CN105001964A - Microemulsified cutting fluid - Google Patents
Microemulsified cutting fluid Download PDFInfo
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- CN105001964A CN105001964A CN201510383451.2A CN201510383451A CN105001964A CN 105001964 A CN105001964 A CN 105001964A CN 201510383451 A CN201510383451 A CN 201510383451A CN 105001964 A CN105001964 A CN 105001964A
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Abstract
The invention provides a microemulsified cutting fluid. The microemulsified cutting fluid comprises following ingredients, by weight, 3.00 to 21.00% of a pH value conditioning agent, 0.50 to 4.00% of an antirust agent, 0.50 to 2.00% of a bacteriostatic agent, 6.00 to 18.00% of an anionic surfactant, 1.00 to 5.00% of a nonionic surfactant, 1.00 to 4.00% of a corrosion inhibitor, 4.00 to 15.00% of a base oil, and 40 to 50% of water. The microemulsified cutting fluid possesses excellent rust resistance, lubricating properties, and especially excellent corrosion resistance on aluminium alloy, so that a problem that corrosion resistance of conventional microemulsified cutting fluid on different aluminium alloy processing is poor is solved. The microemulsified cutting fluid is suitable for processing of metal such as aluminium parts and steel parts. The microemulsified cutting fluid contains no toxic chemicals, such as nitrite and hydrozybenzene, which are harmful for human body or the environment, is friendly to the environment, and is high in efficiency.
Description
Technical field
The present invention relates to a kind of metal working fluid, be specifically related to a kind of micro-emulsion cutting fluid.
Background technology
Cutting fluid is the important supplementary material of metal cutting process, its lubrication in working angles, rake face and chip can be reduced, friction between rear knife face and machined surface, forming section lubricant film, thus reduce cutting force, friction and watt consumption, reduce cutter and workpiece blank and to rub the surface temperature at position and tool wear, improve the machinability of workpiece material.By it and cutter, convection current between chip and workpiece and the carburetion of generating heat because of cutting, heat in metal cutting is taken away from cutter and workpiece simultaneously, thus effectively reduce cutting temperature, reduce the thermal distortion of workpiece and cutter, keep cutter hardness, improve working accuracy and tool life.
Usually adopt a kind of pure oiliness cutting fluid in existing production, namely the cutting fluid made of additive and appropriate machine oil or kerosene, needs time in working angles to be constantly applied on cutter by lead oil.Because this system is pure oiliness, in metal cutting process, workpiece easily with surrounding medium and cutting fluid decomposition of components or deterioration by oxidation and the corrosive mediums such as the greasy filth that produces contact and corrode, therefore the machine tool component surface contacted with cutting fluid also can corrode.And its cooling, cleansing power is poor, causes the processing problem that workpiece cleaning is more difficult afterwards.Emulsion cutting fluid after improvement can alleviate the deficiency of the cleaning of pure oiliness cutting fluid, cooling power to a certain extent, but its oleaginousness is still higher, easily cause the easy breed bacteria of product surface, although sterilant can be added to reach antibacterial effect, but cure the symptoms, not the disease, and then smelly phenomenon in emulsion summer cannot be solved for a long time.
Though the micro-emulsion cutting fluid of further improvement is not easily smelly, and also have stronger cleaning, the effect of cooling, but its poor lubricity, processing request cannot be reached, simultaneously, micro-emulsion cutting fluid is mainly used in, in aluminium alloy processing, causing aluminum component to be oxidized and phenomenon of turning black due to the meta-acid of micro-emulsion cutting fluid or meta-alkali.
Summary of the invention
In view of this, the invention provides a kind of problem that can solve cleaning, cooling, lubrication, and long service life, aluminium alloy is processed with to the micro-emulsion cutting fluid of splendid corrosion mitigating effect.
A kind of micro-emulsion cutting fluid, according to weight percent meter, comprises following component:
PH value conditioning agent 3.00% ~ 21.00%;
Rust-preventive agent 0.50% ~ 4.00%;
Fungistat 0.50% ~ 2.00%;
Anion surfactant 6.00% ~ 18.00%;
Nonionogenic tenside 1.00% ~ 5.00%;
Inhibiter 1.00% ~ 4.00%;
Base oil 4.00% ~ 15.00%;
Water 40% ~ 50%.
