CN105054284A - Fresh and elegant fragrance type electronic cigarette atomization liquid and preparation method thereof - Google Patents
Fresh and elegant fragrance type electronic cigarette atomization liquid and preparation method thereof Download PDFInfo
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- CN105054284A CN105054284A CN201510495503.5A CN201510495503A CN105054284A CN 105054284 A CN105054284 A CN 105054284A CN 201510495503 A CN201510495503 A CN 201510495503A CN 105054284 A CN105054284 A CN 105054284A
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Abstract
The invention provides fresh and elegant fragrance type electronic cigarette atomization liquid and a preparation method thereof. The electronic cigarette atomization liquid is mainly prepared from, by weight, natural nicotine 0.05-2.6, tobacco extract 4-10, menthol 0.05-2, raspberry ketone 0.1-0.5, ethyl acetate 0.1-0.4, beta-ionone 0.02-0.1, USP grade glycerol 26-40 and the balance food grade propylene glycol. According to the fresh and elegant fragrance type electronic cigarette atomization liquid and the preparation method thereof, the substance components such as the menthol, the beta-ionone and the raspberry ketone are adopted, and therefore the nicotine content in the electronic atomization liquid is decreased; meanwhile, the physical health is facilitated, the fresh and elegant fragrance is achieved, and the cigarette liquid quality of electronic cigarettes is improved.
Description
Technical field
The present invention relates to the technical field of electronic cigarette, particularly a kind of electronic cigarette atomizing liquid and preparation method thereof of salubrious elegant odor type.
Background technology
Cigarette is as a kind of preference, be subject to liking of many people, but the tar in cigarette, carbon monoxide (CO) health to human body is harmful, especially containing several 10 kinds of compositions in tar is carcinogens, at present progressively forbid smoking cigarettes (cigarette) being defined in public place with home government abroad, but for a smoker having smoking history, requirement is accomplished no longer to have cigarette smoking, it is a very difficult thing, so commercially there is the substitute of much cigarette, as: lozenge for stopping smoking, electronic cigarette, found that electronic cigarette was the most common in recent years, this electronic cigarette is atomized by cigarette bullet, and then generation smog, but the function singleness of existing tobacco juice for electronic smoke, just as simple substitute of tobacco, the effect of taking good care of that keeps healthy further cannot be played to human body.
Summary of the invention
The object of the invention is electronic cigarette atomizing liquid proposing a kind of salubrious elegant odor type and preparation method thereof, craving for tobacco can be met and be conducive to again healthy, there is salubrious elegant fragrance, promote the tobacco juice quality of electronic cigarette.
For achieving the above object, the present invention proposes a kind of electronic cigarette atomizing liquid of salubrious elegant odor type, it is formulated by weight primarily of following composition:
Natural nicotine 0.05 ~ 2.6, tobacco extract 4 ~ 10, menthol 0.05 ~ 2, raspberry ketone 0.1 ~ 0.5, ethyl acetate 0.1 ~ 0.4, alpha, beta-lonone 0.02 ~ 0.1, USP level (USP standard) glycerine 26 ~ 40, surplus are food grade propylene glycol.
Further, in the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, purity >=99% of natural nicotine.
Further, in the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, the weight ratio of each composition of electronic cigarette atomizing liquid of described salubrious elegant odor type is preferably:
Natural nicotine 2.6, tobacco extract 10, menthol 2, raspberry ketone 0.5, ethyl acetate 0.4, alpha, beta-lonone 0.1, USP level glycerine 40, surplus are food grade propylene glycol.
Further, in the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, the weight ratio of each composition of electronic cigarette atomizing liquid of described salubrious elegant odor type is preferably:
Natural nicotine 2, tobacco extract 6, menthol 1, raspberry ketone 0.3, ethyl acetate 0.3, alpha, beta-lonone 0.05, USP level glycerine 30, surplus are food grade propylene glycol.
Separately, the present invention also provides the preparation method of the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, comprises the following steps:
A () will weigh tobacco extract by formula rate, menthol, 4-(4-hydroxyphenyl)-2-butanone add in deionized water, be heated to 50 DEG C ~ 65 DEG C and fully stirring is dissolved completely;
B () adds previously prepared mixed solution by the solution in step (a), described mixed solution is propane diols, ethyl acetate, alpha, beta-lonone weigh by formula rate and make, and fully stirs, then is heated to 45 DEG C ~ 60 DEG C;
C () adds natural nicotine, USP level glycerine after the solution in step (b) is cooled to 15 ~ 30 DEG C, stir;
D () cools after the filled with solution in step (c) at-5 DEG C ~ 0 DEG C temperature, namely obtain the electronic cigarette atomizing liquid of described salubrious elegant odor type.
