CN104997644A - Oil-control spray for hair and skin - Google Patents
Oil-control spray for hair and skin Download PDFInfo
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- CN104997644A CN104997644A CN201510413867.4A CN201510413867A CN104997644A CN 104997644 A CN104997644 A CN 104997644A CN 201510413867 A CN201510413867 A CN 201510413867A CN 104997644 A CN104997644 A CN 104997644A
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Abstract
The invention discloses oil-control spray for hair and skin. The oil-control spray comprises A, 1.1-9.0wt% of a high efficiency oil control complex comprising (i), 0.5-5.0wt% of modified cassava starch, (ii), 0.5-3.0wt% of porous oil suction particles and (iii), 0.1-1.0wt% of zinc pyrrolidone carboxylate, B, 0.1-2.0wt% of a suspension thickening agent, C, 0.5-2.0wt% of a cooling agent, D, 0-10wt% of denatured alcohol, and E, other cosmetic acceptable water-soluble carriers. The oil-control composition is used in a suspension-type spray product form and can instantly produce oil-control effects.
Description
Technical field
The present invention relates to a kind of the dual-purpose control fluid composition of skin, particularly a kind of floating type control oil spraying of quick acting.
Background technology
The problem of puzzlement oily skin consumer, i.e. glossy, the coarse and acne of skin, and be usually scalp greasy, itch, the greasy abnormal flavour of hair, even becomes the root of dandruff and alopecia problem, also can cause the problem of savouring abnormal grade " upset orders of life ".Therefore the personal care articles of control oil becomes an important effect.Though facial cleaning cream, bath gel, shampoo and facial film, cosmetic water that control oil is declared can provide the daily nursing of control oil for consumer, when hot summer, still can not meet the salubrious demand of whole day of most oily skin consumer.And therefore the allegro modern life and busy social activity are developed one and can be eliminated glossy fast, keep salubrious convenient product to meet the possible period of want or need of consumer.
Summary of the invention
The object of this invention is to provide the quick acting control oil spraying that a kind of skin is dual-purpose.
The object of the present invention is achieved like this:
Send out the spraying of skin dual-purpose control oil, composed of the following components:
(A) account for the oily compounding powder agent of efficient control of composition weight 2.65% to 12%, the component of this compounding powder agent is:
(I) accounts for composition weight 2.0-5.0% porous type oil suction granule;
(II) accounts for the modified tapioca starch of composition weight 0.5-5.0%;
(III) accounts for composition weight 0.1-1.0% zinc pyrrolidone carboxylate;
(IV) accounts for composition weight 0.05-1.0% pepo extract;
(B) the suspension thickening agent of compositions 0.1-5.0% is accounted for;
(C) the cool feeling agent of composition weight 0.5-2.0 is accounted for;
(D) denatured ethyl alcohol of composition weight 0-10% is accounted for;
(E) surplus is cosmetics acceptable carrier.
Technical scheme of the present invention also comprises:
Porous type oil absorbent of the present invention is at least one in spherical cellulose acetate or porous type methyl methacrylate microsphere.
Spherical cellulose acetate selected by the present invention is made up of cellulose acetate, degree of acetylation 58-60%, and mean diameter is 6-10 micron, and oil factor is 2.0-3.0ml/g; Described porous type methyl methacrylate microsphere is methyl methacrylate polymer, and mean diameter is 8 microns, and oil factor is 1.2-2.4ml/g.
Described modified tapioca starch is poly methyl silsesquioxane oil modification tapioca.
Effective Zn content of described zinc pyrrolidone carboxylate is 19.4-21.3%.
Described pepo extract dry powder is 10:1-20:1 alcohol extract, and fineness is 120 orders.
The thickening agent that suspends in the present invention is at least one in bentonite, HANSHENGJIAO, carbomer.Preferably scheme suspension thickening agent selects bentonite, and bentonite is water solublity bentonite, layer structure, and every lattice is about containing the electric charge lower than 0.9 unit.
Cool feeling agent of the present invention is-)-Herba Menthae Oxy-1, at least one in 2 propylene glycol, (-)-MGA, (-) menthyl lactate.
Beneficial effect of the present invention: thick and disorderly powder is on the market the control oil product of professional hair caring, but operation uses inconvenient, and be unsuitable for the large-scale production of traditional daily chemical industry.Antihidrotic spray, due to its emphractic hidroschesis principle, can not be used for scalp and facial-care, and can not realize eliminating glossy effect at once.Therefore, the invention is intended to the drawback overcoming the said goods, utilize efficient, non-stimulated porous type oil suction raw material, prepare the control oil spraying of not grease-contained suspension formula system.Moreover compared with tradition control salted cake fried in sesame oil ripple, bath gel, clean product, control oil of the present invention spraying is disposable product, both directly can be applied to skin (comprising face) and also directly can be applied to hair (comprising scalp), easy to use.The most outstanding advantages of control oil of the present invention spraying, is the control oil effect of its quick acting, can, 10 minutes internal diabetes oil removing soapy feelings, eliminates glossy, and without playing a white phenomenon.
