CN105019226A - Anti-shrinkage anti-pilling wool fabric finishing agent and preparation method thereof - Google Patents
Anti-shrinkage anti-pilling wool fabric finishing agent and preparation method thereof Download PDFInfo
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- CN105019226A CN105019226A CN201510406590.2A CN201510406590A CN105019226A CN 105019226 A CN105019226 A CN 105019226A CN 201510406590 A CN201510406590 A CN 201510406590A CN 105019226 A CN105019226 A CN 105019226A
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Abstract
The invention belongs to the field of finishing agents and discloses an anti-shrinkage anti-pilling wool fabric finishing agent and its preparation method. The finishing agent comprises 9-15 parts of sodium tripolyphosphate, 4-8 parts of fenugreek gum, 3-6 parts of polyethylene glycol, 5-11 parts of hydroxyethyl methylacrylate, 4-7 parts of allyl glycidyl ether, 4-9 parts of sodium N-oleoyl-N-methyl taurinate, 3-6 parts of n-butanol and 240-350 parts of water. The preparation method comprises the following steps: (1) sodium tripolyphosphate, fenugreek gum, polyethylene glycol, hydroxyethyl methylacrylate and allyl glycidyl ether are uniformly stirred to obtain a material A; (2) sodium N-oleoyl-N-methyl taurinate, n-butanol and water are uniformly mixed to obtain a material B; and (3) the material A obtained after uniformly-stirred in the step (1) is put into the material B to obtain a mixture, and the mixture is stirred, sheared and stored so as to obtain the anti-shrinkage anti-pilling wool fabric finishing agent.
Description
Technical field
The invention belongs to finishing agent field, relate to wool fabric finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof.
Background technology
Wool fabric has very many advantages: the features such as such as warming, hair matter softness, good springiness, thermal insulation are strong.But wool fabric also has very many shortcomings.Such as wool fabric shortcoming comprises easy fuzz balls, shrink, felting reaction etc.
Along with improving constantly of the level of consumption and woolen hindlimb unload, the kind of wool fabrics emerges in an endless stream.This not single textile technology can reach, but the set of each side technology such as weaving, chemical industry, macromolecular material and bioengineering, especially show the most outstanding on hindlimb unload.Thus, the hindlimb unload of wool fabrics and the application of various finishing agent are just being subject to the great attention of wool spinning circle personage.At present, wool spinning fabric produce the finishing technique adopted mainly contain soft finish, refuse oil antifouling, shrinkproof, antistatic and hygienic finishing.Resisted shrinkage and Anti-Pilling Finishes are carried out to wool fabric, the performance improving wool fabric is very important.
Summary of the invention
The technical problem solved: wool fabric is as a kind of comparatively common fabric, after long-term use, the phenomenon of shrink and balling-up can be produced, the use of generation to wool fabric of above-mentioned phenomenon has destruction, the object of the invention is wool fabric finishing agent of openly a kind of resisted shrinkage ANTIPILLING and preparation method thereof, solve that wool fabric easily shrinks, the problem of easily balling-up.
Technical scheme: the wool fabric finishing agent that the invention discloses a kind of resisted shrinkage, the wool fabric finishing agent of described resisted shrinkage comprises the composition of following weight parts:
Sodium phosphate trimer 9-15 part,
Fenugreek gum 4-8 part,
Polyethylene glycol 3-6 part,
Hydroxyethyl methylacrylate 5-11 part,
Allyl glycidyl ether 4-7 part,
N-oleoyl-N methyl taurine sodium 4-9 part,
N-butanol 3-6 part,
Water 240-350 part.
Further, the wool fabric finishing agent of described a kind of resisted shrinkage, comprises the composition of following weight parts:
Sodium phosphate trimer 11-13 part,
Fenugreek gum 5-7 part,
Polyethylene glycol 4-5 part,
Hydroxyethyl methylacrylate 7-10 part,
Allyl glycidyl ether 5-6 part,
N-oleoyl-N methyl taurine sodium 5-8 part,
N-butanol 4-5 part,
Water 270-330 part.
The preparation method of the wool fabric finishing agent of described a kind of resisted shrinkage, described preparation method's step is as follows:
(1) respectively sodium phosphate trimer 9-15 part, fenugreek gum 4-8 part, polyethylene glycol 3-6 part, hydroxyethyl methylacrylate 5-11 part, allyl glycidyl ether 4-7 part are poured in container by weight, under rotating speed is 60-120r/min, stir 5-15min, be A material after stirring;
(2) getting N-oleoyl-N methyl taurine sodium 4-9 part, n-butanol 3-6 part, water 240-350 part by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 10-30min is stirred again under rotating speed is 60-120r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 5000rpm-7000rpm, shear time is 5-10min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
The preparation method of the wool fabric finishing agent of described a kind of resisted shrinkage, described step (1) medium speed is 90r/min.
