CN104893299B - 聚丙烯用有机硅阻燃剂及其制备方法 - Google Patents
聚丙烯用有机硅阻燃剂及其制备方法 Download PDFInfo
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- CN104893299B CN104893299B CN201510392553.0A CN201510392553A CN104893299B CN 104893299 B CN104893299 B CN 104893299B CN 201510392553 A CN201510392553 A CN 201510392553A CN 104893299 B CN104893299 B CN 104893299B
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- polypropylene
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- -1 Polypropylene Polymers 0.000 title claims abstract description 58
- 239000004743 Polypropylene Substances 0.000 title claims abstract description 56
- 229920001155 polypropylene Polymers 0.000 title claims abstract description 56
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 51
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 51
- 239000010703 silicon Substances 0.000 title claims abstract description 51
- 239000000835 fiber Substances 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000203 mixture Substances 0.000 claims abstract description 28
- 230000002195 synergetic effect Effects 0.000 claims abstract description 28
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 27
- 229910000077 silane Inorganic materials 0.000 claims abstract description 27
- 230000009970 fire resistant effect Effects 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000002699 waste material Substances 0.000 claims abstract description 23
- 229920002379 silicone rubber Polymers 0.000 claims abstract description 21
- 229920000877 Melamine resin Polymers 0.000 claims abstract description 20
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims abstract description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 239000003921 oil Substances 0.000 claims abstract description 10
- 229920000570 polyether Polymers 0.000 claims abstract description 10
- 150000003376 silicon Chemical class 0.000 claims abstract description 10
- 229910021487 silica fume Inorganic materials 0.000 claims abstract description 9
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 8
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 21
- 239000003063 flame retardant Substances 0.000 claims description 21
- 238000001914 filtration Methods 0.000 claims description 14
- 239000002808 molecular sieve Substances 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 14
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 7
- 239000007795 chemical reaction product Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- 238000002525 ultrasonication Methods 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims 1
- 239000011885 synergistic combination Substances 0.000 claims 1
- 230000002209 hydrophobic effect Effects 0.000 abstract description 9
- 239000000463 material Substances 0.000 abstract description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052760 oxygen Inorganic materials 0.000 abstract description 6
- 239000001301 oxygen Substances 0.000 abstract description 6
- 239000000779 smoke Substances 0.000 abstract description 4
- 238000005452 bending Methods 0.000 abstract description 3
- 229920000642 polymer Polymers 0.000 description 12
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 10
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 8
- 150000001412 amines Chemical class 0.000 description 7
- 239000006227 byproduct Substances 0.000 description 7
- 238000001354 calcination Methods 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 239000002861 polymer material Substances 0.000 description 5
- 235000019504 cigarettes Nutrition 0.000 description 3
- 229910052901 montmorillonite Inorganic materials 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- YUWBVKYVJWNVLE-UHFFFAOYSA-N [N].[P] Chemical compound [N].[P] YUWBVKYVJWNVLE-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- DXZMANYCMVCPIM-UHFFFAOYSA-L zinc;diethylphosphinate Chemical compound [Zn+2].CCP([O-])(=O)CC.CCP([O-])(=O)CC DXZMANYCMVCPIM-UHFFFAOYSA-L 0.000 description 2
