CN104988516B - A kind of aqua type metal cleaner and preparation method thereof - Google Patents
A kind of aqua type metal cleaner and preparation method thereof Download PDFInfo
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- CN104988516B CN104988516B CN201510422932.XA CN201510422932A CN104988516B CN 104988516 B CN104988516 B CN 104988516B CN 201510422932 A CN201510422932 A CN 201510422932A CN 104988516 B CN104988516 B CN 104988516B
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- polyoxyethylene ether
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- deionized water
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Abstract
The invention discloses a kind of aqua type metal cleaners and preparation method thereof, which is prepared from the following components:Potassium stearate, plant fiber powder, cocoanut fatty acid diethanolamide, disodium ethylene diamine tetraacetate, AEO9, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene ether, methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, nonylphenol polyoxyethylene ether, diethylene glycol monobutyl ether, polyvinyl alcohol, nanoscale TiO2, water lily extract lignanoid, cactus root pocket extracting solution, deionized water surplus.Pure plant extracts water lily lignanoid is introduced into the manufacturing field of metal brightener by the present invention, passes through nano-TiO2Addition, clean effect is more notable, can Rapid Cleaning fall the pollutants such as spot, oil stain above part, while can prevent part from getting rusty, part is made to keep bright state for a long time.
Description
Technical field
The present invention relates to cleaning agent fields, and in particular to a kind of aqua type metal cleaner and preparation method thereof.
Background technology
Machining and mechanical equipment, automobile when maintenance and repair when, cleaned mostly using diesel oil, coal Water Oil Or Gas
Liquid cleans part.This not only waste of energy, and there is potential insecurity, it is careless slightly, then it may lead to fire.
In recent years, a kind of novel metal cleaner is gradually widely used, it being capable of diesel oil substitute, kerosene and vapour well
Oil cleans part, and cheap, safe to use, is well suited for mechanized cleaning operation.It can be that metal washs, and
Do not have rust staining.
At present, metal cleaner on the market mostly containing the harmful chemicals such as strong acid, highly basic, phosphate and aluminium salt into
Point, these chemical compositions can not only bring certain damage to metal surface, but also certain harm can be caused to environment, together
When due to complex process, cost is higher, and cleaning ability, antirust period are all to be improved.
Invention content
To solve the above problems, the present invention provides a kind of aqua type metal cleaners and preparation method thereof.
To achieve the above object, the technical solution taken of the present invention is:
A kind of aqua type metal cleaner, is prepared by the component of following mass percent:
Potassium stearate 2-5%, plant fiber powder 3-7%, cocoanut fatty acid diethanolamide 2-4%, ethylenediamine tetrem
Acid disodium 0.5-1%, AE09 2-4%, poly-epoxy succinic acid 1-5%, propylene glycol 2-6%, hexadecanol polyoxyethylene ether 1.5-
4.5%, methyl epichlorohydrin 2.5-6.3%, branched secondary alcohol polyoxyethylene ether 1.1-5.7%, carbamide peroxide 2.3-
5.5%, dodecyl benzene sulfonic acid 2.1-5.7%, nonylphenol polyoxyethylene ether 1-3%, diethylene glycol monobutyl ether 3-6%, poly- second
Enol 1-3%, nanoscale TiO20.3-6.5%, water lily extract lignanoid 3-5%, cactus root pocket extracting solution 3-5%, go
Ion water surplus.
Wherein, plant fiber powder is crushed by stalk, sawdust or timber processing leftover pieces after washing decontamination, mesh number
For 60-100.
To solve the above problems, the embodiment of the present invention additionally provides a kind of preparation method of aqua type metal cleaner, packet
Include following steps:
S1, each component raw material is weighed by above-mentioned formula, the water lily extract lignanoid weighed and cactus root pocket is extracted
Liquid mixes, and adjusts pH value to 4, after freeze-drying, takes out grinding 20 minutes, obtain powder;
S2, the nanoscale TiO that will be weighed2It is scattered in the deionized water weighed by supersonic oscillations equipment;
S3, the deionized water obtained by step S2 is transferred in steam-explosion jar, adds in the potassium stearate weighed, plant fiber
After powder, cocoanut fatty acid diethanolamide, AE09, be passed through nitrogen to steam explosion pressure inside the tank be 0.6~1.1MPa, explosion treatment
7~23min;
After S4, pressure release, it is rapidly added disodium ethylene diamine tetraacetate, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene
Ether, methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, Nonyl pheno
Ether, diethylene glycol monobutyl ether, polyvinyl alcohol, be passed through steam to steam explosion pressure inside the tank be 1.1~1.5MPa, Steam explosion treatment
0.6~2.4min obtains mixed liquor A;
S5, the mixed liquor A of gained is heated to 40 DEG C, adds in step S1 gained powder, stir evenly, until standing 15 points
Clock until deposit-free occurs, obtains mixed liquid B;
S6, the mixed liquid B of gained is down to room temperature naturally, weighed filling to get finished product.