Accompanying drawing explanation
Accompanying drawing 1 is the printing opacity value reading meansigma methods of the SEBUMETER method test oily nebulised sample I-Ⅹ of control on probation in 0-12 hour, and the oily effect of reading meansigma methods less display control is better.
Detailed description of the invention
Below in conjunction with embodiment, further detailed description is carried out to the present invention:
The porous type oil absorbent that the present invention selects is at least one in spherical cellulose acetate and porous type methyl methacrylate microsphere.
The spherical cellulose acetate that the present invention selects is made up of cellulose acetate, degree of acetylation 58-60%, and mean diameter is 6-10 micron, and oil factor is 2.0-3.0ml/g.Described spherical cellulose acetate structural formula is as shown in the formula I, and wherein R is the ratio of acetyl group is 58-60%;
The spherical cellulose acetate that the present invention selects is for white is to the spherical fine granular of off-white color.There is following characteristics: high physical strength, highly porous, high-specific surface area; Safety non-toxic and low stimulation, water, oil are compatible.Also can be used for making emulsification cosmetic and facial treatment milk and particle from caking can not being produced, stability and keeping quality good.Spherical cellulose acetate class oil absorbent is larger than the specific surface area of ball shaped cellulose, can absorb own wt 2-3 oils and fats doubly.Spherical cellulose acetate is microporous spherical cellulose acetate liquid pearl, and it, by cellulose acetate dissolves is obtained in organic solvent, is then dispersed into spherical liquid.Its feature comprises, soft-touch, low skin irritability and good breathability.
The porous type methyl methacrylate microsphere that the present invention selects is methyl methacrylate polymer, and mean diameter is 8 microns, and oil factor is 1.2-2.4ml/g; Preferred 1.7-2.4ml/g; .Described porous type methyl methacrylate microsphere belongs to the one of methyl methacrylate cross linked polymer, is made up of methyl methacrylate monomer, the following formula II of its structural formula:
The porous type methyl methacrylate microsphere selective absorbing oils and fats that the present invention selects, its dispersibility is better than silica flour, polyurethane, nylon-type adsorbent, in the alcoholic solution of 10%, disperse the porous type methyl methacrylate microsphere of 10% not assemble in 3 months, can be used for making emulsification cosmetic and spraying, being particularly suitable for front shaking up series products.Described porous type methyl methacrylate microsphere can be SUNPMMA-COCO130, SUNPMMA-COCO170, SUNPMMA-P, SUNPMMA-PH of Sunjin Chemical; Preferred SUNPMMA-P, SUNPMMA-PH
The zinc pyrrolidone carboxylate that the present invention selects is for white is to yellow powder, and chemical name is Bis (5-oxo-L-prolinato-N1, O2) Zinc, INCI title PCAZn, and chemical structural formula is formula III
The zinc pyrrolidone carboxylate that the present invention selects, effective Zn content is 19.4-21.3% (in anhydrous product), effectively can suppress the release of 5a-reductase, thus adjustment sebum secretion, suppress the oxidation of propionibacterium acnes, lipase, free acid, thus the multiple effect reaching that control is oily, minimizing stimulates inflammation of releiving.
The modified tapioca starch that the present invention selects, INCI name be called tapioca (with) polymethylsilsesquioxane Tapioca Starch (and) Polymethylsilsesquioxane outward appearance for white to beige white powder, aluminum-free modified tapioca starch, its compatibility is good, softness, powdery sense by force, can improve the skinfeel of various dissimilar cosmetics; There is reduction greasy feeling especially, eliminate glossy; Advantage skin not whitening, easily disperses in cold water.In addition, other can reduce formulation cost effectively.Described modified tapioca starch can for Akzo Nobel can be
tS and DRY-FLO TS PURE.
The pepo extract that the present invention selects, INCI name is called Cucurbita pepo extract.Summer Squash, Pattypan Squash, Field Pumpkin, for yellow is to brown color fine powder; Described pepo extract is 10:1-20:1 alcohol extract, crosses 120 mesh sieves, in the oily compound of control, play adjustment fat secretion, and convergence pore, antiinflammatory and antibacterial one are to multiple efficacies.
