CN105055261A - Anti-pollution skincare product and preparation method thereof - Google Patents
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Abstract
The invention relates to an anti-pollution skincare product and a preparation method thereof, in particular to an anti-pollution composition, the anti-pollution composition-containing anti-pollution skincare product, and the preparation method of the anti-pollution skincare product. The anti-pollution skincare product provided by the invention is added with a plurality of natural plant components, such as moringa pterygosperma seed extract, trehalose, tremella polysaccharide and the like, has a protecting effect on skin, repels atmospheric dust with positive charges, conducts complexing of harmful heavy metals, lightens the damage caused by atmospheric pollution, can protect cells and can reduce the injury to the skin caused by dehydration and heat and cold change.
Description
Technical field
The invention belongs to cosmetic field, relate to a kind of antipollution skin-protection product and preparation method thereof particularly.
Background technology
Along with producing and economic express delivery growth, the continuous deterioration of environment, air pollution constantly increases the weight of, and the polluter of the mankind constantly increases.First what be hurt is the skin of the mankind, accumulate over a long period, corrode the health of skin, accelerate the aging of skin, cause a series of skin problem, the skin care item with anti-pollution can resist the infringement of factor to skin of physics and chemistry, corrosion, strengthen the ability that epidermis resists pollution, improve cell viability and just seem particularly urgent.
Ozone excessive in air reduces the content of vitamin C and vitamin E in skin, and lipid peroxidation is increased; Vehicle exhaust and polycyclic aromatic hydrocarbon, increase oxidative stress and cell injury; Pollutant floating in air, be easy to enter pore, heavy damage cuticular update cycle and speed, cause a series of skin problem, shows as follows: blood capillary severe dilation, there is obvious red blood streak, cutaneous sensibility increases, and is very easy to occur anaphylaxis, and the colour of skin is obscure, spot colors is deepened, and microgroove increases.
At present cosmetics are on the market by film forming component mostly or add ultraviolet attractant, the pollution of air-isolation and resist ultraviolet injury, and effect is more single, and can not resist various polluter all sidedly, resistant to pollution effect is not remarkable.So develop a there is antipollution, the skin care item of Cell protection just become urgent in the extreme.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the invention provides a kind of antifouling composition of encroaching on for atmospheric pollution etc. specially, this antifouling composition can repel the harmful heavy metal of positively charged atmospheric dust and complexation, alleviates the injury that skin causes because of atmospheric pollution.
As follows in order to realize the technical scheme that above-mentioned technical purpose adopts:
A kind of antifouling composition, comprises following component raw material according to weight:
Wing seed moringa seeds extract 50 ~ 83%;
Trehalose 15 ~ 49%;
Tremella polysaccharide 1 ~ 5%.
Preferred as one, comprise following component raw material according to weight:
Wing seed moringa seeds extract 65 ~ 83%;
Trehalose 30 ~ 49%;
Tremella polysaccharide 2 ~ 5%.
Another technical purpose of the present invention is to provide a kind of antipollution skin-protection product, and described antipollution skin-protection product contains above-mentioned antifouling composition, and the weight percentage of described antifouling composition in described antipollution skin-protection product is 1 ~ 5%.
In the present invention more preferably, the weight percentage of described antifouling composition in described antipollution skin-protection product is 1.5 ~ 3%.
Further, described antipollution skin-protection product also comprises foundation emulsion, and described foundation emulsion comprises following component raw material according to weight:
In the present invention, preferably, described suspending agent is selected from one or more the material in aluminium-magnesium silicate, xanthan gum, carrageenan, carbomer; Described antiseptic is selected from one or more the material in ethohexadiol, phenoxyethanol, Methylisothiazolinone; Described wetting agent is selected from one or more the material in butanediol, 1,3-PD, sorbitol, betanin.
In the present invention, preferably, described whitening agent is selected from silicon process titanium dioxide and/or alpha-arbutin; Described emollient is selected from one or more the material in isononyl isononanoate, cyclopentasiloxane, lanoline, C12-15 alcohol benzoate; Described colorant is selected from one or more the compositions in silicon process iron oxide yellow, silicon process iron oxide red, silicon process iron oxide black; Described film former to be selected from trimethyl silicane alcoxyl base esters of silicon acis, polyethylene, cellulose one or more material; Described emulsifying agent to be selected from sorbitan sesquioleate, cetearyl glucoside, spermaceti oleth-10 one or more material; Described solvent to be selected from water, ethanol, PEG-8 one or more material.