The invention has the advantages that:
Pure plant extracts water lily lignanoid is introduced into the manufacturing field of metal brightener, passes through adding for nano TiO 2
Add, clean effect is more notable, can Rapid Cleaning fall the pollutants such as spot, oil stain above part, while zero can be prevented
Part gets rusty, and part is made to keep bright state for a long time, and preparation process is simple so that raw material is sufficiently mixed, and is further improved
Dirty ability.
Specific embodiment
In order to which objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further
It is described in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair
It is bright.
In following embodiment, used plant fiber powder processes leftover pieces through washing decontamination by stalk, sawdust or timber
After crush, mesh number 60-100.
Embodiment 1
S1, potassium stearate 2%, plant fiber powder 3%, cocoanut fatty acid diethanolamide 2%, ethylenediamine tetrem are weighed
Acid disodium 0.5%, AE09 2%, poly-epoxy succinic acid 1%, propylene glycol 2%, hexadecanol polyoxyethylene ether 1.5%, methyl epoxy
Chloropropane 2.5%, branched secondary alcohol polyoxyethylene ether 1.1%, carbamide peroxide 2.3%, dodecyl benzene sulfonic acid 2.1%, nonyl
Phenol polyethenoxy ether 1%, diethylene glycol monobutyl ether 3%, polyvinyl alcohol 1%, nanoscale TiO20.3%, water lily extract wood fat
Element 3%, cactus root pocket extracting solution 3%, deionized water surplus;The water lily extract lignanoid weighed and cactus root pocket are carried
Liquid is taken to mix, pH value is adjusted to 4, after freeze-drying, takes out grinding 20 minutes, obtain powder;
S2, the nanoscale TiO that will be weighed2It is scattered in the deionized water weighed by supersonic oscillations equipment;
S3, the deionized water obtained by step S2 is transferred in steam-explosion jar, adds in the potassium stearate weighed, plant fiber
After powder, cocoanut fatty acid diethanolamide, AE09, be passed through nitrogen to steam explosion pressure inside the tank be 0.6MPa, explosion treatment
23min;
After S4, pressure release, it is rapidly added disodium ethylene diamine tetraacetate, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene
Ether, methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, Nonyl pheno
Ether, diethylene glycol monobutyl ether, polyvinyl alcohol, be passed through steam to steam explosion pressure inside the tank be 1.1MPa, Steam explosion treatment 2.4min,
Obtain mixed liquor A;
S5, the mixed liquor A of gained is heated to 40 DEG C, adds in step S1 gained powder, stir evenly, until standing 15 points
Clock until deposit-free occurs, obtains mixed liquid B;
S6, the mixed liquid B of gained is down to room temperature naturally, weighed filling to get finished product.
Embodiment 2
S1, potassium stearate 5%, plant fiber powder 7%, cocoanut fatty acid diethanolamide 4%, ethylenediamine tetrem are weighed
Acid disodium 1%, AE09 4%, poly-epoxy succinic acid 5%, propylene glycol 6%, hexadecanol polyoxyethylene ether 4.5%, methyl epoxy chlorine
Propane 6.3%, branched secondary alcohol polyoxyethylene ether 5.7%, carbamide peroxide 5.5%, dodecyl benzene sulfonic acid 5.7%, nonyl phenol
Polyoxyethylene ether 3%, diethylene glycol monobutyl ether 6%, polyvinyl alcohol 3%, nanoscale TiO26.5%th, water lily extract lignanoid
5%th, cactus root pocket extracting solution 5%, deionized water surplus;The water lily extract lignanoid weighed and cactus root pocket are extracted
Liquid mixes, and adjusts pH value to 4, after freeze-drying, takes out grinding 20 minutes, obtain powder;
S2, the nanoscale TiO that will be weighed2It is scattered in the deionized water weighed by supersonic oscillations equipment;
S3, the deionized water obtained by step S2 is transferred in steam-explosion jar, adds in the potassium stearate weighed, plant fiber
After powder, cocoanut fatty acid diethanolamide, AE09, it is 1.1MPa, explosion treatment 7min to be passed through nitrogen to steam explosion pressure inside the tank;
After S4, pressure release, it is rapidly added disodium ethylene diamine tetraacetate, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene
Ether, methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, Nonyl pheno
Ether, diethylene glycol monobutyl ether, polyvinyl alcohol, be passed through steam to steam explosion pressure inside the tank be 1.5MPa, Steam explosion treatment 0.6min,
Obtain mixed liquor A;
S5, the mixed liquor A of gained is heated to 40 DEG C, adds in step S1 gained powder, stir evenly, until standing 15 points
Clock until deposit-free occurs, obtains mixed liquid B;
S6, the mixed liquid B of gained is down to room temperature naturally, weighed filling to get finished product.
