CN104939082A - Composite prebiotic and preparation method thereof - Google Patents

Composite prebiotic and preparation method thereof Download PDF

Info

Publication number
CN104939082A
CN104939082A CN201510294443.0A CN201510294443A CN104939082A CN 104939082 A CN104939082 A CN 104939082A CN 201510294443 A CN201510294443 A CN 201510294443A CN 104939082 A CN104939082 A CN 104939082A
Authority
CN
China
Prior art keywords
concentrated
weight portion
feverfew
complex prebiotics
labiatae
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510294443.0A
Other languages
Chinese (zh)
Inventor
杨琼
陈尉娜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xi'an Shan Fang Pharmaceutical Technology Co Ltd
Original Assignee
Xi'an Shan Fang Pharmaceutical Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xi'an Shan Fang Pharmaceutical Technology Co Ltd filed Critical Xi'an Shan Fang Pharmaceutical Technology Co Ltd
Priority to CN201510294443.0A priority Critical patent/CN104939082A/en
Publication of CN104939082A publication Critical patent/CN104939082A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention relates to a preparation method of a composite prebiotic. The composite prebiotic comprises the following raw materials: 10-95 parts by weight of a labiatae Stachys plant, and 10-90 parts by weight of a compositae plant. The labiatae Stachys plant includes at least one of Stachys floridana and Stachys sieboldii, and the compositae plant includes at least one of helianthus tuberosus and cichorium intybus. The composite prebiotic is prepared by subjecting the raw materials to crushing, mixing, extraction, concentration, decoloration, concentration, filtering and drying, and is powder containing stachyose, raffinose, natural fructan and a variety of probiotic components. The composite prebiotic provided by the invention has the effects of promoting intestinal probiotic flora proliferation, improving intestinal flora health, relieving constipation, enhancing immunity and the like, and can used directly as the raw material and ingredient of beverages, food and health food.

