CN104982537A - Functional mandulapalka milk rich in crocin and iridoid glycoside and preparing method thereof - Google Patents
Functional mandulapalka milk rich in crocin and iridoid glycoside and preparing method thereof Download PDFInfo
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Abstract
The invention discloses functional mandulapalka milk rich in crocin and iridoid glycoside and a preparing method thereof. The functional mandulapalka milk is composed of, by weight, 1-10 parts of gardenia milk pulp, 1-9 parts of mandulapalka milk pulp and 1-3 parts of tea pulp. The gardenia milk pulp is composed of, by weight, 10-20 parts of gardenia powder and 80-90 parts of water. The gardenia powder is prepared by at least one of gardenia whole fruits, gardenia florida and skim gardenia meal. The mandulapalka milk pulp is composed of, by weight, 10-20 parts of mandulapalka powder and 80-90 parts of water. The mandulapalka powder is prepared by mandulapalka and/or skim mandulapalka meal. The tea pulp is composed of, by weight, 1-5 parts of tea and 95-99 parts of water. The functional mandulapalka milk contains protein, unsaturated fat and other nutritious substance, the health care functions of the crocin and iridoid glycoside in gardenia can be fully utilized, and the functions of being resisting to depression, preventing nerve cell and brain tissue damage and improving the heart and cerebral vessel functions and cognitive ability of middle-aged and aged people are achieved.
Description
Technical field
The present invention relates to a kind of function oil Sha soymilk being rich in crocin and iridoid glycoside and preparation method thereof, belong to technical field of food deep processing.
Background technology
Vegetable milk is a generic term, namely from any yoghurt-like product that plant source obtains.Along with " healthy greatly " idea is more and more rooted in the hearts of the people, comprises America and Europe, reduce the absorption of animal origin food, also become common recognition in west, also promoted the exploitation of various novel plant milk.In the U.S., from 2010, popular almond milk, and just exceeded soya-bean milk in 2013, become current most popular vegetable milk.In Europe, oat milk is the most popular.
East, especially in China, since several thousand, has been for raw material prepares soya-bean milk and soymilk with native country soybean always.Recently, due to the appearance of the genetically engineered soybean relative to high yield and low cost, not only impact native country soybean planting industry, also impacting the soy food product industrial structure, particularly soybean is the soymilk of raw material.Because current food law, genetically engineered soybean albumen is not accepted as the soya-bean milk of human consumption and bean product.Therefore, for solving genetically engineered soybean to the impact of the scarcity of raw material that traditional soymilk industry is brought, non-transgenic plant raw material is paid close attention to more.
Oil Sha's beans (Cyperus esculentus L.), although be also referred to as " beans ", it is not legume.But the same with the rice wheat belonging to " Poales ", be annual herb plant.Be different from and utilize seed to be edible rice wheat, the stem tuber that oily Sha's beans of Poales Cyperaceae are but to provide underground is main edible part.Oil Sha beans are the ancient cereal originating in Mediterranean.Be also called " brave chestnut (Tiger nut) " or " water chestnut ".Its protein content about 8%, far exceedes corn, close to rice.But its oil content about 26%, far away higher than 3% brown rice.Its fat is also mainly unsaturated fat (Agric.J., 5:297,2010).The oily Sha's beans baked have the sweet fragrance of chestnut.The Chinese introduction of plant of the seventies in last century.Already proved really have that vitality is strong, the advantage of wide adaptability, strong stress resistance; Be particularly suitable for, in Inner Mongol and area, semidesert, Xinjiang, realizing extensive, intensive, mechanized cultivation.Promote the plantation of oily Sha's beans, still do not solve the Important Action of the Food Security brought because of climate change and cultivated land area, and integrate again " oil, grain, herd, raise ", the industrial crops that comprehensive utilization value is higher.
China is the original producton location of cape jasmine (Gardenia jasminoides Ellis).Cape jasmine is the same with coffee, belongs to rubiaceous dungarunga.For thousands of years, cape jasmine fruit, is used as food always, particularly makes the herbal cuisine of " all diseases of food therapy old man ".What gram Dong " under health food mirror volume " of the Chen Zhi " food therapy eyes side of holograph food therapy old man all disease sides the 14 is given in endowment " of the Song dynasty and the Qing Dynasty, all records: " cape jasmine congee, controls hot swelling ophthalmalgia, closes cook congee with rice one, two, face ripe enter the last money of gardenia florida, mix well food." research shows, gardenia florida not only containing have an appointment 12% protein, and the fat of about 25%.Be all woody oil, saturated fat is different up to the palm oil of more than 40%, and the fat of cape jasmine oil about 80% is unsaturated fat.Compared with olive oil, cape jasmine oil is mainly polybasic unsaturated fatty acid (i.e. essential fatty acid).Polynary unsaturated fat is about 2:1 with the ratio of unit unsaturated fat; Olive oil is about 1:6 then; Namely olive oil lacks essential fatty acid relatively.Cape jasmine is again Chinese Government's approval " being medicine, is again food ".Chinese Pharmacopoeia 2010 editions, cape jasmine is the medicine as having " purging intense heat relieving restlessness " drug effect and listing in." Angong Niuhuang Wan " of Chinese Famous, and " Qing kailing " parenteral solution in recent years developed and " Xingnaojing " parenteral solution, all contain cape jasmine.