Beneficial effect of the present invention is: compared with existing micro-emulsion cutting fluid, micro-emulsion cutting fluid of the present invention has excellent rust-preventing characteristic, oilness, has splendid rust inhibition to aluminium alloy especially, solves the problem to different aluminum alloys processing slow-releasing difference that existing micro-emulsion cutting fluid exists well.And micro-emulsion cutting fluid of the present invention is suitable for the processing of the metal such as aluminum component, steel part.And micro-emulsion cutting fluid of the present invention is not containing the noxious chemical such as nitrite, organic phenol had a negative impact to human body or environment, is a kind of efficient micro-emulsion cutting fluid of environment-friendly type.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, and following examples are explanation of the invention and the present invention is not limited to following examples.The present invention limits its add-on, is just convenient to enforcement of the present invention, does not illustrate can not to implement outside limited range of the present invention.
The invention provides a kind of micro-emulsion cutting fluid, according to weight percent meter, comprise following component:
PH value conditioning agent 3.00% ~ 21.00%;
Rust-preventive agent 0.50% ~ 4.00%;
Fungistat 0.50% ~ 2.00%;
Anion surfactant 6.00% ~ 18.00%;
Nonionogenic tenside 1.00% ~ 5.00%;
Inhibiter 1.00% ~ 4.00%;
Base oil 4.00% ~ 15.00%;
Water 40% ~ 50%.
PH value conditioning agent is monoethanolamine; diethanolamine; trolamine; dicyclohexyl amine, hexahydroaniline; one or several mixture in alkylolamide, fatty alkanol amide, is adjusted to 9.0 ~ 9.2 by pH value conditioning agent by the pH value of cutting fluid, makes the pH value of cutting fluid be stabilized in optimum value; like this can not only effectively anti-bacteria grow the problem of breeding and avoiding cutting fluid smelly, simultaneously can it be avoided to be corroded by available protecting processing work.
Rust-preventive agent one or more the mixture that to be rust-preventive agent be in aliphatic dicarboxylic acid.Be specially the mixture of one or more in suberic acid, nonane diacid, SA, 11 carbon diacid, dodecanedioic acid, hendecane dicarboxylic acid, 14 carbon diacid.Rust-preventive agent can form one deck lubricant film on the metal surface, can suppress the corrosion that moisture and other Chemical Composition many cause.
Fungistat is one or more mixtures in borate, pyrrolotriazine derivatives, morpholine derivative, polyquaternium, isothiazolinone, growing of bacterium in microemulsion can be suppressed by adding fungistat, can be autologous antibacterial, solve the smelly problem of microemulsion in summer.
Nonionogenic tenside is one or more mixtures in fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, aliphatic amine polyoxyethylene ether, polyoxyethylene sorbitan fatty acid ester.Because nonionogenic tenside is not exist with ionic condition in the solution, so its stability is high, be not subject to the impact that strong electrolyte exists, the impact of acid, alkali is not subject to yet, can be used in combination with other types tensio-active agent, consistency is good, in all kinds of SOLVENTS, all have good solubility, strong adsorption does not occur on a solid surface.And nonionogenic tenside has good resistance to hard water ability, has the feature of low whipability.
Anion surfactant is one or more mixtures in oleic acid, potassium oleate, sodium oleate, tall oil acid, ricinolic acid, fatty alcohol sulfate salt, polyoxyethylenated alcohol sodium sulfate, lipid acid sulfoalkyl acid amides, sulphosuccinates, aliphatic alcohol sulfate.It has dispersion, emulsification, foam, wetting performance, can reduce the interfacial tension in emulsifying system, stops flocculation, smashes micelle, improve the opacifying power of coating, mobility and levelling property, solve the problem of existing micro-emulsion cutting fluid wettability difference.
Inhibiter is aluminum alloy corrosion inhibitor, forms by containing one or more materials in the heterogeneous ring compound of oxynitrides.Be specially one or more mixtures in silicate, molybdate, poly-phosphate, phosphonate, phosphine carboxylic acid, coloured glaze base benzothiazole, sulfonated lignin, phosphoric acid ester, modified phosphate.By adding inhibiter, making micro-emulsion cutting fluid possess satisfactory stability, reducing the probability that metal is corroded, to bacterium and mould, there is resistivity simultaneously, solve the problem that existing emulsion cutting fluid is easily smelly, rotten.
