollution protection object with effect
Fruit.
Experiment conclusion：
1) right hand the back of the hand of the foundation emulsion (embodiment 6), containing antipollution composition and the powder without antipollution composition
Left hand the back of the hand of bottom liquid (embodiment 6) is compared, and adheres to the degree of dirt and quantity is considerably less than left hand the back of the hand.
2), 5 volunteers show consistent experiment effect：Right hand the back of the hand of foundation emulsion containing antipollution composition
On pollutant be considerably less than left hand, effect is as shown in Figure 1.
Foundation emulsion containing antipollution composition it can be seen from experimental result since wherein Moringa albumen is positively charged,
It can repel dust positively charged in air and the harmful heavy metal of complexing, can prevent dust attachment on the skin, tool
There is the effect for resisting air pollution.
Two, absorption pollutant experiment (water purification experiment)：
Test method：
1, antipollution composition (embodiment 1).
2,99.5 grams of pure water is added in the PET bottle of 2 150ML.
3 and then 0.5 gram of black ink (heroic board) is added, stirs evenly.
4,3 grams of prepared antipollution compositions are added in that bottle on the right, stir evenly.
5, it stands, the variation for observation ink color of taking pictures when 20 minutes, 40 minutes, 120 minutes.
As seen in figs. 2a-2c, it can be seen that experimental result：
1) sample, containing antipollution composition can obviously adsorb the pigment in water, so that pigementation is got off, the color of water
It shoals.
2), over time, the adsorption effect of antipollution composition can obviously increase, and purifying water effect is clearly.
By being tested above it is found that antipollution composition energy adsorpting pigment, has effects that purifying contaminated object, played to skin
Automatic cleaning function.
Three, cell viability is tested
Test method：
1, contain 3% antipollution composition culture medium：3 grams of antipollution composition (embodiment 1) is added to 97 grams of culture
(culture medium in base：The lactoalbumin hydrolysate of 99.5% pure water+0.5%.), it stirs evenly；Containing 3% malt sugar culture-medium：3 grams
Maltose be added in 97 grams of culture medium, stir evenly.
2, human fibroblast is placed in the culture medium containing pure water and is cultivated 12 hours.
3, human fibroblast is placed in the culture medium containing 3% maltose and is cultivated 12 hours.
4, human fibroblast is placed in the culture medium containing 3% antipollution composition and is cultivated 12 hours.
5, culture medium is removed, cell is preserved at room temperature 3 hours.
6, at 1 hour, 2 hours and 3 hours, the cell viability of difference test sample, the results are shown in Figure 3.
By experimental result it can be seen that：
1), over time, the survival ability of cell is continuing to decline.
2), in different culture mediums, the survival ability of cell can have larger difference.
3) it is compared with pure water culture medium, malt sugar culture-medium, the holding cell life containing antipollution composition culture medium
It is most strong to deposit ability.
By being tested above it is found that antipollution composition can play a protective role to cells survival, can be used in skin care item having
Help the injury for protecting cell to can suffer from by reasons such as climate changes, such as dehydration, cold and hot variation.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.Here all embodiments can not be exhaustive.It is every to belong to this hair
Row of the obvious changes or variations that bright technical solution is extended out still in protection scope of the present invention.
Claims (8)
1. a kind of antipollution skin-protection product, which is characterized in that containing antifouling composition, the antifouling composition is in the antipollution
Weight percentage in skin-protection product is 1~5%；The antifouling composition includes following according to weight
Component raw material：
Wing seed Moringa seed extract 50~83%；
Trehalose 15~49%；
Tremella polysaccharides 1~5%；The antipollution skin-protection product further includes foundation emulsion, the foundation cream
Liquid includes following component raw material according to weight：
2. antipollution skin-protection product according to claim 1, which is characterized in that the antifouling composition is according to weight percent
Content meter includes following component raw material：
Wing seed Moringa seed extract 65~83%；
Trehalose 30~49%；
Tremella polysaccharides 2~5%.
3. antipollution skin-protection product according to claim 1 or 2, which is characterized in that the antifouling composition is described anti-
It is 1.5~3% to pollute the weight percentage in skin-protection product.
4. antipollution skin-protection product according to claim 1, which is characterized in that the suspending agent is selected from aluminium-magnesium silicate, Huang
The substance of one or more of virgin rubber, carragheen, carbomer；The preservative is selected from ethohexadiol and/or Phenoxyethanol；
The moisturizer is selected from the substance of one or more of butanediol, 1,3-PD, sorbierite, glycine betaine.