The preparation method of the wool fabric finishing agent of described a kind of resisted shrinkage, shearing rotating speed in described step (3) is 6000rpm.
The preparation method of the wool fabric finishing agent of described a kind of resisted shrinkage, in described step (3), shear time is 8min.
Beneficial effect: the wool fabric arranged through wool fabric finishing agent of the present invention has good effect in ANTIPILLING and resisted shrinkage, and ANTIPILLING grade is very high, still has the effect of good resisted shrinkage after repeatedly cleaning.Effectively raise the quality of wool fabric, the hydroxyethyl methylacrylate added in wool fabric of the present invention and allyl glycidyl ether create great effect in performance above-mentioned functions.
Detailed description of the invention
Embodiment 1
(1) pouring in container by sodium phosphate trimer 9 parts, fenugreek gum 8 parts, polyethylene glycol 3 parts, hydroxyethyl methylacrylate 11 parts, allyl glycidyl ether 7 parts respectively by weight, under rotating speed is 120r/min, stirs 5min, is A material after stirring;
(2) getting N-oleoyl-9 parts, N methyl taurine sodium, n-butanol 3 parts, 350 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 30min is stirred again under rotating speed is 120r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 7000rpm, shear time is 10min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Embodiment 2
(1) pouring in container by sodium phosphate trimer 15 parts, fenugreek gum 4 parts, polyethylene glycol 6 parts, hydroxyethyl methylacrylate 5 parts, allyl glycidyl ether 4 parts respectively by weight, under rotating speed is 60r/min, stirs 15min, is A material after stirring;
(2) getting N-oleoyl-4 parts, N methyl taurine sodium, n-butanol 6 parts, 240 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 10min is stirred again under rotating speed is 60r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 5000rpm, shear time is 5min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Embodiment 3
(1) pouring in container by sodium phosphate trimer 13 parts, fenugreek gum 5 parts, polyethylene glycol 4 parts, hydroxyethyl methylacrylate 10 parts, allyl glycidyl ether 6 parts respectively by weight, under rotating speed is 120r/min, stirs 5min, is A material after stirring;
(2) getting N-oleoyl-5 parts, N methyl taurine sodium, n-butanol 5 parts, 330 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 30min is stirred again under rotating speed is 120r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 7000rpm, shear time is 10min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Embodiment 4
(1) pouring in container by sodium phosphate trimer 11 parts, fenugreek gum 7 parts, polyethylene glycol 5 parts, hydroxyethyl methylacrylate 7 parts, allyl glycidyl ether 5 parts respectively by weight, under rotating speed is 60r/min, stirs 15min, is A material after stirring;
(2) getting N-oleoyl-8 parts, N methyl taurine sodium, n-butanol 4 parts, 270 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 10min is stirred again under rotating speed is 60r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 5000rpm, shear time is 5min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Embodiment 5
(1) pouring in container by sodium phosphate trimer 12 parts, fenugreek gum 6 parts, polyethylene glycol 5 parts, hydroxyethyl methylacrylate 8 parts, allyl glycidyl ether 5 parts respectively by weight, under rotating speed is 90r/min, stirs 10min, is A material after stirring;
(2) getting N-oleoyl-7 parts, N methyl taurine sodium, n-butanol 4 parts, 300 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 20min is stirred again under rotating speed is 90r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 6000rpm, shear time is 8min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Comparative example 1
(1) pouring in container by sodium phosphate trimer 9 parts, fenugreek gum 8 parts, polyethylene glycol 3 parts respectively by weight, under rotating speed is 120r/min, stirs 5min, is A material after stirring;
(2) getting N-oleoyl-9 parts, N methyl taurine sodium, n-butanol 3 parts, 350 parts, water by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 30min is stirred again under rotating speed is 120r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 7000rpm, shear time is 10min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
Wool fabric is immersed after leaving standstill 2h, 2h in the finishing agent of embodiments of the invention and comparative example and fabric is dried naturally.Measure the ANTIPILLING grade of wool fabric, after again wool fabric being cleaned 20 times in addition, measure the shrinkage factor of wool fabric, result is as follows:
| ANTIPILLING grade | Shrinkage factor | |
| Embodiment 1 | 4 | 3.5% |
| Embodiment 2 | 4 | 3.7% |
| Embodiment 3 | 4 | 3.2% |
| Embodiment 4 | 4 | 2.9% |
| Embodiment 5 | 5 | 1.3% |
| Comparative example 1 | 2 | 8.7% |
Claims (6)
1. a wool fabric finishing agent for resisted shrinkage, is characterized in that, the wool fabric finishing agent of described resisted shrinkage comprises the composition of following weight parts:
Sodium phosphate trimer 9-15 part,
Fenugreek gum 4-8 part,
Polyethylene glycol 3-6 part,
Hydroxyethyl methylacrylate 5-11 part,
Allyl glycidyl ether 4-7 part,
N-oleoyl-N methyl taurine sodium 4-9 part,
N-butanol 3-6 part,
Water 240-350 part.