For thousands of years, safflower is extensively add in food in west always, particularly adds in milk and dairy produce, be because can make the golden yellow that dairy products become noble, strengthens the health-care effect of food especially.Consider price and the limited output (whole world produces 200 tons per year) of safflower costliness, limit the application of safflower in food industries.By China's law at present, safflower is medicine, does not only allow and adds food, also disapprove and add health products.Cape jasmine be nature except safflower, unique plant containing crocin (Crocins).Crocin is a kind of water-soluble containing oxygen carotenoid, is rare neuron antioxidant.China's Relative resource enriches, low-cost cape jasmine fruit, the iridoids functional mass that the geniposide (geniposide) also do not had containing safflower is representative.A large amount of scientific research proves, crocin and iridoid glycoside all have and improve hyperlipemia and hyperglycemia (CHINA JOURNAL OF CHINESE MATERIA MEDICA, 39:1368,2014), anti-melancholy, even there is prevention brain damage, improve effect (HumPsychopharmacol.29:351,2014 of elderly population memory loss function; Neuropharmacology 89:175,2015).
At present, in technical field of food deep processing, be that the product that development of raw materials goes out mainly contains jasmine tea, cape jasmine beverage and cape jasmine wine etc. with cape jasmine.In addition, be increase the color, smell and taste of food, existing many patents or product, such as CN103651795 A, CN 102450327 A etc., adds with cape jasmine fruit for raw material, through the food additives " Gardenia Yellow " of macroporous resin purification.Be mostly utilize its " water-soluble components " in the said goods, all fail nutriment and the functional mass such as fat, protein, vitamin that make full use of in cape jasmine.
In prior art, a kind of " Ou Qiata (Spanish: horchata) " be prepared from for primary raw material with oily Sha's beans stem tuber, as traditional beverages, still extensively Spain and Western languages are main Hispanic food products market.American-European countries and China in recent years, also the Patent Publication of oily Sha's beans food is in succession had, such as CA2694465 A1, US20140220220 A1, CN 101731710 B, CN 1313056 A, CN 102038180 A and CN 102524884A etc., but find no oily Sha's beans and cape jasmine fruit compatibility prepares patent and the academic article of food.
Summary of the invention
The object of this invention is to provide a kind of function oil Sha soymilk being rich in crocin and iridoid glycoside and preparation method thereof, this function oil Sha soymilk, mainly with oily Sha's beans and cape jasmine for raw material, not containing any soybean and milk raw material, not only containing nutriments such as protein, unsaturated fat and dietary fiber, also can make full use of the health care of crocin in cape jasmine and iridoid glycoside, there is anti-melancholy, prevention neuron and brain tissue impairment, improve the function of mid-aged population cardio and vascular function and cognitive ability.
The present invention provide firstly a kind of cape jasmine milk slurry, this cape jasmine milk slurry is rich in crocin and iridoid glycoside, this cape jasmine milk slurry is starched (or other vegetable milk is starched) mix with oily Sha's soymilk, can prepare dissimilar function vegetable milk, be the important source material preparing vegetable milk.
Cape jasmine milk slurry provided by the invention, with weight parts, described cape jasmine milk slurry can be made up of the gardenia powder of 10 ~ 20 parts and the water of 80 ~ 90 parts;
Described gardenia powder is prepared by least one in the full fruit of cape jasmine, gardenia florida and the degreasing cape jasmine dregs of rice;
The described degreasing cape jasmine dregs of rice be cape jasmine kernel is refined cape jasmine oil after the remaining dregs of rice, can be specifically 201310278649.5 according to application number, denomination of invention prepares for a kind of method disclosed in " cape jasmine fruit oily and sub-critical flow preparation ".In the described degreasing cape jasmine dregs of rice, the mass percentage of total crocin is 0.9% ~ 1.5%, and the mass percentage of total iridoid glycoside is 4.8 ~ 6.1%.Degreasing cape jasmine is broken into 200 orders through superfine powder, and lucifuge refrigerates, for subsequent use.
In above-mentioned cape jasmine milk slurry, described cape jasmine milk slurry specifically can be made up of the gardenia powder of 10 parts and the water of 90 parts.
In above-mentioned cape jasmine milk slurry, the average fineness of described cape jasmine milk slurry can be 1 ~ 5 micron, specifically can be 2 microns.