5. antipollution skin-protection product according to claim 1, which is characterized in that the whitening agent is selected from silicon and handles titanium dioxide
Titanium and/or alpha-arbutin；The emollient is selected from isononyl isononanoate, cyclopentasiloxane, lanolin, C12-15 alcohol benzoic ethers
One or more of substance；The colorant is selected from silicon processing iron oxide yellow, silicon processing iron oxide red, silicon processing oxidation
The composition of one or more of iron oxide black；The film forming agent is selected from trimethyl silicane alkoxy esters of silicon acis, polyethylene, fiber
One or more kinds of substance in element；The emulsifier is selected from sorbitan sesquioleate, cetearyl glucoside, spermaceti
One or more kinds of substance in oleth -10；The solvent is one or more kinds of in water, ethyl alcohol, PEG-8
Substance.
6. antipollution skin-protection product according to claim 5, which is characterized in that the silicon processing is in object to be treated
Wrap up last layer ring five dimethyl silicone polymer in matter surface.
7. a kind of preparation method preparing the antipollution skin-protection product as described in any one of claim 1-6, which is characterized in that
Include the following steps：
1) preparation of antifouling compositions：Wing seed Moringa seed extract, trehalose and tremella polysaccharides are proportionally added into emulsification pot
In, it stirs evenly, it is spare to obtain component C；
2) preparation of foundation emulsions：It is added in water phase pot after suspending agent is soaked with moisturizer, opens stirring, sequentially add anti-corrosion
Agent and solvent are warming up to 70~80 DEG C, and 10~15min of heat preservation obtains component A to being completely dissolved after homogeneous；By whitening agent, moisturizing
Agent, colorant, film forming agent, emulsifier sequentially add in emulsification pot, are heated to 70~80 DEG C and obtain B component；Then the component A is added
Enter into the B component, stirs simultaneously low speed 5~10min of homogeneous, be cooled to 40~50 DEG C；
3) antifouling composition described in step 1) is added in the foundation emulsion obtained by step 2), stirs evenly, it is cooled to 35~
40 DEG C discharge up to the antipollution skin-protection product.
8. preparation method according to claim 7, which is characterized in that the speed stirred in the step 2) is 25~30 turns/
Min, the homogeneous speed are 2300~2600 revs/min, and component A is added to the B component and is inhaled using vacuum in the step 2)
Enter or be pressurized addition.
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| CN105434289B (en) * | 2016-01-12 | 2018-08-17 | 广州智媛生物科技有限公司 | A kind of sun-proof foundation emulsion |
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| CN106420500B (en) * | 2016-11-30 | 2019-07-12 | 广东芭薇生物科技股份有限公司 | A kind of composition of the extract containing Inonotus obliquus and its application |
| CN106727231A (en) * | 2016-12-22 | 2017-05-31 | 广州睿森生物科技有限公司 | A kind of antipollution composition and cosmetics |
| CN106983684B (en) * | 2017-04-05 | 2020-01-24 | 安徽大学 | Anti-pollution cream and preparation method thereof |
| CN107080725A (en) * | 2017-04-19 | 2017-08-22 | 云南宁泽生物科技有限公司 | Moringa Chinese medicine epithelium maintenance liquid and its processing method |
| CN106963689A (en) * | 2017-04-28 | 2017-07-21 | 广州市雅蝶化妆品制造有限公司 | A kind of effective antipollution material combination |
| CN107095842A (en) * | 2017-05-04 | 2017-08-29 | 广州诺胜化妆品有限公司 | A kind of moringa seeds elite antipollution facial mask and preparation technology |
| CN107412062B (en) * | 2017-08-09 | 2019-09-13 | 广东丸美生物技术股份有限公司 | For the composition of antipollution cosmetics, liposome, cream type cosmetics, emulsion-type cosmetics and its preparation method and application |
| CN107929113B (en) * | 2017-12-27 | 2020-09-22 | 广州智媛生物科技有限公司 | Anti-pollution skin care composition and cosmetic |
| CN108785201B (en) * | 2018-07-10 | 2021-04-06 | 广东芭薇生物科技股份有限公司 | Anti-pollution cosmetic composition and cosmetic using same |
| CN108904436B (en) * | 2018-09-16 | 2021-09-24 | 韩后化妆品股份有限公司 | Anti-pollution skin care composition with anti-inflammatory and anti-aging effects |
| CN109464339B (en) * | 2018-12-26 | 2021-05-14 | 广州蜜妆生物科技有限公司 | Anti-pollution composition and application thereof |
| CN112076100A (en) * | 2019-06-12 | 2020-12-15 | 西安博鸿生物技术有限公司 | Anti-pollution skin care composition and preparation method thereof |
| CN113925817B (en) * | 2021-11-26 | 2023-12-05 | 苍南老中医化妆品有限公司 | Skin care essence with anti-pollution effect and preparation method thereof |
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Effective date of registration: 20191226 Address after: 510920 213 Lidu Road, Chengjiao street, Conghua District, Guangzhou, Guangdong Province Patentee after: Guangzhou bolichen cosmetics technology Co.,Ltd. Address before: 510000 Tianhe District, Guangdong Tianhe East Road, No. 240, No. Patentee before: GUANGZHOU ZHIYUAN BIOTECHNOLOGY CO.,LTD. |
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