Micro-emulsion cutting fluid of the present invention is mainly used in aluminium alloy processing, because fine aluminium aluminium alloy density is low, but strength ratio is higher, close to or exceed high-quality steel, plasticity is good, can be processed into various section bar, has excellent electroconductibility, thermal conductivity and corrosion stability, industrially widely use, usage quantity is only second to steel.Some aluminium alloys can adopt thermal treatment to obtain good mechanical property, physicals and corrosion resistance.But the meta-acid of existing micro-emulsion cutting fluid or meta-alkali, aluminum component is easily caused to be oxidized and phenomenon of turning black, the application is coordinated with aluminum alloy corrosion inhibitor by pH value conditioning agent, make the micro-emulsion cutting fluid of alkalescence when cutting aluminum alloy materials, there will not be On Blackening, maintain smooth finish and the aesthetic property of aluminium alloy cut surface.
Meanwhile, the present invention also provides the production method of micro-emulsion cutting fluid:
At normal temperatures, be specially within the scope of 0 ~ 40 DEG C, first in reactor, appropriate water is added, then feeding sequence is as follows successively: pH value adjusting agent, rust-preventive agent, fungistat, anion surfactant, nonionogenic tenside, mix to and transparently namely to have produced, wherein dosing intervals is 8 minutes, and stirring velocity is 60 revs/min.
Need to carry out production intermediate compared to most of manufacturer now to compare, the production method of micro-emulsion cutting fluid of the present invention does not need intermediate completely, but disposable uninterruptedly feeding intake is processed till formed product, effectively raise production efficiency, the waste avoiding unnecessary chemical feedstocks and the pollution decreased environment.
Micro-emulsion cutting fluid of the present invention is introduced below in conjunction with embodiment.
Embodiment one
A kind of micro-emulsion cutting fluid described in the present embodiment, comprises following component by weight:
PH value conditioning agent: 20%, rust-preventive agent: 0.5%, fungistat: 0.5%, nonionogenic tenside: 1.5%, anion surfactant: 10%, inhibiter: 1%, base oil: 10%, water: 43.5%.
Specifically comprise following several embodiment:
Concrete, according to weight percent meter, it comprises following component: trolamine: 20%; 11 carbon diacid: 0.5%; Molybdate: 0.5%; Fatty alcohol-polyoxyethylene ether: 1.5%; Ricinolic acid, oleic acid mixture: 10%; Modified phosphate: 1%; Naphthenic mineral oil: 10%; Water: 43.5%.
Concrete, according to weight percent meter, it comprises following component: diethanolamine: 20%; SA: 0.5%; Pyrrolotriazine derivatives: 0.5%; Tall oil acid: 10%; Polyoxyethylene sorbitan fatty acid ester: 1.5%; Silicate: 1%; Intermediate base mineral oil: 10%; Water: 43.5%.
Concrete, according to weight percent meter, it comprises following component: trolamine, diethanolamine, monoethanolamine mixture: 20%; Suberic acid: 0.5%; Isothiazolinone: 0.5%; Aliphatic amine polyoxyethylene ether: 1.5%; Lipid acid sulfoalkyl acid amides: 1.5%; Tryfac 5573: 1%; Naphthenic mineral oil and Viscotrol C unsaturated fatty acid ester: 10%; Water: 43.5%.
Embodiment 2:
A kind of micro-emulsion cutting fluid described in the present embodiment, comprises following component by weight:
PH value conditioning agent: 15%, rust-preventive agent: 1%, fungistat: 1%, nonionogenic tenside: 5%, anion surfactant: 18%, inhibiter: 2%, base oil: 8%, water: 50%.
Specifically comprise following several embodiment:
Concrete, according to weight percent meter, it comprises following component: trolamine, monoethanolamine mixture: 15%; Nonane diacid: 1%; Borate: 1%; Oleic acid: 18%; Alkylphenol polyoxyethylene: 2%; Phosphate diester: 2%; Polyalphaolefin: 8%; Water: 50%.