In above-mentioned cape jasmine milk slurry, described gardenia powder is prepared by least one in the full fruit of cape jasmine, gardenia florida and the degreasing cape jasmine dregs of rice:
When with cape jasmine, fruit and/or gardenia florida are for raw material entirely, the cape jasmine milk slurry prepared is " underflow cape jasmine milk slurry ", and wherein, total solid is not less than 8%; Fat is not less than 2%, and wherein 80% is unsaturated fat; Not containing cholesterol and trans-fatty acid; Albumen is not less than 2%;
When the raw material of described gardenia powder comprises the degreasing cape jasmine dregs of rice, namely described gardenia powder is by 1) the full fruit of cape jasmine and the degreasing cape jasmine dregs of rice, 2) gardenia florida and the degreasing cape jasmine dregs of rice or 3) and cape jasmine entirely really, gardenia florida and the degreasing cape jasmine dregs of rice are when preparing, the cape jasmine milk slurry prepared is " low fat cape jasmine milk slurry ", wherein, total solid is not less than 8%; Fat is not less than 1%, and wherein 80% is unsaturated fat; Not containing cholesterol and trans-fatty acid; Albumen is not less than 2%; Described gardenia powder can be specifically that the gardenia florida of 1:1 and the degreasing cape jasmine dregs of rice prepare by mass ratio.
In above-mentioned cape jasmine milk slurry, in described cape jasmine milk, the content of total crocin is 1000 ~ 2000ppm, and the content of total iridoid is 2000 ~ 4000ppm.In the described degreasing cape jasmine dregs of rice, the mass percentage of total crocin is 0.9% ~ 1.5%, and the mass percentage of total iridoid glycoside is 4.8% ~ 6.1%; By the amount of the degreasing cape jasmine dregs of rice in the raw material that regulates described gardenia powder, not only can be used for regulating the content of fat in described cape jasmine milk, also can be used for regulating the content of the total crocin of functional mass and the content of total iridoid in described cape jasmine milk.In the present invention, 1ppm all represents 1mg/kg, i.e. mass fraction 0.0001%.
Present invention also offers the above-mentioned preparation method preparing milk slurry, it comprises the steps: at least one in complete for above-mentioned cape jasmine fruit, gardenia florida and the degreasing cape jasmine dregs of rice to mix with water after preliminary pulverizing; And then carry out ultramicro grinding, obtain slurries, be described cape jasmine milk slurry.
In the preparation method of above-mentioned cape jasmine milk slurry, described preliminary pulverizing be vibromill pulverize or air-flow crushing into about 200 orders, described method also comprised the step of being toasted at 100 ~ 130 DEG C of temperature by described cape jasmine before pulverizing;
The condition of described ultramicro grinding is as follows: solid-to-liquid ratio 1g:(5 ~ 10) mL, abrasive media 0.1 ~ 0.5mm, rotating speed 1000 ~ 3000r/min, circulating cooling control temperature 30 ~ 60 DEG C, milling time 30 ~ 90min; Specifically can be: solid-to-liquid ratio 1g:5mL, abrasive media 0.5mm, rotating speed 2000r/min, circulating cooling control temperature 40 DEG C, milling time 60min.
Described method also comprises after centrifugal for described slurries after ultramicro grinding, collects solid content, then through 2 ~ 3 described ultramicro grinding, merges the step of slurries.
Above-mentioned preparation method also comprises the steps: at above-mentioned cape jasmine milk slurry after modulating the nutrition and function composition reaching setting, mixed liquor is added homogenizer, homogeneous is carried out under the pressure conditions of the temperature of 40 ~ 50 DEG C, 30 ~ 50MPa, mixed liquor after homogeneous is carried out high-temperature sterilization at 135 DEG C, bottling and packaging.
By above-mentioned cape jasmine milk powder after concentrated and spraying dry, obtain described cape jasmine milk powder, this cape jasmine milk powder is also in protection scope of the present invention.
In the preparation method of above-mentioned cape jasmine milk powder, described drying can be spraying dry, and the moisture content being dried to described cape jasmine milk powder is 3% ~ 5%; Described spray-dired condition is as follows: atomisation pressure 100 ~ 110kg/cm
2, EAT 135 ~ 140 DEG C, temperature of outgoing air 60 ~ 65 DEG C.
Invention further provides a kind of function oil Sha soymilk being rich in crocin and iridoid glycoside, with weight parts, this function oil Sha soymilk can be starched by the cape jasmine milk slurry of 1 ~ 10 part, 1 ~ 9 part of oily Sha's soymilk slurry and 1 ~ 3 part of tea and form;
With weight parts, described cape jasmine milk slurry is made up of the gardenia powder of 10 ~ 20 parts and the water of 80 ~ 90 parts; Described gardenia powder is prepared by least one in the full fruit of cape jasmine, gardenia florida and the degreasing cape jasmine dregs of rice; The described degreasing cape jasmine dregs of rice are by the remaining dregs of rice after cape jasmine kernel refinement cape jasmine oil;
With weight parts, described oily Sha's soymilk slurry can be made up of oily Sha's bean powder of 10 ~ 20 parts and the water of 80 ~ 90 parts; Described oily Sha's bean powder is prepared by oily Sha's beans and/or degreasing oil Sha dregs of beans; Described degreasing oil Sha dregs of beans is by the remaining dregs of rice after oily Sha's beans refinement cyperus esculentus oil;
With weight parts, described tea slurry is made up of the tealeaves of 1 ~ 5 part and the water of 95 ~ 99 parts.