The suspension thickening agent that the present invention selects can at least one in bentonite, HANSHENGJIAO, carbomer, preferred bentonite; Described suspension thickening agent bentonite, also referred to as volcanic clay, silicon Bentonite, for natural hydrated aluminium silicate (Al2O3.4 (SiO2) .H2O), sallow or milky superfine powder, diameter is 1 ~ 150 μm, wherein normal containing mineral such as quartz, Anhydrite, dolomite, calcites, water insoluble or sour, but expand in water, volume increase about 10 times, forms high viscosity and tool thixotropy and pseudoplastic gel.Utilize the thixotropy of thixotrope, i.e. the character of gel and colloidal sol isothermal transformation, form gel when leaving standstill and prevent microparticles settle, become colloidal sol during jolting and be conducive to pouring out.There is some cation in the layer structure formed due to bentonite structure cell, as Cu, Mg, Na, K etc., the fewer inter-layer bonding force of its amount of ions is about little, bentonite more easily expands, therefore do the bentonite that suspension thickening agent selects low cation or anionic charge, preferred each structure cell electric charge is less than the bentonite of 0.9 unit.Swelling great soil group thixotropy suspension thickening agent is used to be conducive to the stable of suspending system.Described bentonite itself has astriction, can promote the control oil effect of formula system.Described suspension thickening agent consumption with realize formula system viscosity for 2000-10000cps be good.
The cool feeling agent that the present invention selects is (-)-Herba Menthae Oxy-1, the one in 2 propylene glycol, (-)-MGA, (-)-menthyl lactate.
(-) that the present invention selects-Herba Menthae Oxy-1,2 propylene glycol, by 2R (formula IV) and 2S (formula V) two kinds of optical isomers, wherein the large 2-3 of the strength ratio 2R of 2S doubly, 1.5-2 multiple stronger than the isomer of racemization.Described (-)-Herba Menthae Oxy-1,2 propylene glycol are STOL coolant agent 10 (coolant agent 10), and its threshold values is 1ppm, are menthol 20%-100%, (-)-Herba Menthae Oxy-1, the cold air intensity of 2 propylene glycol is 2-2.5 times of menthol.
(-) that the present invention selects-MGA, is levo form (VI), is also called 6-isopropyl-9-methyl isophthalic acid, 4-dioxy spiral shell (4,5)-decane-2-methanol; L-9-methyl-6-(1-Methylethyl)-Isosorbide-5-Nitrae-dioxy spiral shell (4,5)-decane-2-methanol, 5 ~ 10mg/kg concentration, can feel that in oral cavity the cool sense of taste strengthened gradually is felt; 10% concentration does not have the abnormal smells from the patient of menthol.Described (-)-MGA is water solublity, can be the FRESCOLAT MGA of the fragrant company of moral.
(-) that the present invention selects-menthyl lactate, for levo form (formula VII), be also called 2 hydroxy propanoic acid-5-methyl-2-isopropyl cyclohexyl), lactic acid ester in the Meng, (-)-menthanol lactic acid ester, 2 hydroxy propanoic acid-5-methyl-2-isopropyl cyclohexyl, be a kind of Herba Menthae derivant; Have slight Herba Menthae fragrance, taste almost insipidness, but with lasting, pleasant cooling effect can be the FRESCOLAT ML of the fragrant company of moral.
Cool feeling agent that the present invention selects plays that local is antipruritic, pain relieving, refrigerant effect, the cold receptor that the effect of cool feeling agent is also on the chafe that cool feeling agent is transmitted is used in control fluid composition of the present invention, though do not cause actual temperature change, Human Physiology produces slight chill in the air, the cool feeling information being delivered to brain can cause nervous system to feed back the signal of suppression sweat gland, smegma, therefore can strengthen the oily effect of control.
In the oily spray composite of control of the present invention, other cosmetics acceptable carriers also comprise, appropriate amount of essence, antiseptic, chelating agen, antioxidant, astringent etc.The preferred methyl parahydroxybenzoate of described antiseptic, propyl p-hydroxybenzoate etc., the preferred disodiumedetate of described chelating agen, described antioxidant is ditertbutylparacresol, the preferred polymeric aluminum chloride of described astringent.
Control fluid composition of the present invention is milky white to translucent liquid product, can use with Sprayable.Spraying of the present invention is liquid under referring to room temperature, by the automatic sprayer containing propellant of conventional hand-held pump spray or routine, adopts finger pressure mode just content can be administered on subject matter.Solid particle in described spraying must reach enough little particle diameter, in 0.05-50 micrometer range, when using conventional sprayer unit, can arrive nozzle by conduit.
