CN104910726A - Flame-retardant reflective heat-insulating paint and preparation technique thereof - Google Patents
Flame-retardant reflective heat-insulating paint and preparation technique thereof Download PDFInfo
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- CN104910726A CN104910726A CN201510340255.7A CN201510340255A CN104910726A CN 104910726 A CN104910726 A CN 104910726A CN 201510340255 A CN201510340255 A CN 201510340255A CN 104910726 A CN104910726 A CN 104910726A
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Abstract
The invention discloses a flame-retardant reflective heat-insulating paint and a preparation technique thereof. The flame-retardant reflective heat-insulating paint comprises the following components in parts by weight: 25-35 parts of acrylic emulsion, 10-25 parts of butyl acetate, 5-15 parts of halogen-free flame retardant, 2-12 parts of heat-reflection heat-insulating powder, 10-20 parts of hollow microbead, 1-8 parts of coupling agent, 2-7 parts of leveling agent, 3-9 parts of film-forming assistant and 20-30 parts of deionized water. The flame-retardant reflective heat-insulating paint is free of halogens, and thus, is nontoxic and environment-friendly. The flame-retardant reflective heat-insulating paint has the advantages of high thermal resistance, high reflectivity and favorable radiant heat transfer performance, can simultaneously have the functions of heat insulation and flame retardancy, has more balanced flame retardancy and heat-insulating property, can implement better flame-retardant and heat-insulating effects, and is suitable for the field of decoration of dwelling houses, school buildings, hotel buildings and other buildings.
Description
Technical field
The present invention relates to paint field, particularly relate to a kind of Flame-retardant reflection insulation paint and preparation technology thereof.
Background technology
Reflective heat-insulation paint is a kind of new energy-saving material that development in recent years is got up, by effectively reflecting, intercepting, the energy of radiation sunlight, can obviously reduce skin, roof and room temp, thus effectively reduce refrigeration equipment such as air-conditioning energy consumption under the high temperature conditions.Therefore, reflective heat-insulation paint can improve Working environment, again saves a large amount of energy.
Along with people are to the multi-purpose requirement of coating, the coating more and more inadaptable social demand of simple function.Flame-retardant reflection insulation paint is the multifunctional coating of the fire-retardant and heat insulating of a kind of equal tool, modern architecture material or the flame retardant properties of other industry to coating propose very high requirement, and exploitation has heat insulation and coating that is anti-flaming function simultaneously and has very important significance.
But, although prior art has the existence of various flame-retardant insulating paint, these coating otherwise flame retardant effect undesirable, or heat-proof quality is poor, or containing halogen, does not meet environmental requirement.
Summary of the invention
The object of the invention is to overcome the deficiency that above-mentioned prior art exists, a kind of strong adhesion, excellent fireproof performance, Flame-retardant reflection insulation paint that heat-insulation and heat-preservation is good are provided.
Meanwhile, present invention also offers a kind of preparation technology of Flame-retardant reflection insulation paint.
For achieving the above object, the present invention is achieved by the following technical solutions:
A kind of Flame-retardant reflection insulation paint, meter comprises following component by weight: ACRYLIC EMULSION 25 ~ 35 parts, N-BUTYL ACETATE 10 ~ 25 parts, halogen-free flame retardants 5 ~ 15 parts, 2 ~ 12 parts, heat-reflecting heat-insulating powder, cenosphere 10 ~ 20 parts, coupling agent 1 ~ 8 part, flow agent 2 ~ 7 parts, film coalescence aid 3 ~ 9 parts, deionized water 20 ~ 30 parts.
Preferably, described halogen-free flame retardants is any one in aluminium hydroxide, magnesium hydroxide, antimonous oxide.
Preferably, described cenosphere is any one in hollow glass micropearl, hollow ceramic microspheres.
Preferably, described coupling agent is any one in silane coupling agent, aluminate coupling agent, titanate coupling agent.
Preferably, described film coalescence aid is any one in glycol ether, butyl glycol ether, alcohol ester 12.
Above-mentioned Flame-retardant reflection insulation paint, its step of preparation process is as follows:
(1) mark takes the material in composition of raw materials by weight;
(2) in stirred pot, add halogen-free flame retardants, heat-reflecting heat-insulating powder, cenosphere, deionized water, mix, obtained mixed slurry;
(3) add in stirred pot by ACRYLIC EMULSION, N-BUTYL ACETATE, be warming up to 70 ~ 90 DEG C, high-speed stirring 2 ~ 4 hours, adds coupling agent, flow agent, film coalescence aid, and high-speed stirring 1 ~ 3h, mixes; Adjust ph 7 ~ 9, after reaching uniform and stable state, is down to normal temperature, filters, and packaging, obtains Flame-retardant reflection insulation paint.