In above-mentioned functions oil Sha soymilk, the average fineness of described cape jasmine milk slurry can be 1 ~ 5 micron, specifically can be 2 microns; The average fineness of described oily Sha's soymilk slurry can be 1 ~ 5 micron, specifically can be 2 microns; The average fineness of described tea slurry can be 1 ~ 5 micron, specifically can be 2 microns.
In above-mentioned functions oil Sha soymilk, in described oily Sha's soymilk slurry, described oily Sha's bean powder is prepared by oily Sha's beans (fruit) and/or degreasing oil Sha dregs of beans, cereal because oily Sha's beans are high fat content: 1) when described oily Sha's bean powder is prepared by oily Sha's beans, namely with complete oily Sha's beans for raw material time, described oily Sha's soymilk slurry is referred to as " underflow oil Sha soymilk ".Wherein total solid is not less than 8%; Fat is not less than 4%, and wherein 80% is unsaturated fat; Not containing cholesterol and trans-fatty acid; Albumen is not less than 2%.2) when described oily Sha's bean powder is prepared by oily Sha's beans and degreasing oil Sha dregs of beans, namely adding degreasing oil Sha dregs of beans is that raw material regulates, and described oily Sha's soymilk is referred to as " low-fat Sha soymilk slurry ".Wherein total solid is not less than 8%; Fat is not less than 1%, and wherein 80% is unsaturated fat; Not containing cholesterol and trans-fatty acid; Albumen is not less than 2%.Described oily Sha's bean powder can be specifically that oily Sha's beans of 1:3 and degreasing oil Sha dregs of beans prepare by mass ratio.
In above-mentioned functions oil Sha soymilk, described degreasing oil Sha dregs of beans is by the remaining dregs of rice after oily Sha's beans refinement cyperus esculentus oil, can be specifically 201310278649.5 according to application number, denomination of invention is a kind of method disclosed in " cape jasmine fruit oil and sub-critical flow preparation thereof ", namely with subcritical butane method, cyperus esculentus oil is extracted to oily Sha's beans, concrete operations are as follows: it is 40 orders that oily Sha's bean powder is broken to granularity, add extractor, introduce liquefied butane again, controlled pressure is 0.5Mpa, temperature is 40 DEG C, extraction time is 30min, in evaporator, butane gasifying after step-down, cyperus esculentus oil can directly be separated with butane.The dregs of rice in extractor are described degreasing oil Sha dregs of beans.
In above-mentioned functions oil Sha soymilk, described tea slurry is except can providing the functional mass such as Tea Polyphenols and caffeine, also can replace the synthetized oxidation preventive agent commonly used and anticorrisive agent, ensure the stability of product, described tealeaves is at least one in green tea, yellow tea, white tea, oolong tea and black tea.
In above-mentioned functions oil Sha soymilk, in described function oil Sha soymilk, total solid is not less than 4%; Fat content is not less than 1%, and wherein unsaturated fat accounts for total fat about 80%; Not containing trans-fatty acid and cholesterol; Protein is not less than 2%; Content 100 ~ the 400ppm of total crocin, content to the 400 ~ 600ppm of total iridoid; Content 200 ~ the 400ppm of total plant polyphenol.
Invention further provides the preparation method of above-mentioned functions oil Sha soymilk, comprise the steps: to mix after at least one pulverizing in complete for cape jasmine fruit, gardenia florida and the degreasing cape jasmine dregs of rice with water, then carry out ultramicro grinding, obtain cape jasmine milk slurry; Mix with water after oily Sha's beans and/or degreasing oil Sha dregs of beans are pulverized, then carry out ultramicro grinding, obtain oily Sha's soymilk slurry; Mix with water after tealeaves is pulverized, then carry out ultramicro grinding, obtain tea slurry; Mix described cape jasmine milk slurry, described oily Sha's soymilk slurry and described tea slurry, obtain described oily Sha's soymilk.
In the preparation method of above-mentioned functions oil Sha soymilk, described pulverizing is that vibromill is pulverized or air-flow crushing, and described method also comprised the step of described cape jasmine, described oily Sha's beans or described tealeaves being toasted at 100 ~ 130 DEG C of temperature before pulverizing;
The condition of described ultramicro grinding is as follows: solid-to-liquid ratio 1g:(5 ~ 10) mL, abrasive media 0.1 ~ 0.5mm, rotating speed 1000 ~ 3000r/min, circulating cooling control temperature 30 ~ 60 DEG C, milling time 30 ~ 90min; Specifically can be: solid-to-liquid ratio 1g:5mL, abrasive media 0.5mm, rotating speed 2000r/min, circulating cooling control temperature 40 DEG C, milling time 60min;
Described method also comprises after centrifugal for described slurries after ultramicro grinding, collects solid content, then through 2 ~ 3 described ultramicro grinding, merges the step of slurries.