Further, in the preparation method of the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, described alpha, beta-lonone is made up of following extracting method:
Adopt the fruit of a cubeb litsea tree (mainly originate in various places on the south China the Changjiang river, have wild and cultivated woods, have very high economic worth) to make condensing agent with NaOH, synthesize 1.5 hours, obtain pseudoionone (productive rate reaches 87%);
In cyclization directly with the pseudoionone crude product without vacuum topping for raw material, add benzene and make solvent, react 0.5 hour, obtain α-ionone (productive rate can reach 67%) and alpha, beta-lonone (productive rate reaches 70%).
Further, in the preparation method of the electronic cigarette atomizing liquid of above-mentioned salubrious elegant odor type, described menthol is made up of following extracting method:
By the aerial part (stem of labiate peppermint; Branch; Leaf and inflorescence) obtain raw peppermint oil (oil yield is 0.5-0.6) through steam distillation;
By freezing for above-mentioned raw peppermint oil rear crystallization, the low solvent recrystallization of boiling of centrifugal gained crystallization obtains pure levorotatory menthol;
Except the mother liquor (still containing menthol 40% ~ 50%, also containing relatively large menthones) after decrystallizing changes the mixture of levorotatory menthol and dextrorotation neomenthol into through hydrogenation;
Partly-hydrolysed by above-mentioned ester, through crystallization, distills or point to go other parts in raw peppermint oil after making its borate, obtaining more levorotatory menthol.
What the electronic cigarette atomizing liquid of the salubrious elegant odor type of the present invention adopted is the material compositions such as menthol, alpha, beta-lonone, raspberry ketone, thus reduce the content of nicotine in electronic atomized liquid, be conducive to healthy simultaneously, there is salubrious elegant fragrance, improve the tobacco juice quality of electronic cigarette.
Wherein, irisone mainly contains 3 kinds of isomeric compounds, but first position and second position is more common.First position person: colourless to light yellow liquid.Boiling point 237 DEG C, relative density 0.927-0.933, refractive index 1.497-1.502, flash-point more than 100 DEG C, is dissolved in 3 volume 70% ethanol and oils.Second position person: pale yellow to colourless liquid, boiling point 239 DEG C, relative density 0.941-0.947, refractive index 1.5190-1.5215, flash-point more than 100 DEG C, has the sweet fragrance of a flower to hold concurrently the banksia rose be with the fragrant and fruital of cream.Fragrance is pure and honest and stay length.Second position person's fragrance is sweet not as first position person, but and fruital more fragrant than the many cream of first position person, and effectively.The sweet banksia rose taste band fruital that first and second persons are strong, micro-hardship was the fragrance of flowers and trees fragrance afterwards.
Irisone is used for various odor type, can play modify and close, increase sweet, increase the fragrance of a flower, the effect such as skillful.It is the conventional perfumes of joining the essence such as gillyflower, sweet osmanthus, tree orchid, rose, Acacia, bashfully flower, tuberose, the lily of the valley, cymbidium, chypre, banksia rose type.Also ambergris, the fragrant class essence of cream is applicable to.Also it can be used in herbal, pine perfume or tangerine odor type.Also the fragrant or fruital of the berry such as raspberry, strawberry, cherry, grape, pine apple nanas and the flavoring essence such as nut, the fragrance of a flower is applicable to.
Cover a kind of spices with quiet and tastefully laid out fruital that plate ketone is at present both at home and abroad extensive use, in raspberry fragrance with the fragrant and sweet taste of fruit.Be widely used in edible and daily essence, its main application comprises: fixastive, dressing agent, modulation cosmetics, fat-reducing and pharmacological action.
The organic compound of menthol is colorless needle crystals or granular, is the main component in peppermint and lavender essential oil, exists with the state of ester with free.Menthol has 8 kinds of isomers, they in fragrance matter different, levorotatory menthol has peppermint fragrance and has refrigerant effect, and racemization menthol also has refrigerant effect, and other isomers is without refrigerant effect.Can be used as the odorant of toothpaste, perfume, beverage and candy etc.Being pharmaceutically used as excitants, acting on skin or mucous membrane, having refrigerant itching-relieving action; For oral administration can be used for, has a headache and nose, pharynx, laryngitis etc.