Beneficial effect of the present invention:
Flame-retardant reflection insulation paint prepared by the present invention, not halogen-containing, asepsis environment-protecting.Have thermal resistance large, reflectivity is high, radiative transfer performance is good, and can have the performance of heat-insulating flame-retardant concurrently, fire-retardant with heat insulation performance is more balanced simultaneously, can realize better anti-flaming thermal-insulation effect, is applicable to the decorations field of the buildings such as house, school and hotel.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail.Following examples will contribute to those skilled in the art and understand the present invention further, but not limit the present invention in any form.It should be pointed out that to those skilled in the art, without departing from the inventive concept of the premise, some distortion and improvement can also be made.These all belong to protection scope of the present invention.
A kind of Flame-retardant reflection insulation paint, meter comprises following component by weight: ACRYLIC EMULSION 25 ~ 35 parts, N-BUTYL ACETATE 10 ~ 25 parts, halogen-free flame retardants 5 ~ 15 parts, 2 ~ 12 parts, heat-reflecting heat-insulating powder, cenosphere 10 ~ 20 parts, coupling agent 1 ~ 8 part, flow agent 2 ~ 7 parts, film coalescence aid 3 ~ 9 parts, deionized water 20 ~ 30 parts.
Step of preparation process is as follows:
(1) mark takes the material in composition of raw materials by weight;
(2) in stirred pot, add halogen-free flame retardants, heat-reflecting heat-insulating powder, cenosphere, deionized water, mix, obtained mixed slurry;
(3) add in stirred pot by ACRYLIC EMULSION, N-BUTYL ACETATE, be warming up to 70 ~ 90 DEG C, high-speed stirring 2 ~ 4 hours, adds coupling agent, flow agent, film coalescence aid, and high-speed stirring 1 ~ 3h, mixes; Adjust ph 7 ~ 9, after reaching uniform and stable state, is down to normal temperature, filters, and packaging, obtains Flame-retardant reflection insulation paint.
Flame-retardant reflection insulation paint prepared by the present invention, has the advantages such as strong adhesion, excellent fireproof performance, heat-insulation and heat-preservation be good.
Embodiment 1
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 35 parts, N-BUTYL ACETATE 10 parts, 5 parts, aluminium hydroxide, 12 parts, heat-reflecting heat-insulating powder, hollow glass micropearl 20 parts, silane coupling agent 1 part, flow agent 2 parts, glycol ether 9 parts, deionized water 30 parts.
Embodiment 2
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 25 parts, N-BUTYL ACETATE 25 parts, magnesium hydroxide 15 parts, 2 parts, heat-reflecting heat-insulating powder, hollow ceramic microspheres 10 parts, aluminate coupling agent 1 part, flow agent 7 parts, butyl glycol ether 3 parts, deionized water 20 parts.
Embodiment 3
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 30 parts, N-BUTYL ACETATE 17 parts, antimonous oxide 10 parts, 7 parts, heat-reflecting heat-insulating powder, hollow glass micropearl 15 parts, titanate coupling agent 5 parts, flow agent 4 parts, alcohol ester 12 parts, deionized water 25 parts.
Embodiment 4
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 27 parts, N-BUTYL ACETATE 13 parts, magnesium hydroxide 7 parts, 4 parts, heat-reflecting heat-insulating powder, hollow ceramic microspheres 13 parts, aluminate coupling agent 3 parts, flow agent 4 parts, butyl glycol ether 5 parts, deionized water 22 parts.
Embodiment 5
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 33 parts, N-BUTYL ACETATE 22 parts, antimonous oxide 13 parts, 10 parts, heat-reflecting heat-insulating powder, hollow glass micropearl 18 parts, titanate coupling agent 7 parts, flow agent 6 parts, alcohol ester 12 parts, deionized water 28 parts.
Embodiment 6
Flame-retardant reflection insulation paint of the present invention, meter comprises following component by weight: ACRYLIC EMULSION 25 parts, N-BUTYL ACETATE 19 parts, 11 parts, aluminium hydroxide, 4 parts, heat-reflecting heat-insulating powder, hollow glass micropearl 14 parts, silane coupling agent 8 parts, flow agent 2 parts, glycol ether 9 parts, deionized water 25 parts.
Performance test
Basic mechanical design feature of the present invention is as shown in table 1:
Table 1
As seen from Table 1, Flame-retardant reflection insulation paint prepared by the present invention, has the advantages such as strong adhesion, excellent fireproof performance, heat-insulation and heat-preservation be good.
Above specific embodiments of the invention are described.It is to be appreciated that the present invention is not limited to above-mentioned particular implementation, those skilled in the art can make various distortion or amendment within the scope of the claims, and this does not affect flesh and blood of the present invention.
Claims (6)
1. a Flame-retardant reflection insulation paint, it is characterized in that, meter comprises following component by weight: ACRYLIC EMULSION 25 ~ 35 parts, N-BUTYL ACETATE 10 ~ 25 parts, halogen-free flame retardants 5 ~ 15 parts, 2 ~ 12 parts, heat-reflecting heat-insulating powder, cenosphere 10 ~ 20 parts, coupling agent 1 ~ 8 part, flow agent 2 ~ 7 parts, film coalescence aid 3 ~ 9 parts, deionized water 20 ~ 30 parts.