Above-mentioned preparation method also comprises the steps: in the mixed liquor of described cape jasmine milk slurry, oily Sha's soymilk slurry and tea slurry, after modulating the nutrition and function composition reaching setting, mixed liquor is added homogenizer, homogeneous is carried out under the pressure conditions of the temperature of 40 ~ 50 DEG C, 30 ~ 50MPa, mixed liquor after homogeneous is carried out high-temperature sterilization at 135 DEG C, bottling and packaging.
Present invention provides the preparation method of a kind of function oil Sha soymilk powder, comprise the steps:, by concentrated for above-mentioned functions oil Sha soymilk warp and spraying dry, described function oil Sha soymilk powder can be obtained.
In the preparation method of above-mentioned functions oil Sha soymilk powder, spraying dry is 3% ~ 5% to the moisture content of described function oil Sha soymilk powder; Described spray-dired condition is as follows: atomisation pressure 100 ~ 110kg/cm
2, EAT 135 ~ 140 DEG C, temperature of outgoing air 60 ~ 65 DEG C.
The function oil Sha soymilk powder prepared by above-mentioned preparation method is also in protection scope of the present invention.
In the present invention, total crocin refers near 440nm, have characteristic absorption peak crocetin and glycosides derivatives summation thereof; Total iridoid glycoside refers to the derivative summation such as Geniposide and glucosides thereof having characteristic absorption peak near 238nm; Total plant polyphenol comprises monomer or the polymeric derivative that plant origin contains phenolic hydroxyl group.
Oily Sha's beans (Cyperus esculentus L.) in the present invention equally with rice wheat belong to Poales (Poales).Be " grass " on the ground, the stem tuber of underground similar " pearl " shape.
Cape jasmine in the present invention, all refer to that original producton location is China, what early summer was opened is white six lobes, autumn Mo knot golden red fruit fructus gardeniae (Gardenia jasminoides Ellis), or its mutation water cape jasmine (Gardenia jasminoides Ellisvar.grandiflora Nakai).
Tea in the present invention, preferred green tea, " aged tea leaf " after particularly utilizing the autumn in summer to prune.Although amino acid content is lower relative to the tender tea of " two leaves and a bud ", Tea Polyphenols is still between 15 ~ 18%, and content of caffeine is about 3%, and raw material must meet " nuisanceless ", " green agricultural product " specification.
The present invention has following beneficial effect:
(1) the oily Sha's beans in the present invention are the ancient cereal of original Mediterranean.Its protein content about 8%, far exceedes corn, close to rice.But its oil content about 26%, far away higher than 3% brown rice.Be the western desert of applicable China, integrate again " oil, grain, herd, raise ", the more much higher novel economizer crop of comprehensive utilization value.
(2) the present invention adopts gardenia florida, cape jasmine fruit or the degreasing cape jasmine dregs of rice to be that raw material is to prepare vegetable milk first.
(3) the cape jasmine fruit adopted in the present invention, gardenia florida contain abundant cape jasmine fruit oil.Cape jasmine fruit oil is not only rich in unsaturated fat, is also rich in phytosterol, squalene, and safflower acids functional mass, is the woody oil of health of distinct Chinese characteristics.In essential fatty acid content and content of phytosterol etc., also exceed the woody olive oil of west characteristic.
(4) although, the present invention is industrialization and large-scale crowd health assessment not yet, according to this R&D team and domestic and international scientific achievement, can predict that the present invention's oil Sha soymilk has the effect improving cardio and vascular function.Its Main Basis is as follows:
A) oily Sha's beans are widely used in field of food.Ministry of Health of China is ratified, and cape jasmine is first approved " being medicine, is again food ".Namely with oily Sha's soymilk that cape jasmine and oily Sha's beans are produced for raw material, also as other vegetable milk, can be regarded as safe " food ".
B) version " Chinese Pharmacopoeia " in 2010, is clearly decided to be " purging intense heat relieving restlessness " the medicinal function of cape jasmine.I.e. removing toxic substances and anti-melancholy effect.
C) nearest, Phytomedicine (17 (2010) 840-843) reports, cape jasmine crocetin is improved the effect of sleep quality, meanwhile, does not also observe the generation of any side reaction.The research of Phytomedicine (18 (2011) 575-578) pharmacokinetic shows that healthy population cape jasmine crocetin infiltration rate is more than beta carotene, lutein and lycopene are all fast, take single dose 22.5mg crocetin, also do not observe any side reaction of cape jasmine crocetin.
D) international scientific journals Molecules (19:19350-19360,2014) reports, and cape jasmine oil can reduce the desperate introgression of melancholia mouse effectively.Domestic magazine XI AN JIAOTONG UNIVERSITY Subject Index (31 volumes the 6th phase in 2010) and " Nanfang Medical Univ's journal (2008,28 volumes the 9th phase) is all reported, cape jasmine fruit oil can improve memory and the learning functionality of brain damage mouse; Also effect that is calm and improving water flood can be had.