To sum up, electronic cigarette atomizing liquid of the salubrious elegant odor type of the present invention and preparation method thereof is by adopting the material compositions such as tobacco extract, ginseng extract, green-tea extract, decrease nicotine to harm, be conducive to healthy simultaneously, there is salubrious elegant fragrance, improve the tobacco juice quality of electronic cigarette.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described:
Embodiment 1
Take each component materials of the electronic cigarette atomizing liquid of the salubrious elegant odor type of preparation the present invention by weight, described each composition raw material is by weight: natural nicotine (purity >=99%) 2.6, tobacco extract 10, menthol 2, raspberry ketone 0.5, ethyl acetate 0.4, alpha, beta-lonone 0.1, USP level glycerine 40, surplus are food grade propylene glycol; During preparation,
A () will weigh tobacco extract by formula rate, menthol, 4-(4-hydroxyphenyl)-2-butanone add in deionized water, be heated to 65 DEG C and fully stirring is dissolved completely;
B () adds previously prepared mixed solution by the solution in step (a), described mixed solution is propane diols, ethyl acetate, alpha, beta-lonone weigh by formula rate and make, and fully stirs, then is heated to 60 DEG C;
C () adds natural nicotine, USP level glycerine after the solution in step (b) is cooled to 30 DEG C, stir;
D () cools after the filled with solution in step (c) at 0 DEG C of temperature, namely obtain the electronic cigarette atomizing liquid of described salubrious elegant odor type.
Embodiment 2
Take each component materials of the electronic cigarette atomizing liquid of the salubrious elegant odor type of preparation the present invention by weight, described each composition raw material is by weight: natural nicotine (purity >=99%) 2, tobacco extract 6, menthol 1, raspberry ketone 0.3, ethyl acetate 0.3, alpha, beta-lonone 0.05, USP level glycerine 30, surplus are food grade propylene glycol; During preparation,
A () will weigh tobacco extract by formula rate, menthol, 4-(4-hydroxyphenyl)-2-butanone add in deionized water, be heated to 60 DEG C and fully stirring is dissolved completely;
B () adds previously prepared mixed solution by the solution in step (a), described mixed solution is propane diols, ethyl acetate, alpha, beta-lonone weigh by formula rate and make, and fully stirs, then is heated to 50 DEG C;
C () adds natural nicotine, USP level glycerine after the solution in step (b) is cooled to 20 DEG C, stir;
D () cools after the filled with solution in step (c) at-4 DEG C of temperature, namely obtain the electronic cigarette atomizing liquid of described salubrious elegant odor type.
Embodiment 3
Take each component materials of the electronic cigarette atomizing liquid of the salubrious elegant odor type of preparation the present invention by weight, described each composition raw material is by weight:
Natural nicotine (purity >=99%) 0.05, tobacco extract 4, menthol 0.05, raspberry ketone 0.1, ethyl acetate 0.1, alpha, beta-lonone 0.02, USP level glycerine 26, surplus are food grade propylene glycol; During preparation,
A () will weigh tobacco extract by formula rate, menthol, 4-(4-hydroxyphenyl)-2-butanone add in deionized water, be heated to 50 DEG C and fully stirring is dissolved completely;
B () adds previously prepared mixed solution by the solution in step (a), described mixed solution is propane diols, ethyl acetate, alpha, beta-lonone weigh by formula rate and make, and fully stirs, then is heated to 45 DEG C;
C () adds natural nicotine, USP level glycerine after the solution in step (b) is cooled to 15, stir;
D () cools after the filled with solution in step (c) at-5 DEG C of temperature, namely obtain the electronic cigarette atomizing liquid of described salubrious elegant odor type.
Here description of the invention and application is illustrative, not wants by scope restriction of the present invention in the above-described embodiments.Distortion and the change of embodiment disclosed are here possible, are known for the replacement of embodiment those those of ordinary skill in the art and the various parts of equivalence.Those skilled in the art are noted that when not departing from spirit of the present invention or substantive characteristics, the present invention can in other forms, structure, layout, ratio, and to realize with other assembly, material and parts.When not departing from the scope of the invention and spirit, can other distortion be carried out here to disclosed embodiment and change.
Claims (7)
1. an electronic cigarette atomizing liquid for salubrious elegant odor type, is characterized in that, it is formulated by weight primarily of following composition:
Natural nicotine 0.05 ~ 2.6, tobacco extract 4 ~ 10, menthol 0.05 ~ 2, raspberry ketone 0.1 ~ 0.5, ethyl acetate 0.1 ~ 0.4, alpha, beta-lonone 0.02 ~ 0.1, USP level glycerine 26 ~ 40, surplus are food grade propylene glycol.