Preferably, described silicon is treated to is needing material surface to be processed to superscribe one deck ring five polydimethylsiloxane, the compatibility of titanium dioxide and oils and fats can be increased like this, also can increase the compatibility of iron oxide yellow, iron oxide red, iron oxide black and other materials.
More preferably, the particle diameter of described silicon process titanium dioxide is 20 ~ 40 microns.Particle diameter is too little not easily hides face's flaw, and particle diameter is too large not easily Dermallly affixed again.
Another technical purpose of the present invention is to provide a kind of preparation method of antipollution skin-protection product, comprises the following steps:
The preparation of antifouling composition: wing seed moringa seeds extract, trehalose and tremella polysaccharide are added in emulsifying pot in proportion, stirs, obtain component C for subsequent use;
2). the preparation of foundation emulsion: add in aqueous phase pot by after the moistening of suspending agent wetting agent, open and stir, add antiseptic and solvent successively, be warming up to 70 ~ 80 DEG C, insulation 10 ~ 15min, to dissolving completely, obtains component A after homogenizing; Whitening agent, emollient, colorant, film former, emulsifying agent are added in emulsifying pot successively, is heated to 70 ~ 80 DEG C and obtains B component; Then described component A is added in described B component, stirs and low speed homogenizing 5 ~ 10min, be cooled to 40 ~ 50 DEG C;
3). by step 1) described antifouling composition adds step 2) and obtained by foundation emulsion in, stir, be cooled to 35 ~ 40 DEG C of dischargings and namely obtain described antipollution skin-protection product.
In the present invention, preferably, described step 2) in the speed that stirs be 25 ~ 30 turns/min, described homogenizing speed is 2300 ~ 2600 revs/min.
In the present invention, preferably, described step 2) middle B component is added to described component A employing vacuum suction or supercharging adds.
Wing seed moringa seeds (MoringaPterygosperma) extract: Moringa is herbaceos perennial, originating in sub-Himalayas, the India northwestward, is the tropical plants with unique economic value, the tree that western scientist's praise is mystery.Moringa Herb is precious, leaf of Moringa, seed nutritional are very abundant, be rich in the mineral such as vitamin, low-molecular-weight cationic protein (6000-13000 dalton) and calcium, ferrum, potassium, simultaneously, active component containing fabulous flocculating properties in Moringa seed, its seed water extract obviously can reduce bacterial content in mixed water turbidity, hardness and mixed water.It has lotus-effect, the Dermallly affixed surface of decreasing pollution thing; Cell protection, to the murder by poisoning of preventing from heavy metal, plays a protective role to skin.The wing seed moringa seeds extract added in formula of the present invention, obtain for buying from commercial channel, if not specified in specific embodiment, be and obtain from BASF AG, its name of product is
pOELS9726.
Trehalose has excellent maintenance cell viability and the characteristic of biomacromolecule activity; it can form the special protecting film of one deck at cell surface layer when severe; the mucus separated out from film not only moistens Skin Cell; also there is the function of being gone out by external heat radiation, thus protection skin is unlikely impaired.Be naturally occurring saccharide in various plants, life can be used to be maintained under worst weather.It protects skin flbroblast to prevent dehydration, the injury that it can reduce dehydration, cold and hot change causes by replacing the moisture in tissue, thus maintenance skin and the natural structure of hair, can the Cell protection injury that may be subjected to because of climate change.The trehalose added in formula of the present invention, obtain for buying from commercial channel, if not specified in specific embodiment, be and obtain from Japanese Lin Yuan company, its name of product is TREHALOSE100.
Tremella polysaccharide: obtaining tremella polysaccharide (Tremellam) from Tremella (being commonly called as Tremella) sporophore is a kind of acid heteroglycan, its backbone structure is the mannan connected by α-(1 → 3) glycosidic bond, and side chain is made up of glucuronic acid and xylose.A kind of revolutionary plant-derived efficient moisture-retention agent, it has and surmounts hyaluronic moistening effect, and it integrates moisture retention, defying age, increase skinfeel three zones, and its main active is different polysaccharide protein nucleic acid complex.The tremella polysaccharide added in formula of the present invention, obtain for buying from commercial channel, if not specified in specific embodiment, be and obtain from Shanghai Huiwen Bio-Tech Co., Ltd., its name of product is WSK.