Concrete, according to weight percent meter, it comprises following component: hexahydroaniline, diethanolamine mixture: 15%; SA: 1%; Polyquaternium: 1%; Alkylphenol polyoxyethylene: 2%; Oleic acid, potassium oleate mixture: 18%; Sulphosuccinates: 2%; Poly-phosphate: 2%; Sunflower seed oil: 8%; Water: 50%.
Concrete, according to weight percent meter, it comprises following component: diethanolamine, trolamine: 15%; 11 carbon diacid: 1%; Pyrrolotriazine derivatives: 1%; Fatty alcohol-polyoxyethylene ether: 2%; Aliphatic alcohol sulfate: 2%; Phosphotriester: 2%; Oleum Gossypii semen: 8%; Water: 50%.
Embodiment 3:
A kind of micro-emulsion cutting fluid described in the present embodiment, comprises following component by weight:
Ph value conditioning agent: 20%, rust-preventive agent: 3%, fungistat: 2%, nonionogenic tenside: 4%, anion surfactant: 9%, inhibiter: 3%, base oil: 15%, water: 44%.
Specifically comprise following several embodiment:
Concrete, according to weight percent meter, it comprises following component: trolamine, dicyclohexyl amine: 20%; Dodecanedioic acid: 3%; Isothiazolinone: 2%; Fatty alcohol-polyoxyethylene ether: 4%; Oleic acid, sulphosuccinates: 9%; Phosphotriester: 3%; Rapeseed oil: 15%; Water: 44%.
Concrete, according to weight percent meter, it comprises following component: dicyclohexyl amine: 20%; Hendecane dicarboxylic acid: 3%; Borate: 2%; Sodium oleate, oleic acid mixture: 9%; Aliphatic amine polyoxyethylene ether: 4%; Phosphate kalium salt: 3%; No. 7 white oils: 15%; Water: 44%.
Concrete, according to weight percent meter, it comprises following component: hexahydroaniline: 20%; 14 carbon diacid: 3%; Polyquaternium: 2%; Oleic acid, polyoxyethylenesorbitan sorbitan monooleate: 9%; Fatty alcohol-polyoxyethylene ether: 4%; Isooctyl alcohol ether phosphate: 3%; Naphthenic mineral oil: 15%; Water: 44%.
Now made a service test by the like product that micro-emulsion cutting fluid of the present invention and market are sold at present and contrast, its result is as shown in table 1.
Table 1:
Note: compare with market sale similar-type products: A: excellent performance, B: performance is suitable, C: poor performance.
1. lubricity test
Ring wear test: utilize the abrasion area of wear test and mensuration Metal contacts to evaluate oil product, abrasion area is less, then lubricity is more excellent, and this test adopts label to be the carbon steel of S-45C, and the concentration of test cutting fluid is: 20 times.Described lubricity test result is in table 2.
Table 2:
2. rustless property test
Cast iron powder is tested: with hexane and acetone the break flour of cast iron powder FC-200 is cleaned, dry, say that filter paper is positioned over the shallow chassis that diameter is 90mm, the FC powder getting 10 grams to be placed on filter paper and to import till it soaks by each sample liquid completely, after 5 minutes, dry test portion, be positioned over indoor, observe and whether have situation of getting rusty to occur.Described rustless property test result is in table 3.
Table 3
Note: compare with market sale similar-type products: A: without getting rusty; B: part is got rusty; C: comprehensively get rusty.
3. resistance to corrupt performance test
PH value assay method: the cutting fluid of getting identical deal, while stirring 0.1N hydrochloric acid soln is instilled in each sample liquid, pH value to cutting fluid reaches 8.5, PH maintenance is evaluated again according to the amount of instillation hydrochloric acid soln, the amount of hydrochloric acid instillation is more, then represent PH maintenance and corrupt excellent performance, the concentration of this test cutting fluid is: 50 times.Described resistance to corrupt the performance test results is in table 4.
Table 4
4. aluminium corrosion inhibition test
The aluminum component of equal size is immersed in completely in 500g sample liquid, observes aluminium workpiece surface phenomenon.Described aluminium corrosion inhibition test result is in table 5.
Table 5
Note: compare with market sale similar-type products: A. is without variable color; B. part variable color; C. variable color completely.