Embodiment 3
S1, potassium stearate 3.5%, plant fiber powder 5%, cocoanut fatty acid diethanolamide 3%, ethylenediamine tetraacetic are weighed
Acetic acid disodium 0.75%, AE09 3%, poly-epoxy succinic acid 3%, propylene glycol 4%, hexadecanol polyoxyethylene ether 3%, methyl ring
Oxygen chloropropane 4.4%, branched secondary alcohol polyoxyethylene ether 3.4%, carbamide peroxide 3.9%, dodecyl benzene sulfonic acid 3.9%, nonyl
Base phenol polyethenoxy ether 2%, diethylene glycol monobutyl ether 4.5%, polyvinyl alcohol 2%, nanoscale TiO23.4%th, water lily extract
Lignanoid 4%, cactus root pocket extracting solution 4%, deionized water surplus;By the water lily extract lignanoid weighed and cactus root
Capsule extracting solution mixes, and adjusts pH value to 4, after freeze-drying, takes out grinding 20 minutes, obtain powder;
S2, the nanoscale TiO that will be weighed2It is scattered in the deionized water weighed by supersonic oscillations equipment;
S3, the deionized water obtained by step S2 is transferred in steam-explosion jar, adds in the potassium stearate weighed, plant fiber
After powder, cocoanut fatty acid diethanolamide, AE09, be passed through nitrogen to steam explosion pressure inside the tank be 0.85MPa, explosion treatment
15min;
After S4, pressure release, it is rapidly added disodium ethylene diamine tetraacetate, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene
Ether, methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, Nonyl pheno
Ether, diethylene glycol monobutyl ether, polyvinyl alcohol, be passed through steam to steam explosion pressure inside the tank be 1.3MPa, Steam explosion treatment 1.5min,
Obtain mixed liquor A;
S5, the mixed liquor A of gained is heated to 40 DEG C, adds in step S1 gained powder, stir evenly, until standing 15 points
Clock until deposit-free occurs, obtains mixed liquid B;
S6, the mixed liquid B of gained is down to room temperature naturally, weighed filling to get finished product
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the principle of the present invention, several improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (3)
1. a kind of aqua type metal cleaner, which is characterized in that be prepared by the component of following mass percent:
Potassium stearate 2-5%, plant fiber powder 3-7%, cocoanut fatty acid diethanolamide 2-4%, ethylenediamine tetra-acetic acid two
Sodium 0.5-1%, AEO9 2-4%, poly-epoxy succinic acid 1-5%, propylene glycol 2-6%, hexadecanol polyoxyethylene ether 1.5-4.5%,
Methyl epichlorohydrin 2.5-6.3%, branched secondary alcohol polyoxyethylene ether 1.1-5.7%, carbamide peroxide 2.3-5.5%, 12
Alkyl benzene sulphonate 2.1-5.7%, nonylphenol polyoxyethylene ether 1-3%, diethylene glycol monobutyl ether 3-6%, polyvinyl alcohol 1-3%,
Nanoscale TiO20.3-6.5%, water lily extract lignanoid 3-5%, cactus root pocket extracting solution 3-5%, deionized water surplus.
2. a kind of aqua type metal cleaner according to claim 1, which is characterized in that plant fiber powder is by stalk, saw
End or timber processing leftover pieces crush after washing decontamination, mesh number 60-100.