Beneficial effect of the present invention:
Compared with prior art, antipollution skin-protection product of the present invention has beneficial effect:
Antipollution skin-protection product of the present invention with the addition of the multiple natural plant compositions such as wing seed moringa seeds extract, trehalose, tremella polysaccharide; skin is played a protective role; repel the heavy metal that positively charged atmospheric dust and complexation are harmful; alleviate the injury that skin causes because of atmospheric pollution; and can Cell protection, dehydration can be reduced, injury that cold and hot change causes skin.
Accompanying drawing explanation
Fig. 1 is design sketch after road assists the hand skin of diligent personnel to amplify 10 times.Left hand view skin is only coated with the foundation emulsion of the embodiment of the present invention 6, and right part of flg dermal application has the antipollution skin-protection product of the embodiment of the present invention 6.
Fig. 2 A is the purifying water effect figure leaving standstill 20 minutes of antipollution skin-protection product of the present invention, and left figure is ink, and right figure is the mixture of the antipollution skin-protection product being added with ink and embodiment 6.
Fig. 2 B is the purifying water effect figure leaving standstill 40 minutes of antipollution skin-protection product of the present invention, and left figure is ink, and right figure is the mixture of the antipollution skin-protection product being added with ink and embodiment 6.
Fig. 2 C is the purifying water effect figure leaving standstill 120 minutes of antipollution skin-protection product of the present invention, and left figure is ink, and right figure is the mixture of the antipollution skin-protection product being added with ink and embodiment 6.
Fig. 3 is cell viability test pattern of the present invention.
Detailed description of the invention
In order to make the object, technical solutions and advantages of the present invention definitely, below the preferred embodiments of the present invention are described in detail.
Embodiment 1-6
Below the preparation method of antifouling composition and antipollution skin-protection product is introduced.
1, antifouling composition preparation
Described in embodiment 1-3, the preparation method of antifouling composition is as follows: wing seed moringa seeds extract, trehalose, tremella polysaccharide are joined successively in emulsifying pot in the ratio of table 1, then stir, until mixing completely, then for subsequent use.
2. the preparation of antipollution skin-protection product
Embodiment 3 ~ 6 weighs each component materials according to the formula of table 2, and prepare the preparation method of described antipollution skin-protection product, its step is as follows:
1), by Magnesiumaluminumsilicate, xanthan gum butanediol moistening, then add in aqueous phase pot, open and stir, add the component A of other remainder successively, be warming up to 80 DEG C, be incubated 10 minutes, until dissolve completely.
2), by the raw material of B component add successively in emulsifying pot, be heated to 80 DEG C, then component A is sucked in described emulsifying pot by vacuum, open and stir, with 2500 revs/min of speed homogenizing 10 minutes, and be cooled to 45 DEG C and namely obtain foundation emulsion;
3), by component C add in emulsifying pot, stir, now antipollution compositions is selected from embodiment 1;
4), discharging when being down to 38 DEG C is stirred.
5), be up to the standards, discharging fill.
Table 1 antipollution compositions each component raw material proportioning (each raw material weight percentage composition meter sum is 100%)
| Raw material | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Wing seed moringa seeds extract | 83.00 | 50.00 | 65.00 |
| Trehalose | 15.00 | 49.00 | 30.00 |
| Tremella polysaccharide | 2.00 | 1.00 | 5.0 |
Each component raw material proportioning (each raw material weight percentage composition meter sum is 100%) of table 2 antipollution skin-protection product
Effect example
One, Pollution protection thing attachment test
Method of testing:
1, antipollution compositions (embodiment 1).
2, foundation emulsion (embodiment 6).
3, antipollution skin-protection product (embodiment 6): add the antipollution compositions (embodiment 1) of 3% in foundation emulsion (embodiment 6), stir.
4, select 5 roads to assist diligent personnel, with handwashing liquid, both hands are cleaned up, dry with napkin.
5, the place of the back of the hand leftward, the area of about 2 square centimeters is coated the foundation emulsion (embodiment 6) of 0.3 gram; In the place of its right hand the back of the hand, the area of about 2 square centimeters is coated the foundation emulsion (embodiment 6) containing 3% antipollution compositions of 0.3 gram.
6, allow them on road limit 2 hours on duty, then observe the contaminated situation scribbling the position of foundation emulsion (embodiment 6) when amplification 10 times.