5. antifoam performance test
5.1 stirring-type foaming tests
Pour sample liquid 500g into stirrer, stir after 30 seconds, measure foam height when just stopping, and measure the time needed for lather collapse to the page, the concentration of this test cutting fluid is: 20 times.Described stirring-type foaming test the results are shown in Table 6.
Table 6
5.2 mixer for well-distribution foaming tests
Use mixer for well-distribution, each sample liquid 500g is poured in beaker, stirs after 5 minutes, measure foam height when just stopping, and measure lather collapse to liquid level required time.The concentration of this test cutting fluid is: 20 times.Described stirring-type foaming test the results are shown in Table 7.
Table 7
From table 1 to table 7, micro-emulsion cutting fluid provided by the invention is compared with existing micro-emulsion cutting fluid, there is excellent rust-preventing characteristic, oilness, have splendid rust inhibition to aluminium alloy especially, solve the problem to different aluminum alloys processing rust inhibition difference that existing micro-emulsion cutting fluid exists well.And micro-emulsion cutting fluid of the present invention is suitable for the processing of the metal such as aluminum component, steel part.And micro-emulsion cutting fluid of the present invention is not containing the noxious chemical such as nitrite, organic phenol had a negative impact to human body or environment, is a kind of efficient micro-emulsion cutting fluid of environment-friendly type.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., within the protection domain that all should be included in invention.
Claims (10)
1. a micro-emulsion cutting fluid, is characterized in that, according to weight percent meter, comprises following component:
PH value conditioning agent 3.00% ~ 21.00%;
Rust-preventive agent 0.50% ~ 4.00%;
Fungistat 0.50% ~ 2.00%;
Anion surfactant 6.00% ~ 18.00%;
Nonionogenic tenside 1.00% ~ 5.00%;
Inhibiter 1.00% ~ 4.00%;
Base oil 4.00% ~ 15.00%;
Water 40% ~ 50%.
2. micro-emulsion cutting fluid according to claim 1, is characterized in that, the pH value of described micro-emulsion cutting fluid is adjusted to 9.0 ~ 9.2.
3. micro-emulsion cutting fluid according to claim 1, is characterized in that, described pH value conditioning agent is at least one in following substances: monoethanolamine, diethanolamine, trolamine, dicyclohexyl amine, hexahydroaniline, alkylolamide, fatty alkanol amide.
4. micro-emulsion cutting fluid according to claim 1, is characterized in that, described rust-preventive agent is at least one in following substances: suberic acid, nonane diacid, SA, 11 carbon diacid, dodecanedioic acid, hendecane dicarboxylic acid, 14 carbon diacid.
5. micro-emulsion cutting fluid according to claim 1, is characterized in that, described fungistat is at least one in following substances: borate, pyrrolotriazine derivatives, morpholine derivative, polyquaternium, isothiazolinone.
6. micro-emulsion cutting fluid according to claim 1, it is characterized in that, described nonionogenic tenside is at least one in following substances: fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, aliphatic amine polyoxyethylene ether, polyoxyethylene sorbitan fatty acid ester.
7. micro-emulsion cutting fluid according to claim 1, it is characterized in that, described anion surfactant is at least one in following substances: oleic acid, potassium oleate, sodium oleate, tall oil acid, ricinolic acid, fatty alcohol sulfate salt, polyoxyethylenated alcohol sodium sulfate, lipid acid sulfoalkyl acid amides, sulphosuccinates, aliphatic alcohol sulfate.
8. micro-emulsion cutting fluid according to claim 1, is characterized in that, described inhibiter is aluminum alloy corrosion inhibitor.
9. micro-emulsion cutting fluid according to claim 8, it is characterized in that, described inhibiter is at least one in following substances: silicate, molybdate, poly-phosphate, phosphonate, phosphine carboxylic acid, coloured glaze base benzothiazole, sulfonated lignin, phosphoric acid ester, modified phosphate.
10. micro-emulsion cutting fluid according to claim 1, it is characterized in that, described base oil or oiliness improver are at least one in following substances: mineral oil, polyalphaolefin, vegetables oil, modified vegetable oil or department of botany's oleic acid ester, polyunsaturated fatty acid ester, unsaturated fatty acid ester.
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Application publication date: 20151028 |