E) recent international scholarly journal Hum Psychopharmacol.29:351,2014; And Neuropharmacology89:175,2015) all reporting that safflower extract and cape jasmine berry extract prove at clinical and animal experiment respectively all can effective prevention and therapy senile dementia.
(5) cape jasmine is only two Plants containing crocin of nature with safflower.Have the cape jasmine cultivated area exceeding hundreds thousand of mu in China, compared with safflower, resource is abundanter, cheaper.
(6) the present invention replaces conventional synthetized oxidation preventive agent and anticorrisive agent with ultra-fine full leaf green tea slurry.
(7) the west healthy food take cape jasmine as the east healthy food of representative and oily Sha's beans being representative, be scientifically combined in a creative way " golden milk " with Chinese characteristics, large healthy food industry development can be promoted.Owing to extending cape jasmine, the industrial chain of oily Sha's beans and tealeaves, improves agricultural product added value, also must promote the plantation enthusiasm of peasant to cape jasmine and oily Sha's beans, favourable peasant programme.
Detailed description of the invention
The experimental technique used in following embodiment if no special instructions, is conventional method.
Material used in following embodiment, reagent etc., if no special instructions, all can obtain from commercial channels.
The degreasing cape jasmine dregs of rice in following embodiment, refer to by number of patent application 201310278649.5, and denomination of invention is the dregs of rice after a kind of method recorded in embodiment 1 in " cape jasmine fruit oil and sub-critical flow preparation thereof " refines cape jasmine oil.Through 120 DEG C of bakings, pulverize, cross 200 mesh sieves for subsequent use, in order to allocate the fat in cape jasmine milk slurry and function oil Sha soymilk, the content of total crocin and total iridoid.
Degreasing oil Sha dregs of beans in following embodiment, refer to that by number of patent application be 201310278649.5, denomination of invention is the dregs of rice after the method lard oil Sha beans recorded in " a kind of cape jasmine fruit oil and sub-critical flow preparation thereof ", and concrete operations are as follows: it is 40 orders that oily Sha's bean powder is broken to granularity, add extractor, introduce liquefied butane again, controlled pressure is 0.5Mpa, and temperature is 40 DEG C, extraction time is 30min, in evaporator, butane gasifying after step-down, cyperus esculentus oil can directly be separated with butane.The dregs of rice in extractor are degreasing oil Sha dregs of beans.
In following embodiment, the content of total crocin and total iridoid glycoside measures by the following method, the content of aqueous soluble active constituent (about 440nm) and the content sum of fat-soluble active ingredient (about 440nm) are the content of total crocin, and the content of aqueous soluble active constituent (about 238nm) and the content sum of fat-soluble active ingredient (about 238nm) are the content of total iridoid glycoside.
(1) aqueous soluble active constituent in cape jasmine: mainly detected by HPLC method according to Chinese Pharmacopoeia (2010 editions) and GB (GB/T5009.149-2003).
(2) fat-soluble active ingredient in cape jasmine: the method is mainly for mouse colon cancer line C26 such as the liposoluble substance crocetin in grease and Geniposides, step is as follows: by cape jasmine milk of the present invention slurry or the sampling of function oil Sha soymilk slurry, shakes extract through ethyl acetate (be 3:1 with grease volume ratio) normal temperature; Again after ethyl acetate constant volume, with methyl alcohol (30): acetonitrile (30): ethyl acetate (40) is for mobile phase, and C18 post, under normal temperature, detects through HPLC fado wavelength detecting.Respectively with Geniposide (measuring under 238nm) and crocetin (measuring under 440nm) for standard items.
In following embodiment, the content of total plant polyphenol adopts ferrous tartrate spectrophotometric Colo to measure.
The preparation of embodiment 1, cape jasmine milk slurry and cape jasmine milk powder
(1) cape jasmine milk slurry
Prepare cape jasmine milk slurry as follows:
Through 120 DEG C of bakings, 200 mesh sieves will be crossed by not sticking with paste not burnt gardenia florida and the degreasing cape jasmine dregs of rice first process vibrations mill or air-flow crushing.Mix with deionized water, add Ultra-Micro Grinding Equipment NNM03 (German Cacique company produces NORWA type ball mill), condition is as follows: solid-to-liquid ratio is 1:10 (g/mL) again; Abrasive media 0.5mm, rotating speed 2000r/min, circulating cooling control temperature 40 DEG C, milling time 60min.Kambi grinding slurry is separated through centrifugal (4000r/min), solid content is again through 3 ultra micro glue mills, merge slurries, the fineness of grind on average slurries of about 2 microns, after modulating the nutrition and function composition reaching setting, mixed liquor is added homogenizer, homogeneous is carried out under the pressure conditions of the temperature of 45 DEG C, 40MPa, mixed liquor after homogeneous is carried out high-temperature sterilization at 135 DEG C, bottling and packaging, cape jasmine milk slurry can be obtained.