7, according to the amount of pollutants of attachment and degree that scribble product position judge its Pollution protection thing along with effect.
Experiment conclusion:
1) right hand the back of the hand of the foundation emulsion (embodiment 6), containing antipollution compositions is compared with the left hand the back of the hand of the foundation emulsion (embodiment 6) not containing antipollution compositions, and degree and the quantity of attachment dirt are obviously less than left hand the back of the hand.
2), 5 volunteers present consistent experiment effect: the pollutant on right hand the back of the hand of the foundation emulsion containing antipollution compositions are obviously less than left hand, and its effect as shown in Figure 1.
As can be seen from experimental result, foundation emulsion containing antipollution compositions is due to wherein Moringa protein band positive charge, it can repel the harmful heavy metal of dust positively charged in air and complexation, and dust can be prevented to be attached on skin, has opposing air-polluting effect.
Two, adsorption fouling thing experiment (water purification experiment):
Method of testing:
1, antipollution compositions (embodiment 1).
2, in the PET bottle of 2 150ML, add the pure water of 99.5 grams.
3, then add the black ink (heroic board) of 0.5 gram, stir.
4, add 3 grams of antipollution compositionss prepared in that bottle on the right, stir.
5, leave standstill, respectively at 20 minutes, 40 minutes, take pictures when 120 minutes and observe the change of ink color.
As seen in figs. 2a-2c, experimental result can be found out:
1) sample, containing antipollution compositions can pigment obviously in adsorbed water, pigementation is got off, the lighter of water.
2), As time goes on, the adsorption effect of antipollution compositions can obviously increase, and purifying water effect clearly.
From testing above, antipollution compositions energy adsorpting pigment, has effect of purifying contaminated thing, plays automatic cleaning function to skin.
Three, cell viability test
Method of testing:
1, containing 3% antipollution compositions culture medium: (culture medium: the lactoalbumin hydrolysate of the pure water+0.5% of 99.5% that the antipollution compositions (embodiment 1) of 3 grams joins in the culture medium of 97 grams.), stir; Containing 3% maltose culture medium: the maltose of 3 grams joins in the culture medium of 97 grams, stirs.
2, culture medium human fibroblast be placed in containing pure water is cultivated 12 hours.
3, culture medium human fibroblast be placed in containing the maltose of 3% is cultivated 12 hours.
4, culture medium human fibroblast be placed in containing 3% antipollution compositions is cultivated 12 hours.
5, remove culture medium, cell is at room temperature preserved 3 hours.
6, at 1 hour, 2 hours and 3 hours, test the cell viability of sample respectively, its result as shown in Figure 3.
As can be seen from experimental result:
1), As time goes on, the survival ability of cell is at continuous decrease.
2), in different culture medium, can there is larger difference in the survival ability of cell.
3) compare with pure water culture medium, maltose culture medium, the maintenance cell viability containing antipollution compositions culture medium is the strongest.
From testing above, antipollution compositions can play a protective role to cells survival, can be used for contributing in skin care item the injury that Cell protection may suffer because of reasons such as climate changes, such as, dewater, cold and hot change.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here cannot give exhaustive to all embodiments.Every belong to technical scheme of the present invention the apparent change of extending out or variation be still in the row of protection scope of the present invention.
Claims (10)
1. an antifouling composition, is characterized in that, comprises following component raw material according to weight:
Wing seed moringa seeds extract 50 ~ 83%;
Trehalose 15 ~ 49%;
Tremella polysaccharide 1 ~ 5%.
2. antifouling composition according to claim 1, is characterized in that, comprises following component raw material according to weight:
Wing seed moringa seeds extract 65 ~ 83%;
Trehalose 30 ~ 49%;
Tremella polysaccharide 2 ~ 5%.
3. an antipollution skin-protection product, is characterized in that, described antipollution skin-protection product contains antifouling composition described in claim 1 or 2, and the weight percentage of described antifouling composition in described antipollution skin-protection product is 1 ~ 5%.
4. antipollution skin-protection product according to claim 3, is characterized in that, the weight percentage of described antifouling composition in described antipollution skin-protection product is 1.5 ~ 3%.
5. antipollution skin-protection product according to claim 3, is characterized in that, described antipollution skin-protection product also comprises foundation emulsion, and described foundation emulsion comprises following component raw material according to weight:
6. antipollution skin-protection product according to claim 5, is characterized in that, described suspending agent is selected from one or more the material in aluminium-magnesium silicate, xanthan gum, carrageenan, carbomer; Described antiseptic is selected from one or more the material in ethohexadiol, phenoxyethanol, Methylisothiazolinone; Described wetting agent is selected from one or more the material in butanediol, 1,3-PD, sorbitol, betanin.