2. the electronic cigarette atomizing liquid of salubrious elegant odor type according to claim 1, is characterized in that, purity >=99% of described natural nicotine.
3. the electronic cigarette atomizing liquid of salubrious elegant odor type according to claim 1, is characterized in that, the weight ratio of each composition of electronic cigarette atomizing liquid of described salubrious elegant odor type is preferably:
Natural nicotine 2.6, tobacco extract 10, menthol 2, raspberry ketone 0.5, ethyl acetate 0.4, alpha, beta-lonone 0.1, USP level glycerine 40, surplus are food grade propylene glycol.
4. the electronic cigarette atomizing liquid of salubrious elegant odor type according to claim 1, is characterized in that, the weight ratio of each composition of electronic cigarette atomizing liquid of described salubrious elegant odor type is preferably:
Natural nicotine 2, tobacco extract 6, menthol 1, raspberry ketone 0.3, ethyl acetate 0.3, alpha, beta-lonone 0.05, USP level glycerine 30, surplus are food grade propylene glycol.
5. a preparation method for the electronic cigarette atomizing liquid of the salubrious elegant odor type as described in any one of claim 1-4, is characterized in that, said method comprising the steps of:
A () will weigh tobacco extract by formula rate, menthol, 4-(4-hydroxyphenyl)-2-butanone add in deionized water, be heated to 50 DEG C ~ 65 DEG C and fully stirring is dissolved completely;
B () adds previously prepared mixed solution by the solution in step (a), described mixed solution is propane diols, ethyl acetate, alpha, beta-lonone weigh by formula rate and make, and fully stirs, then is heated to 45 DEG C ~ 60 DEG C;
C () adds natural nicotine, USP level glycerine after the solution in step (b) is cooled to 15 ~ 30 DEG C, stir;
D () cools after the filled with solution in step (c) at-5 DEG C ~ 0 DEG C temperature, namely obtain the electronic cigarette atomizing liquid of described salubrious elegant odor type.
6. the preparation method of the electronic cigarette atomizing liquid of salubrious elegant odor type according to claim 5, it is characterized in that, described alpha, beta-lonone is made up of following extracting method:
Adopt fruit of a cubeb litsea tree NaOH to make condensing agent, synthesize 1.5 hours, obtain pseudoionone;
In cyclization directly with the pseudoionone crude product without vacuum topping for raw material, add benzene and make solvent, react 0.5 hour, obtain alpha, beta-lonone.
7. the preparation method of the electronic cigarette atomizing liquid of salubrious elegant odor type according to claim 5, it is characterized in that, described menthol is made up of following extracting method:
The aerial part of labiate peppermint is obtained raw peppermint oil through steam distillation;
By freezing for above-mentioned raw peppermint oil rear crystallization, the low solvent recrystallization of boiling of centrifugal gained crystallization obtains pure levorotatory menthol;
Except the mother liquor after decrystallizing to change the mixture of levorotatory menthol and dextrorotation neomenthol into through hydrogenation;
Partly-hydrolysed by above-mentioned ester, through crystallization, distills or point to go other parts in raw peppermint oil after making its borate, obtaining more levorotatory menthol.
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Cited By (3)
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| CN106974323A (en) * | 2017-04-13 | 2017-07-25 | 泉州美丽星空健康科技有限公司 | A kind of clearing lung-heat electronics tobacco tar and its processing technology |
| CN108030143A (en) * | 2017-12-25 | 2018-05-15 | 武汉黄鹤楼香精香料有限公司 | A kind of peppermint tobacco composite electronic tobacco tar |
| CN111714682A (en) * | 2020-07-09 | 2020-09-29 | 杭州承影生物科技有限公司 | Multi-effect patch type medical sanitary towel |
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| CN102154060A (en) * | 2011-03-02 | 2011-08-17 | 广州市澳键香料有限公司 | Formula of tobacco additive essence of hami melon fragrance |
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| CN106974323A (en) * | 2017-04-13 | 2017-07-25 | 泉州美丽星空健康科技有限公司 | A kind of clearing lung-heat electronics tobacco tar and its processing technology |
| CN108030143A (en) * | 2017-12-25 | 2018-05-15 | 武汉黄鹤楼香精香料有限公司 | A kind of peppermint tobacco composite electronic tobacco tar |
| CN111714682A (en) * | 2020-07-09 | 2020-09-29 | 杭州承影生物科技有限公司 | Multi-effect patch type medical sanitary towel |
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| CN105054284B (en) | 2016-08-24 |
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