The formula of the present embodiment cape jasmine milk slurry is as follows: with weight parts: 1 part of gardenia powder (0.5 part of gardenia florida and 0.5 part of degreasing cape jasmine dregs of rice) and 9 parts of deionized waters.
The cape jasmine milk slurry that the present embodiment prepares is golden red emulsus for dense fluids, containing total solid 8wt%, fatty 1wt%, protein 2wt%, total crocin 1000ppm (0.1wt%), total iridoid glycoside 4000ppm (0.4wt%).
(2) cape jasmine milk powder
Prepare cape jasmine milk powder as follows:
Above-mentioned cape jasmine milk slurry is suitably concentrated, spray-dried to moisture content be 4%, packaging, cape jasmine milk powder.Wherein spray-dired condition is as follows: atomisation pressure 100kg/cm
2, EAT 138 DEG C, temperature of outgoing air 62 DEG C.
The cape jasmine milk powder that the present embodiment prepares, about fatty 8wt%, protein 16wt%, total crocin 0.8wt%, total iridoid glycoside 3.2wt%.
Embodiment 2, the function oil Sha's soymilk being rich in crocin and iridoid and the preparation of oily Sha's soymilk powder
(1) oily Sha's soymilk slurry is prepared
Prepare function oil Sha soymilk slurry in accordance with the following steps:
A, prepare oily Sha's soymilk slurry
By the direct oily Sha's beans being bought cleaned rear drying by plantation, scrape off epidermis through skinning machine, and degreasing oil Sha dregs of beans is through 120 DEG C of bakings, then crosses 200 mesh sieves through vibrations mill or air-flow crushing.Again with deionized water, be that 1:5 mixes with solid-to-liquid ratio, add Ultra-Micro Grinding Equipment NNM03 (German Cacique company produces NORWA type ball mill) grinding.Abrasive media 0.5mm, turns 2000r/min, circulating cooling control temperature 40 DEG C, milling time 60min.Oil Sha bean gum grinding slurry is separated through centrifugal (4000r/min), and solid content through 3 ultra micro glue mills, merges slurries again, obtain fineness of grind on average oily Sha's soymilk of about 2 microns starch.Lucifuge refrigerates.
The formula of above-mentioned oily Sha's soymilk slurry is as follows: with weight parts: 2 parts of oily Sha's bean powderes (0.5 part of full-cream oily Sha's beans and 1.5 parts of degreasing oil Sha dregs of beans); 8 parts of deionized waters.
B, prepare tea slurry: this example take green tea as representative.200 mesh sieves are crossed through vibrations mill or air-flow crushing.Mix with deionized water again, with solid-to-liquid ratio 1:5, add Ultra-Micro Grinding Equipment NNM03 (German Cacique company produces NORWA type ball mill); Abrasive media 0.5mm, turns 2000r/min, circulating cooling control temperature 40 DEG C, milling time 60min.Tealeaves glue grinding slurry is separated through centrifugal (4000r/min), and solid content through 3 ultra micro glue mill, merges slurries again, obtains the fineness of grind on average tealeaves slurry of about 2 microns.
The formula of tealeaves slurry is as follows: with weight parts: 1.5 parts of green teas, 10 parts of deionized waters.
The above-mentioned light green emulsus for dense fluids prepared; Wherein total polyphenol content is 2500ppm (0.25wt%).Lucifuge refrigerates.
C, preparation function oil Sha soymilk: by the tea slurry prepared in the oily Sha's soymilk slurry prepared in real examination example 1 gained cape jasmine dense milk slurry, above-mentioned steps (A) and above-mentioned steps (B), take mass ratio as the ratio mixing of 1.5:8:1, add in homogenizer, homogeneous to carry out under the pressure of the temperature of 45 DEG C, 40MPa.Solution after homogeneous carries out high-temperature sterilization at 135 DEG C, bottling and packaging, can obtain described function oil Sha soymilk.
Function oil Sha soymilk slurry that the present embodiment prepares is golden yellow emulsus for dense fluids, containing total solid 8wt%, fatty 1wt%, protein 2wt%, total crocin 150ppm (0.015wt%), total iridoid glycoside 600ppm (0.06wt%); Total Tea Polyphenols 250ppm (0.025wt%).
(2) function oil Sha soymilk powder is prepared in accordance with the following steps:
Slurry above-mentioned functions oil Sha soymilk slurry is concentrated, spray-dried and be packaged into function oil Sha soymilk powder, its atomisation pressure 100kg/cm
2, EAT 138 DEG C, temperature of outgoing air 62 DEG C.
The about fatty 8wt% of function oil Sha's soymilk powder that the present embodiment prepares, protein 16wt%, total crocin 0.12wt%, total iridoid glycoside 0.48wt%, total Tea Polyphenols 0.2wt%.
Claims (9)
1. a cape jasmine milk slurry, is characterized in that: with weight parts, and described cape jasmine milk slurry is made up of the gardenia powder of 10 ~ 20 parts and the water of 80 ~ 90 parts;
Described gardenia powder is prepared by least one in the full fruit of cape jasmine, gardenia florida and the degreasing cape jasmine dregs of rice;
The described degreasing cape jasmine dregs of rice are by the remaining dregs of rice after cape jasmine kernel refinement cape jasmine oil.