Description

A kind of complex prebiotics and preparation method thereof
Technical field
The present invention relates to a kind of combination of prebiotics, belong to functional food and health products and additive, in particular to a kind of complex prebiotics and the preparation method that regulate functions of intestines and stomach.
Background technology
Prebiotics is a kind of dietary supplements, by optionally stimulate the growth of the bacterium in a kind of or minority kind bacterium colony with active and wholesome effect is produced to host thus improve host health can not be digested food composition.Successful prebiotics should be when by UGI, major part not digested and can ferment by gut flora.The most important thing is that it just stimulates the growth of profitable strain, instead of have the harmful bacteria of potential pathogenic or corrupt activity.
Prebiotics mainly comprises various oligosaccharide kind material (Oligosaccharides) or claims compound sugar (being made up of 2 ~ 10 molecule monose).More generally method is functional oligose.
Containing containing the compositions such as stachydrine, stachyose, protein, amino acid, fat, trigonelline in Labiatae betony, and feverfew is as contained composition higher amino acid, inulin, vitamin etc. in jerusalem artichoke, witloof etc.This two classes functional plants is the main source of prebiotic component.Therefore these functional plants containing higher prebiotic component can be obtained natural a kind of complex prebiotics by certain preparation method.This complex prebiotics have promote beneficial flora propagation in intestines, improve intestinal flora health, alleviate constipation, the effect such as enhancing immunity, can be used as beverage, food, health food former, batching directly use.
Summary of the invention
The invention provides a kind of complex prebiotics, in particular to a kind of complex prebiotics and the preparation method that regulate functions of intestines and stomach.
The present invention is achieved through the following technical solutions:
A kind of complex prebiotics, it is characterized in that, described complex prebiotics is that raw material is prepared from by the component of following proportioning:
Labiatae betony 10-95 weight portion
Feverfew 10-90 weight portion;
Preferred:
Labiatae betony 20-70 weight portion
Feverfew 20-65 weight portion;
Preferred:
Labiatae betony 40-60 weight portion
Feverfew 35-55 weight portion;
Preferred:
Labiatae betony 50-55 weight portion
Feverfew 45-50 weight portion.
Labiatae betony of the present invention comprises one or both combinations in Chinese artichoke, kobold, uses fresh or dried complete stool, aerial part or under ground portion.Described feverfew comprises one or both combinations in jerusalem artichoke, witloof, uses fresh or dried complete stool, aerial part or under ground portion.
Complex prebiotics of the present invention be by described raw material components through pulverizing, mixing, extract, concentrated, decolouring, concentrated, filter, obtained after drying.Can be used as beverage, food, health food former, batching directly use.
The preparation method of a kind of complex prebiotics of the present invention, comprises the steps:
1) pulverize and mix
Get Labiatae betony and feverfew, pulverize after mixing or mixing after pulverizing respectively.
2) extract
By the mixture of step 1) gained, be placed in extractor, add Extraction medium, control temperature, lixiviate certain hour, collect extract; Residue repeats extraction operation; Merge the extract extracting operation gained.
3) concentrated
By step 2) extract of gained concentrates, and is concentrated into certain proportion.
4) decolour
The concentrate of step 3) gained is decoloured, collects the liquid after decolouring.
5) concentrated
By liquid after the decolouring of step 4) gained, carry out secondary concentration, be concentrated into certain proportion, cool.
6) filter
By the liquid after cooling in step 5), filter, collect filtrate.
7)
Complex prebiotics is obtained by after the filtrate drying of collecting in step 6).
Wherein step 2) in Extraction medium be the mixture of water or second alcohol and water, Extracting temperature is 20 DEG C-80 DEG C, and extraction time is 30-120min, and extraction time is 1-5 time.Proportion is concentrated between 1.05-1.12 in step 3); Proportion is concentrated between 1.10-1.15 in step 5).Decolouring in step 4) can adopt adsorption bleaching and chromatographic decolorization two kinds of modes.Drying mode in step 7) can adopt spraying dry and drying under reduced pressure two kinds of modes.
The complex prebiotics preparing gained with method of the present invention can be used as beverage, food, health food former, batching directly use.Its primary efficacy is:
1, promote beneficial flora propagation in intestines, improve intestinal flora health, alleviate constipation.
2, immunity of organisms is strengthened.
Detailed description of the invention:
Further illustrate the present invention by the following examples, but not as limitation of the present invention.
Embodiment 1
Get fresh kobold and each 100kg of jerusalem artichoke, it is placed in extractor, adds the water of 1500kg and be heated to 80 DEG C after pulverizing by homogenate jointly, after keeping temperature 60min, filters, collects filtrate; Filter residue repeats extraction and operates 2 times; Merge No. 3 extracts, be placed in decompression concentrator, 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.10; Above-mentioned concentrate is transferred in the reactor that band stirs, starts and stir and about keeping temperature 60 C, 10kg active carbon slowly added in reactor, filters after insulated and stirred 30min, collection filtrate; The filtrate of collection is placed in decompression concentrator again, and 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.15, leave standstill 30min, filter; Filtrate spraying dry, to obtain final product.
Embodiment 2
Get dry kobold and each 100kg of jerusalem artichoke, after co-grinding, be placed in extractor, add the water of 1000kg and be heated to 80 DEG C, after keeping temperature 60min, filter, collect filtrate; Filter residue repeats extraction and operates 2 times; Merge No. 3 extracts, be placed in decompression concentrator, 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.10; Above-mentioned concentrate is transferred in the reactor that band stirs, starts and stir and about keeping temperature 60 C, 10kg active carbon slowly added in reactor, filters after insulated and stirred 30min, collection filtrate; The filtrate of collection is placed in decompression concentrator again, and 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.15, leave standstill 30min, filter; Filtrate decompression crushed after being dried, to obtain final product.
Embodiment 3
Get each 100kg of fresh kobold, Chinese artichoke and jerusalem artichoke, it is placed in extractor, adds the water of 2000kg and be heated to 80 DEG C after pulverizing by homogenate jointly, after keeping temperature 60min, filters, collects filtrate; Filter residue repeats extraction and operates 2 times; Merge No. 3 extracts, be placed in decompression concentrator, 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.10; Above-mentioned concentrate is cooled rear activated-charcoal column excessively, collect efflux; The efflux of collection is placed in decompression concentrator again, and 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.15, leave standstill 30min, filter; Filtrate spraying dry, to obtain final product.
Embodiment 4
Get dry kobold, jerusalem artichoke and each 100kg of witloof, after co-grinding, be placed in extractor, add the water of 1500kg and be heated to 80 DEG C, after keeping temperature 60min, filter, collect filtrate; Filter residue repeats extraction and operates 2 times; Merge No. 3 extracts, be placed in decompression concentrator, 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.10; Above-mentioned concentrate is transferred in the reactor that band stirs, starts and stir and about keeping temperature 60 C, 10kg active carbon slowly added in reactor, filters after insulated and stirred 30min, collection filtrate; The filtrate of collection is placed in decompression concentrator again, and 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.15, leave standstill 30min, filter; Filtrate decompression crushed after being dried, to obtain final product.
Embodiment 5
Get fresh kobold, Chinese artichoke, jerusalem artichoke, each 100kg of witloof, it is placed in extractor, adds the water of 2500kg and be heated to 80 DEG C after pulverizing by homogenate jointly, after keeping temperature 60min, filters, collects filtrate; Filter residue repeats extraction and operates 2 times; Merge No. 3 extracts, be placed in decompression concentrator, 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.10; Above-mentioned concentrate is cooled rear activated-charcoal column excessively, collect efflux; The efflux of collection is placed in decompression concentrator again, and 65 DEG C of reduced pressure concentrations, are concentrated into proportion about 1.15, leave standstill 30min, filter; Filtrate spraying dry, to obtain final product.
By the validity of following description of test complex prebiotics of the present invention.
Complex prebiotics prepared by embodiment 1-5 is tested the impact of Bifidobacterium in-vitro multiplication:
Sample is prepared respectively according to the method for embodiment 1-5 of the present invention.The sample culture medium prepared is configured to 1% solution, with glucose configuration contrast solution, for subsequent use.Get fresh excreta 10 g to add in 200 ml physiological saline and fully mix, get supernatant 1 ml respectively and add in the culture medium of configuration and cultivate, 37 DEG C of fermentations 12 hours, detect bifidobacteria, experimental result is as table 1:
Group The material combination that product uses Bifidobacterium concentration (lgCFU/g is wet just)
Control group Nothing 8.16
Embodiment 1 Kobold, jerusalem artichoke fresh goods 8.66
Embodiment 2 Kobold, jerusalem artichoke dry product 8.68
Embodiment 3 Kobold, Chinese artichoke, witloof fresh goods 8.76
Embodiment 4 Kobold, jerusalem artichoke, witloof dry product 8.86
Embodiment 5 Kobold, Chinese artichoke, jerusalem artichoke, witloof fresh goods 8.75
The results show: all have the effect well promoting Bifidobacterium propagation with the complex prebiotics prepared by inventive method.