2. the wool fabric finishing agent of a kind of resisted shrinkage according to claim 1, is characterized in that, the wool fabric finishing agent of described resisted shrinkage comprises the composition of following weight parts:
Sodium phosphate trimer 11-13 part,
Fenugreek gum 5-7 part,
Polyethylene glycol 4-5 part,
Hydroxyethyl methylacrylate 7-10 part,
Allyl glycidyl ether 5-6 part,
N-oleoyl-N methyl taurine sodium 5-8 part,
N-butanol 4-5 part,
Water 270-330 part.
3. the preparation method of the wool fabric finishing agent of a kind of resisted shrinkage according to claim 1, is characterized in that, described preparation method's step is as follows:
(1) respectively sodium phosphate trimer 9-15 part, fenugreek gum 4-8 part, polyethylene glycol 3-6 part, hydroxyethyl methylacrylate 5-11 part, allyl glycidyl ether 4-7 part are poured in container by weight, under rotating speed is 60-120r/min, stir 5-15min, be A material after stirring;
(2) getting N-oleoyl-N methyl taurine sodium 4-9 part, n-butanol 3-6 part, water 240-350 part by weight respectively, also mixed in a reservoir by the composition of step (2), is B material;
(3) B material put into by the A material after step (1) being stirred, 10-30min is stirred again under rotating speed is 60-120r/min, with cutter, again shear treatment is carried out to the mixed liquor after mixing again, shearing rotating speed is 5000rpm-7000rpm, shear time is 5-10min, preserving after shearing, is the wool fabric finishing agent of resisted shrinkage ANTIPILLING.
4. the preparation method of the wool fabric finishing agent of a kind of resisted shrinkage according to claim 3, is characterized in that, described step (1) medium speed is 90r/min.
5. the preparation method of the wool fabric finishing agent of a kind of resisted shrinkage according to claim 3, is characterized in that, shearing rotating speed in described step (3) is 6000rpm.
6. the preparation method of the wool fabric finishing agent of a kind of resisted shrinkage according to claim 3, is characterized in that, in described step (3), shear time is 8min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510406590.2A CN105019226A (en) | 2015-07-13 | 2015-07-13 | Anti-shrinkage anti-pilling wool fabric finishing agent and preparation method thereof |
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| CN201510406590.2A CN105019226A (en) | 2015-07-13 | 2015-07-13 | Anti-shrinkage anti-pilling wool fabric finishing agent and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350303A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of blended fabric finishing liquid |
| CN107829198A (en) * | 2017-11-30 | 2018-03-23 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of anti-pilling warming-type looped fabric |
| CN109281174A (en) * | 2018-08-28 | 2019-01-29 | 上海题桥纺织染纱有限公司 | A kind of anti pilling imitates woollen fabric and preparation method thereof |
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| US20040220072A1 (en) * | 1998-10-23 | 2004-11-04 | The Procter & Gamble Company | Fabric color care method |
| CN103643484A (en) * | 2013-11-22 | 2014-03-19 | 江苏波波熊纺织品有限公司 | Knitted fabric anti-pilling finishing agent and preparation method thereof |
| CN103866577A (en) * | 2014-04-01 | 2014-06-18 | 许金补 | Weaving process of wool blended fabrics |
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2015
- 2015-07-13 CN CN201510406590.2A patent/CN105019226A/en active Pending
Patent Citations (3)
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|---|---|---|---|---|
| US20040220072A1 (en) * | 1998-10-23 | 2004-11-04 | The Procter & Gamble Company | Fabric color care method |
| CN103643484A (en) * | 2013-11-22 | 2014-03-19 | 江苏波波熊纺织品有限公司 | Knitted fabric anti-pilling finishing agent and preparation method thereof |
| CN103866577A (en) * | 2014-04-01 | 2014-06-18 | 许金补 | Weaving process of wool blended fabrics |
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| 孟祥英: "烯类单体与羊毛纤维的接枝共聚改性研究", 《纺织学报》 * |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350303A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of blended fabric finishing liquid |
| CN107829198A (en) * | 2017-11-30 | 2018-03-23 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of anti-pilling warming-type looped fabric |
| CN109281174A (en) * | 2018-08-28 | 2019-01-29 | 上海题桥纺织染纱有限公司 | A kind of anti pilling imitates woollen fabric and preparation method thereof |
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Application publication date: 20151104 |