2. a preparation method for cape jasmine milk powder, it comprises the steps: concentrated for cape jasmine milk slurry according to claim 1 and spraying dry.
3. the cape jasmine milk powder for preparing of preparation method according to claim 2.
4. function oil Sha soymilk, is characterized in that: with weight parts, and described function oil Sha soymilk is starched by the cape jasmine milk slurry of 1 ~ 10 part, 1 ~ 9 part of oily Sha's soymilk slurry and 1 ~ 3 part of tea and formed;
With weight parts, described cape jasmine milk slurry is made up of the gardenia powder of 10 ~ 20 parts and the water of 80 ~ 90 parts; Described gardenia powder is prepared by least one in the full fruit of cape jasmine, gardenia florida and the degreasing cape jasmine dregs of rice; The described degreasing cape jasmine dregs of rice are by the remaining dregs of rice after cape jasmine kernel refinement cape jasmine oil;
With weight parts, described oily Sha's soymilk slurry is made up of oily Sha's bean powder of 10 ~ 20 parts and the water of 80 ~ 90 parts; Described oily Sha's bean powder is prepared by oily Sha's beans and/or degreasing oil Sha dregs of beans; Described degreasing oil Sha dregs of beans is by the remaining dregs of rice after oily Sha's beans refinement cyperus esculentus oil;
With weight parts, described tea slurry is made up of the tealeaves of 1 ~ 5 part and the water of 95 ~ 99 parts.
5. function oil Sha soymilk according to claim 4, is characterized in that: the average fineness of described cape jasmine milk slurry is 1 ~ 5 micron; The average fineness of described oily Sha's soymilk slurry is 1 ~ 5 micron; The average fineness of described tea slurry is 1 ~ 5 micron;
Described tealeaves is at least one in green tea, yellow tea, white tea, oolong tea and black tea.
6. a preparation method for function oil Sha soymilk, comprises the steps: to mix after at least one pulverizing in complete for cape jasmine fruit, gardenia florida and the degreasing cape jasmine dregs of rice with water, then carries out ultramicro grinding, obtain cape jasmine milk slurry; Mix with water after oily Sha's beans and/or degreasing oil Sha dregs of beans are pulverized, then carry out ultramicro grinding, obtain oily Sha's soymilk slurry; Mix with water after tealeaves is pulverized, then carry out ultramicro grinding, obtain tea slurry; Mix described cape jasmine milk slurry, described oily Sha's soymilk slurry and described tea slurry, obtain described oily Sha's soymilk.
7. preparation method according to claim 6, it is characterized in that: the condition of described ultramicro grinding is as follows: solid-to-liquid ratio 1g:(5 ~ 10) mL, abrasive media 0.1 ~ 0.5mm, rotating speed 1000 ~ 3000r/min, circulating cooling control temperature 30 ~ 60 DEG C, milling time 30 ~ 90min.
8. a preparation method for function oil Sha soymilk powder, it comprises the steps: concentrated for the function oil Sha soymilk described in claim 4 or 5 and spraying dry.
9. the function oil Sha soymilk powder for preparing of preparation method according to claim 8.
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| CN201510309971.9A CN104982537B (en) | 2015-06-08 | A kind of function cyperue esculentus milk rich in crocin and iridoid glycoside and preparation method thereof |
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| CN201510309971.9A CN104982537B (en) | 2015-06-08 | A kind of function cyperue esculentus milk rich in crocin and iridoid glycoside and preparation method thereof |
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| CN104982537A true CN104982537A (en) | 2015-10-21 |
| CN104982537B CN104982537B (en) | 2018-06-01 |
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| CN106212835A (en) * | 2016-07-25 | 2016-12-14 | 王志远 | One kind coffee |
| CN106993687A (en) * | 2017-05-09 | 2017-08-01 | 福建岳海水产食品有限公司 | A kind of preparation method of jasmine tea |
| CN111264626A (en) * | 2020-03-16 | 2020-06-12 | 陈世金 | Cyperus esculentus modified soybean milk and preparation method thereof |
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| CN102524884A (en) * | 2011-12-09 | 2012-07-04 | 湖北欧博美生态食品有限公司 | Preparation method of multi-flavor cyperus esculentus fruit beverage |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106212835A (en) * | 2016-07-25 | 2016-12-14 | 王志远 | One kind coffee |
| CN106993687A (en) * | 2017-05-09 | 2017-08-01 | 福建岳海水产食品有限公司 | A kind of preparation method of jasmine tea |
| CN106993687B (en) * | 2017-05-09 | 2020-03-27 | 福建岳海水产食品有限公司 | Preparation method of gardenia tea |
| CN111264626A (en) * | 2020-03-16 | 2020-06-12 | 陈世金 | Cyperus esculentus modified soybean milk and preparation method thereof |
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