2. Flame-retardant reflection insulation paint according to claim 1, is characterized in that: described halogen-free flame retardants is any one in aluminium hydroxide, magnesium hydroxide, antimonous oxide.
3. Flame-retardant reflection insulation paint according to claim 1, is characterized in that: described cenosphere is any one in hollow glass micropearl, hollow ceramic microspheres.
4. Flame-retardant reflection insulation paint according to claim 1, is characterized in that: described coupling agent is any one in silane coupling agent, aluminate coupling agent, titanate coupling agent.
5. Flame-retardant reflection insulation paint according to claim 1, is characterized in that: described film coalescence aid is any one in glycol ether, butyl glycol ether, alcohol ester 12.
6. a preparation technology for Flame-retardant reflection insulation paint as claimed in claim 1, is characterized in that, comprises the following steps:
(1) mark takes the material in composition of raw materials by weight;
(2) in stirred pot, add halogen-free flame retardants, heat-reflecting heat-insulating powder, cenosphere, deionized water, mix, obtained mixed slurry;
(3) add in stirred pot by ACRYLIC EMULSION, N-BUTYL ACETATE, be warming up to 70 ~ 90 DEG C, high-speed stirring 2 ~ 4 hours, adds coupling agent, flow agent, film coalescence aid, and high-speed stirring 1 ~ 3h, mixes; Adjust ph 7 ~ 9, after reaching uniform and stable state, is down to normal temperature, filters, and packaging, obtains Flame-retardant reflection insulation paint.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510340255.7A CN104910726A (en) | 2015-06-18 | 2015-06-18 | Flame-retardant reflective heat-insulating paint and preparation technique thereof |
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| CN201510340255.7A CN104910726A (en) | 2015-06-18 | 2015-06-18 | Flame-retardant reflective heat-insulating paint and preparation technique thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106118179A (en) * | 2016-06-25 | 2016-11-16 | 南京和木新材料科技发展有限公司 | A kind of processing method of high resistance combustion decoration panel |
| CN106118180A (en) * | 2016-06-25 | 2016-11-16 | 南京和木新材料科技发展有限公司 | A kind of processing method of fire-resistant waterproof decoration panel |
| CN107057489A (en) * | 2016-12-16 | 2017-08-18 | 吴中区穹窿山天仲高分子材料技术研究所 | It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof |
| CN107459921A (en) * | 2017-09-22 | 2017-12-12 | 广州市黑本新材料科技有限公司 | A kind of transparent heat-insulated anti-flaming dope and preparation method thereof |
| CN110484081A (en) * | 2018-05-15 | 2019-11-22 | 湖北文理学院 | A kind of polyacrylic acid coating of heat-insulating flame-retardant and preparation method thereof |
| CN116445067A (en) * | 2023-04-24 | 2023-07-18 | 东莞市山力高分子材料科研有限公司 | Bi-component fireproof flame-retardant heat-insulating coating and application thereof in automobile production |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101319121A (en) * | 2008-06-03 | 2008-12-10 | 董善刚 | Multifunctional high-efficiency thermal insulation insulating mold paint |
| CN101671523A (en) * | 2009-10-01 | 2010-03-17 | 厦门大学 | Aqueous flame-retardant and thermal-insulated coating and preparation method thereof |
-
2015
- 2015-06-18 CN CN201510340255.7A patent/CN104910726A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101319121A (en) * | 2008-06-03 | 2008-12-10 | 董善刚 | Multifunctional high-efficiency thermal insulation insulating mold paint |
| CN101671523A (en) * | 2009-10-01 | 2010-03-17 | 厦门大学 | Aqueous flame-retardant and thermal-insulated coating and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106118179A (en) * | 2016-06-25 | 2016-11-16 | 南京和木新材料科技发展有限公司 | A kind of processing method of high resistance combustion decoration panel |
| CN106118180A (en) * | 2016-06-25 | 2016-11-16 | 南京和木新材料科技发展有限公司 | A kind of processing method of fire-resistant waterproof decoration panel |
| CN107057489A (en) * | 2016-12-16 | 2017-08-18 | 吴中区穹窿山天仲高分子材料技术研究所 | It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof |
| CN107459921A (en) * | 2017-09-22 | 2017-12-12 | 广州市黑本新材料科技有限公司 | A kind of transparent heat-insulated anti-flaming dope and preparation method thereof |
| CN110484081A (en) * | 2018-05-15 | 2019-11-22 | 湖北文理学院 | A kind of polyacrylic acid coating of heat-insulating flame-retardant and preparation method thereof |
| CN110484081B (en) * | 2018-05-15 | 2021-08-10 | 湖北文理学院 | Heat-insulating flame-retardant polyacrylic acid coating and preparation method thereof |
| CN116445067A (en) * | 2023-04-24 | 2023-07-18 | 东莞市山力高分子材料科研有限公司 | Bi-component fireproof flame-retardant heat-insulating coating and application thereof in automobile production |
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Application publication date: 20150916 |