Claims (9)

1. a complex prebiotics, is characterized in that, described complex prebiotics is that raw material is prepared from by the component of following proportioning:
Labiatae betony 10-95 weight portion
Feverfew 10-90 weight portion;
Preferred:
Labiatae betony 20-70 weight portion
Feverfew 20-65 weight portion;
Preferred:
Labiatae betony 40-60 weight portion
Feverfew 35-55 weight portion;
Preferred:
Labiatae betony 50-55 weight portion
Feverfew 45-50 weight portion.
2. complex prebiotics according to claim 1, it is characterized in that, described Labiatae betony comprises one or both combinations in Chinese artichoke, kobold, use fresh or dried complete stool, aerial part or under ground portion, described feverfew comprises one or both combinations in jerusalem artichoke, witloof, uses fresh or dried complete stool, aerial part or under ground portion.
3. complex prebiotics according to claim 1 and 2, is characterized in that, described complex prebiotics be by described raw material components through pulverizing, mixing, extract, concentrated, decolouring, concentrated, filter, obtained after drying.
4. the purposes of the complex prebiotics according to any one of claim 1-3, is characterized in that, former, batching as beverage, food, health food directly use.
5. a preparation method for the complex prebiotics described in claim 1-3 any one, is characterized in that, described preparation method comprises the steps:
1) pulverize and mix
Get Labiatae betony and feverfew, pulverize after mixing or mixing after pulverizing respectively;
2) extract
By the mixture of step 1) gained, be placed in extractor, add Extraction medium, control temperature, lixiviate certain hour, collect extract; Residue repeats extraction operation; Merge the extract extracting operation gained;
3) concentrated
By step 2) extract of gained concentrates, and is concentrated into certain proportion;
4) decolour
The concentrate of step 3) gained is decoloured, collects the liquid after decolouring;
5) concentrated
By liquid after the decolouring of step 4) gained, carry out secondary concentration, be concentrated into certain proportion, cool;
6) filter
By the liquid after cooling in step 5), filter, collect filtrate;
7)
Complex prebiotics is obtained by after the filtrate drying of collecting in step 6).
6. method according to claim 5, is characterized in that, step 2) in Extraction medium be the mixture of water or second alcohol and water, Extracting temperature is 20 DEG C-80 DEG C, and extraction time is 30-120min, and extraction time is 1-5 time.
7. method according to claim 5, is characterized in that, is concentrated into proportion between 1.05-1.12 in step 3); Proportion is concentrated between 1.10-1.15 in step 5).
8. method according to claim 5, is characterized in that, the decolouring in step 4) can adopt adsorption bleaching and chromatographic decolorization two kinds of modes.
9. method according to claim 5, is characterized in that, the drying mode in step 7) can adopt spraying dry and drying under reduced pressure two kinds of modes.
CN201510294443.0A 2015-06-02 2015-06-02 Composite prebiotic and preparation method thereof Pending CN104939082A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510294443.0A CN104939082A (en) 2015-06-02 2015-06-02 Composite prebiotic and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510294443.0A CN104939082A (en) 2015-06-02 2015-06-02 Composite prebiotic and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104939082A true CN104939082A (en) 2015-09-30

Family

ID=54154604

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510294443.0A Pending CN104939082A (en) 2015-06-02 2015-06-02 Composite prebiotic and preparation method thereof

Country Status (1)