Here is the non-limiting example of of the present invention skin dual-purpose control oil spraying.The providing of these embodiments is only used to the object illustrated, can not be interpreted as limitation of the invention, because without departing from the spirit and scope of the present invention, can carry out many changes to the present invention.In these embodiments, unless stated otherwise, all concentration is all percentage by weight.
Preparation embodiment I-Ⅹ
The oily spray composite of control of the present invention can by any known or other be effectively applicable to provide the technology of spray composite to prepare, the method preparing the oily spray composite of control of the present invention comprises conventional preparation and hybrid technology.The suitable method preparing spray composite described in embodiment I-Ⅹ is as follows: suitable quantity of water joined in retort, adds the oily compound powder of efficient control, dispersed with stirring; Then suspension thickening agent is added, abundant dispersed with stirring, the suitable viscosity of adjustment; With adding in aforementioned mixture after dissolve with ethanol essence, cool feeling agent, stir.
Embodiment I-V
Embodiment VI-Ⅹ
The optimum embodiment of the present invention:
| Component: | % by weight |
| Spherical cellulose acetate | 3.0 |
| MPM methyl polymethacrylate microsphere | 2.0 |
| Tapioca | 2.0 |
| Zinc pyrrolidone carboxylate | 0.5 |
| Pepo extract | 0.6 |
| Bentonite | 1.0 |
| Ethanol | 6.0 |
| (-)-Herba Menthae Oxy-1,2 propylene glycol | 0.5 |
| (-)-MGA | 0 |
| (-)-menthyl lactate | 1.0 |
| Methyl parahydroxybenzoate | 0.1 |
| Essence | 0.25 |
| Water | To 100% |
Efficacy assessments embodiment
Efficacy assessments adopts universally acknowledged in the world
the method that method and sensory evaluation combine.
method, it is based on photometer principle, and after the special delustring adhesive tape that a kind of 0.1mm is thick absorbs the oils and fats on human body skin, will become a kind of translucent adhesive tape, its light transmission capacity will change, and the oils and fats of absorption is more, and light transmission capacity will be larger.
Preparation embodiment I-Ⅹ is issued 30 oily skin (transmittance is greater than 70) testers to try out.Sample is applied to facial T block and head respectively near scalp portion; Carry out unified outdoor activity in 30 minutes before on probation, then constant temperature 23 ± 2 DEG C, relative humidity remains on 50 ± 10% room tests.Before using, (0 minute) is used
sM815 tests background, uses within latter 10 minutes, 30 minutes, 1 hour, 6 hours and 12 hours, measure transparency value respectively, gets its average reading value and draws the oily effect curve of control (Fig. 1).Wherein data result meansigma methods < 50 is extremely remarkable for controlling oily effect; Meansigma methods 50-70 is the oily Be very effective of control; Meansigma methods > 70 is not for remarkable without controlling oily effect or controlling oily effect.Sensory evaluation be instrument test simultaneously trier give a mark voluntarily, 0-1 be divided into without the oily effect of control or control oily effect not significantly, 1-2 is divided into the oily Be very effective of control, 2-3 is divided into the oily effect of control very remarkable; Its appraisal result close with instrument test on probation after 10 minutes average score be 1.6, namely control oil of the present invention on probation is sprayed, and within 10 minutes, significantly can experience and alleviate greasy feeling.
Claims (11)
1. send out the spraying of skin dual-purpose control oil for one kind, composed of the following components:
(A) account for the oily compounding powder agent of efficient control of composition weight 2.65% to 12%, the component of this compounding powder agent is:
(I) accounts for composition weight 2.0-5.0% porous type oil suction granule;
(II) accounts for the modified tapioca starch of composition weight 0.5-5.0%;
(III) accounts for composition weight 0.1-1.0% zinc pyrrolidone carboxylate;
(IV) accounts for composition weight 0.05-1.0% pepo extract dry powder;
(B) the water solublity suspension thickening agent of compositions 0.1-5.0% is accounted for;
(C) the cool feeling agent of composition weight 0.5-2.0% is accounted for;
(D) ethanol of composition weight 2-10% is accounted for;
(E) surplus is cosmetics acceptable carrier.
2. control oil according to claim 1 spraying, is characterized in that described porous type oil absorbent is at least one of spherical cellulose acetate or porous type methyl methacrylate microsphere.
3. want the spraying of the oil of the control described in 2 to it is characterized in that described spherical cellulose acetate is made up of cellulose acetate, degree of acetylation 58-60% according to right, mean diameter is 6-10 micron, and oil factor is 2.0-3.0ml/g.