3. the preparation method of a kind of aqua type metal cleaner according to claim 1, which is characterized in that including walking as follows
Suddenly:
S1, potassium stearate 2-5%, plant fiber powder 3-7%, cocoanut fatty acid diethanolamide 2- are weighed by mass percentage
4%, disodium ethylene diamine tetraacetate 0.5-1%, AEO9 2-4%, poly-epoxy succinic acid 1-5%, propylene glycol 2-6%, hexadecanol gather
Ethylene oxide ether 1.5-4.5%, methyl epichlorohydrin 2.5-6.3%, branched secondary alcohol polyoxyethylene ether 1.1-5.7%, peroxidating
Urea 2.3-5.5%, dodecyl benzene sulfonic acid 2.1-5.7%, nonylphenol polyoxyethylene ether 1-3%, diethylene glycol monobutyl ether 3-
6%, polyvinyl alcohol 1-3%, nanoscale TiO20.3-6.5%, water lily extract lignanoid 3-5%, cactus root pocket extracting solution
3-5%, surplus supply 100% with deionized water, and the water lily extract lignanoid weighed and cactus root pocket extracting solution are mixed,
PH value is adjusted to 4, after freeze-drying, grinding 20 minutes is taken out, obtains powder;
S2, the nanoscale TiO that will be weighed2It is scattered in the deionized water weighed by supersonic oscillations equipment;
S3, the deionized water obtained by step S2 is transferred in steam-explosion jar, adds in the potassium stearate weighed, plant fiber powder, coconut palm
After seed oil fatty diglycollic amide, AEO9, be passed through nitrogen to steam explosion pressure inside the tank be 0.6~1.1MPa, explosion treatment 7~
23min;
After S4, pressure release, be rapidly added disodium ethylene diamine tetraacetate, poly-epoxy succinic acid, propylene glycol, hexadecanol polyoxyethylene ether,
Methyl epichlorohydrin, branched secondary alcohol polyoxyethylene ether, carbamide peroxide, dodecyl benzene sulfonic acid, nonylphenol polyoxyethylene ether,
Diethylene glycol monobutyl ether, polyvinyl alcohol, be passed through steam to steam explosion pressure inside the tank be 1.1~1.5MPa, Steam explosion treatment 0.6~
2.4min obtains mixed liquor A;
S5, the mixed liquor A of gained is heated to 40 DEG C, adds in step S1 gained powder, stir evenly, until 15 minutes are stood,
Until deposit-free occurs, mixed liquid B is obtained;
S6, the mixed liquid B of gained is down to room temperature naturally, weighed filling to get finished product.
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CN108149264A (en) * | 2016-04-27 | 2018-06-12 | 宁波高新区夏远科技有限公司 | A kind of aqua type metal cleaner and preparation method thereof |
WO2018112853A1 (en) * | 2016-12-22 | 2018-06-28 | 郑均思 | Composite detergent of luffa fibers, lotus fibers and wild cane fibers |
WO2018112854A1 (en) * | 2016-12-22 | 2018-06-28 | 郑均思 | Plant fiber detergent |
CN107312634A (en) * | 2017-05-11 | 2017-11-03 | 安徽省金寨县新诚机械制造有限公司 | A kind of high-efficient aluminium alloy mold clean liquid |
CN107841750A (en) * | 2017-11-07 | 2018-03-27 | 常州禾吉纺织品有限公司 | A kind of anti-rust metal detergent |
Citations (3)
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US5895781A (en) * | 1997-12-22 | 1999-04-20 | S. C. Johnson & Son, Inc. | Cleaning compositions for ceramic and porcelain surfaces and related methods |
CN104404544A (en) * | 2014-12-12 | 2015-03-11 | 常熟市天河机械设备制造有限公司 | Metal shell degreasing cleaning agent |
CN104711616A (en) * | 2015-03-25 | 2015-06-17 | 武汉工程大学 | Water-based metal detergent and preparation method thereof |
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2015
- 2015-07-11 CN CN201510422932.XA patent/CN104988516B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5895781A (en) * | 1997-12-22 | 1999-04-20 | S. C. Johnson & Son, Inc. | Cleaning compositions for ceramic and porcelain surfaces and related methods |
CN104404544A (en) * | 2014-12-12 | 2015-03-11 | 常熟市天河机械设备制造有限公司 | Metal shell degreasing cleaning agent |
CN104711616A (en) * | 2015-03-25 | 2015-06-17 | 武汉工程大学 | Water-based metal detergent and preparation method thereof |
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