7. antipollution skin-protection product according to claim 5, is characterized in that, described whitening agent is selected from silicon process titanium dioxide and/or α place arbutin; Described emollient is selected from one or more the material in isononyl isononanoate, cyclopentasiloxane, lanoline, C12-15 alcohol benzoate; Described colorant is selected from one or more the compositions in silicon process iron oxide yellow, silicon process iron oxide red, silicon process iron oxide black; Described film former to be selected from trimethyl silicane alcoxyl base esters of silicon acis, polyethylene, cellulose one or more material; Described emulsifying agent to be selected from sorbitan sesquioleate, cetearyl glucoside, spermaceti oleth-10 one or more material; Described solvent to be selected from water, ethanol, PEG-8 one or more material.
8. antipollution skin-protection product according to claim 5, is characterized in that, described silicon is treated to is needing material surface to be processed to superscribe one deck ring five polydimethylsiloxane.
9. prepare the preparation method as antipollution skin-protection product as described in any one in claim 3-8, it is characterized in that, comprise the following steps:
1). the preparation of antifouling composition: wing seed moringa seeds extract, trehalose and tremella polysaccharide are added in emulsifying pot in proportion, stirs, obtain component C for subsequent use;
2). the preparation of foundation emulsion: add in aqueous phase pot by after the moistening of suspending agent wetting agent, open and stir, add antiseptic and solvent successively, be warming up to 70 ~ 80 DEG C, insulation 10 ~ 15min, to dissolving completely, obtains component A after homogenizing; Whitening agent, emollient, colorant, film former, emulsifying agent are added in emulsifying pot successively, is heated to 70 ~ 80 DEG C and obtains B component; Then described component A is added in described B component, stirs and low speed homogenizing 5 ~ 10min, be cooled to 40 ~ 50 DEG C;
3). by step 1) described in antifouling composition add step 2) obtained by foundation emulsion in, stir, be cooled to 35 ~ 40 DEG C of dischargings and namely obtain described antipollution skin-protection product.
10. preparation method according to claim 9, it is characterized in that, described step 2) in stir speed be 25 ~ 30 turns/min, described homogenizing speed is 2300 ~ 2600 revs/min, described step 2) in component A be added to described B component adopt vacuum suck or supercharging add.
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| CN107412062B (en) * | 2017-08-09 | 2019-09-13 | 广东丸美生物技术股份有限公司 | For the composition of antipollution cosmetics, liposome, cream type cosmetics, emulsion-type cosmetics and its preparation method and application |
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| CN108785201A (en) * | 2018-07-10 | 2018-11-13 | 广东芭薇生物科技股份有限公司 | A kind of antipollution cosmetic composition and its cosmetics of application |
| CN108785201B (en) * | 2018-07-10 | 2021-04-06 | 广东芭薇生物科技股份有限公司 | Anti-pollution cosmetic composition and cosmetic using same |
| CN108904436A (en) * | 2018-09-16 | 2018-11-30 | 韩后化妆品股份有限公司 | It is a kind of to have both anti-inflammatory, anti-aging effect antipollution skin care compositions |
| CN108904436B (en) * | 2018-09-16 | 2021-09-24 | 韩后化妆品股份有限公司 | Anti-pollution skin care composition with anti-inflammatory and anti-aging effects |
| CN109464339A (en) * | 2018-12-26 | 2019-03-15 | 广州蜜妆生物科技有限公司 | A kind of antipollution composition and its application |
| CN109464339B (en) * | 2018-12-26 | 2021-05-14 | 广州蜜妆生物科技有限公司 | Anti-pollution composition and application thereof |
| CN112076100A (en) * | 2019-06-12 | 2020-12-15 | 西安博鸿生物技术有限公司 | Anti-pollution skin care composition and preparation method thereof |
| CN113925817A (en) * | 2021-11-26 | 2022-01-14 | 刘均亮 | Skin care essence with anti-pollution effect and preparation method thereof |
| CN113925817B (en) * | 2021-11-26 | 2023-12-05 | 苍南老中医化妆品有限公司 | Skin care essence with anti-pollution effect and preparation method thereof |
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