Country Link
CN (1) CN104939082A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105456407A (en) * 2015-12-16 2016-04-06 西安膳方医药科技有限公司 Novel functional plant composition and application thereof
CN109007586A (en) * 2017-06-09 2018-12-18 鲁南制药集团股份有限公司 A kind of health nutritious noodle

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1300857A (en) * 1999-12-23 2001-06-27 中国食品发酵工业研究所 Stachyose and its preparing process
CN1466459A (en) * 2000-07-24 2004-01-07 �Ʒ� Nutritional composition
CN101081874A (en) * 2007-07-12 2007-12-05 鞍山中兴医药集团有限公司 Preparation technique for abstraction of inulin from chicory
KR20090030441A (en) * 2007-09-20 2009-03-25 (주)아모레퍼시픽 Food composition for reducing abdominal obesity containing dietary fiber and fructooligosaccharide
CN103478530A (en) * 2013-09-02 2014-01-01 陕西科技大学 Oligosaccharide probiotics composition and application thereof as well as method for preparing capsules by using composition
CN104187670A (en) * 2014-09-02 2014-12-10 高鹏 Special dietary formula for assisting patients with diabetes in regulating blood sugar

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1300857A (en) * 1999-12-23 2001-06-27 中国食品发酵工业研究所 Stachyose and its preparing process
CN1466459A (en) * 2000-07-24 2004-01-07 �Ʒ� Nutritional composition
CN101081874A (en) * 2007-07-12 2007-12-05 鞍山中兴医药集团有限公司 Preparation technique for abstraction of inulin from chicory
KR20090030441A (en) * 2007-09-20 2009-03-25 (주)아모레퍼시픽 Food composition for reducing abdominal obesity containing dietary fiber and fructooligosaccharide
CN103478530A (en) * 2013-09-02 2014-01-01 陕西科技大学 Oligosaccharide probiotics composition and application thereof as well as method for preparing capsules by using composition
CN104187670A (en) * 2014-09-02 2014-12-10 高鹏 Special dietary formula for assisting patients with diabetes in regulating blood sugar

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105456407A (en) * 2015-12-16 2016-04-06 西安膳方医药科技有限公司 Novel functional plant composition and application thereof
CN109007586A (en) * 2017-06-09 2018-12-18 鲁南制药集团股份有限公司 A kind of health nutritious noodle

Similar Documents

Publication Publication Date Title
Luo et al. Hydration properties and binding capacities of dietary fibers from bamboo shoot shell and its hypolipidemic effects in mice
CN106173773A (en) A kind of ferment probiotic bacteria solid beverage and preparation method thereof
US9427452B2 (en) Method for preparing fermentation broth of fruits and vegetables
CN105192798B (en) Composite enzyme beverage and preparation method thereof
CN108796017B (en) Bovine bone peptide and enzymolysis extraction method thereof
CN102318806B (en) Preparation method of probiotics fermented pumpkin and carrot vegetable powder
KR101254740B1 (en) A method for preparing an extract of fermented ginger and ginger tea using the smae
CN105767823A (en) Selenium-enriched hericium erinaceus enzyme and preparation method thereof
CN104304749A (en) Chinese herbal medicine feed additive for improving milk yield of dairy cattle and improving dairy quality
CN106072519A (en) A kind of plant fat-reducing ferment and preparation method thereof
CN106234589A (en) A kind of preparation method of antioxidation probiotics fermention breast
CN105886423A (en) Preparation method of biofermentation rice bran meal
CN108433101A (en) A kind of method that leaf of bamboo Ultramicro-powder prepares leaf of bamboo ferment and leaf of bamboo enzyme beverage
CN111329055B (en) Preparation method of trifoliate acanthopanax enzyme
Wang et al. Effects of crude Sphallerocarpus gracilis polysaccharides as potential prebiotics on acidifying activity and growth of probiotics in fermented milk
CN104904918A (en) Functional instant tea and preparation technology thereof
CN106108003A (en) A kind of preparation method rich in the black ginseng of rare ginsenoside Rh2
CN104939082A (en) Composite prebiotic and preparation method thereof
CN102524453A (en) Saussurea involucrate fruit tea
KR101585957B1 (en) Manufacturing method of fermentation product having vitamines and fermentation product manufactured thereby
CN104855628A (en) Formula of functional tea for regulating intestines and stomach and preparation process thereof
CN105724849A (en) Spirulina and probiotic powder and production method thereof
KR20190072923A (en) Antioxidant and Immune-enhancing functional beverage and food composition comprising the extract of edible flowers fermented by lactic acid bacteria and preparation method of the same
CN106901107A (en) A kind of meat ganoderma active bacterium fermented beverage and preparation method thereof
CN113287699A (en) Elaeagnus angustifolia enzyme and preparation process thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20150930