4. want the control oil spraying described in 2 according to right, it is characterized in that described porous type methyl methacrylate microsphere is methyl methacrylate polymer, mean diameter is 8 microns, and oil factor is 1.2-2.4ml/g.
5. want the control oil spraying described in 1 according to right, it is characterized in that described modified tapioca starch is poly methyl silsesquioxane oil modification tapioca.
6. want the control oil spraying described in 1 according to right, it is characterized in that effective Zn content of described zinc pyrrolidone carboxylate is 19.4-21.3%.
7. want the control oil spraying described in 1 according to right, it is characterized in that described pepo extract dry powder is 10:1-20:1 alcohol extract, fineness is 120 orders.
8. want the control oil spraying described in 1 according to right, it is characterized in that described water solublity suspension thickening agent is at least one in bentonite, HANSHENGJIAO, carbomer.
9. want the control oil spraying described in 8 according to right, it is characterized in that described water solublity suspension thickening agent is bentonite.
10. want the control oil spraying described in 9 according to right, it is characterized in that described bentonite is layer structure, every lattice is about containing the electric charge lower than 0.9 unit.
11. want the control oil spraying described in 1 according to right, it is characterized in that described cool feeling agent is for (-)-Herba Menthae Oxy-1, at least one in 2 propylene glycol, (-)-MGA, (-)-menthyl lactate.
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| CN104997644B CN104997644B (en) | 2018-09-25 |
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Cited By (9)
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| CN106726646A (en) * | 2016-12-16 | 2017-05-31 | 广州市白云联佳精细化工厂 | A kind of clarity oil-control matifying lotion and preparation method thereof |
| CN108771635A (en) * | 2018-08-15 | 2018-11-09 | 广州艾蓓生物科技有限公司 | A kind of foundation compositions and preparation method thereof |
| CN111631965A (en) * | 2020-07-07 | 2020-09-08 | 美丽链接生物科技研究院(广东)有限公司 | Plant-derived facial mask with cleaning and makeup removing functions |
| CN111728892A (en) * | 2020-08-14 | 2020-10-02 | 宋家豪 | Oil-control cosmetic cream for improving oily skin and preparation method thereof |
| CN112641640A (en) * | 2020-12-31 | 2021-04-13 | 彭氏(惠州)实业发展有限公司 | Powder-containing oil-control spray and preparation method thereof |
| US11147775B2 (en) * | 2018-09-04 | 2021-10-19 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| US11229610B2 (en) * | 2018-09-04 | 2022-01-25 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| CN114272156A (en) * | 2021-12-10 | 2022-04-05 | 广州融汇化妆品有限公司 | Oil-removing fluffy washing-free hair drying spray and preparation method thereof |
| CN115779131A (en) * | 2022-10-09 | 2023-03-14 | 湖南中腾湘岳生物科技有限公司 | Processing technology of medical dressing and medical dressing thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726646A (en) * | 2016-12-16 | 2017-05-31 | 广州市白云联佳精细化工厂 | A kind of clarity oil-control matifying lotion and preparation method thereof |
| CN108771635A (en) * | 2018-08-15 | 2018-11-09 | 广州艾蓓生物科技有限公司 | A kind of foundation compositions and preparation method thereof |
| US11147775B2 (en) * | 2018-09-04 | 2021-10-19 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| US11229610B2 (en) * | 2018-09-04 | 2022-01-25 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| CN111631965A (en) * | 2020-07-07 | 2020-09-08 | 美丽链接生物科技研究院(广东)有限公司 | Plant-derived facial mask with cleaning and makeup removing functions |
| CN111728892A (en) * | 2020-08-14 | 2020-10-02 | 宋家豪 | Oil-control cosmetic cream for improving oily skin and preparation method thereof |
| CN112641640A (en) * | 2020-12-31 | 2021-04-13 | 彭氏(惠州)实业发展有限公司 | Powder-containing oil-control spray and preparation method thereof |
| CN114272156A (en) * | 2021-12-10 | 2022-04-05 | 广州融汇化妆品有限公司 | Oil-removing fluffy washing-free hair drying spray and preparation method thereof |
| CN114272156B (en) * | 2021-12-10 | 2023-06-16 | 广州融汇化妆品有限公司 | Deoiling fluffy washing-free hair drying spray and preparation method thereof |
| CN115779131A (en) * | 2022-10-09 | 2023-03-14 | 湖南中腾湘岳生物科技有限公司 | Processing technology of medical dressing and medical dressing thereof |
| CN115779131B (en) * | 2022-10-09 | 2024-02-23 | 湖南中腾湘岳生物科技有限公司 | Processing technology of medical dressing and medical dressing thereof |
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