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- DDEUBQILYNQUME-UHFFFAOYSA-N S(=O)(=O)([O-])[O-].[NH4+].N1=C(N)N=C(N)N=C1N.[NH4+] Chemical compound S(=O)(=O)([O-])[O-].[NH4+].N1=C(N)N=C(N)N=C1N.[NH4+] DDEUBQILYNQUME-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000004079 fireproofing Methods 0.000 description 1
- 239000012757 flame retardant agent Substances 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 208000021760 high fever Diseases 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 1
- 239000000347 magnesium hydroxide Substances 0.000 description 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000005543 nano-size silicon particle Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/10—Homopolymers or copolymers of propene
- C08L23/12—Polypropene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (7)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710735537.6A CN107474387A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201710735556.9A CN107501940A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201510392553.0A CN104893299B (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510392553.0A CN104893299B (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
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CN201710735537.6A Division CN107474387A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201710735556.9A Division CN107501940A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104893299A CN104893299A (zh) | 2015-09-09 |
CN104893299B true CN104893299B (zh) | 2017-11-14 |
Family
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Family Applications (3)
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CN201710735537.6A Withdrawn CN107474387A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201710735556.9A Withdrawn CN107501940A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201510392553.0A Active CN104893299B (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
Family Applications Before (2)
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CN201710735537.6A Withdrawn CN107474387A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
CN201710735556.9A Withdrawn CN107501940A (zh) | 2015-07-06 | 2015-07-06 | 聚丙烯用有机硅阻燃剂及其制备方法 |
Country Status (1)
Country | Link |
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CN (3) | CN107474387A (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105161203A (zh) * | 2015-09-28 | 2015-12-16 | 张翔 | 一种耐高温阻燃电缆及其制作方法 |
CN107553624A (zh) * | 2017-09-09 | 2018-01-09 | 王莉 | 一种阻燃竹地板的加工方法 |
CN111378215A (zh) * | 2020-04-29 | 2020-07-07 | 嘉兴学院 | 一种无卤阻燃剂及其制备方法 |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101235175A (zh) * | 2008-01-14 | 2008-08-06 | 宁波永发新材料发展有限公司 | 一种阻燃性聚丙烯复合材料及其制备方法 |
CN101293983A (zh) * | 2007-04-28 | 2008-10-29 | 中国石油化工股份有限公司 | 一种膨胀阻燃聚丙烯组合物及其制备方法 |
CN102286171A (zh) * | 2011-06-21 | 2011-12-21 | 公安部四川消防研究所 | 吹塑型无卤阻燃聚丙烯材料 |
CN102558674A (zh) * | 2011-12-19 | 2012-07-11 | 金发科技股份有限公司 | 一种具有高灼热丝引燃温度的阻燃聚丙烯组合物 |
CN102816405A (zh) * | 2012-08-30 | 2012-12-12 | 宁波聚泰新材料科技有限公司 | 一种低烟无卤阻燃热塑性弹性体及其制备方法 |
CN103319748A (zh) * | 2013-06-03 | 2013-09-25 | 公安部四川消防研究所 | 磷氮复合型阻燃剂及其制备方法 |
CN103626796A (zh) * | 2012-08-28 | 2014-03-12 | 杨晓林 | 一种硅橡胶的回收方法 |
CN103665870A (zh) * | 2013-11-09 | 2014-03-26 | 国家电网公司 | 一种废弃复合绝缘子硅橡胶材料的回收再利用方法 |
CN104130505A (zh) * | 2014-08-15 | 2014-11-05 | 广州市海弘塑料科技有限公司 | 一种无卤阻燃交联聚丙烯及其制备方法与应用 |
CN105038241A (zh) * | 2015-07-03 | 2015-11-11 | 东至绿洲环保化工有限公司 | 一种回收有机硅橡胶废料再加工的有机硅阻燃剂及其制备方法 |
-
2015
- 2015-07-06 CN CN201710735537.6A patent/CN107474387A/zh not_active Withdrawn
- 2015-07-06 CN CN201710735556.9A patent/CN107501940A/zh not_active Withdrawn
- 2015-07-06 CN CN201510392553.0A patent/CN104893299B/zh active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101293983A (zh) * | 2007-04-28 | 2008-10-29 | 中国石油化工股份有限公司 | 一种膨胀阻燃聚丙烯组合物及其制备方法 |
CN101235175A (zh) * | 2008-01-14 | 2008-08-06 | 宁波永发新材料发展有限公司 | 一种阻燃性聚丙烯复合材料及其制备方法 |
CN102286171A (zh) * | 2011-06-21 | 2011-12-21 | 公安部四川消防研究所 | 吹塑型无卤阻燃聚丙烯材料 |
CN102558674A (zh) * | 2011-12-19 | 2012-07-11 | 金发科技股份有限公司 | 一种具有高灼热丝引燃温度的阻燃聚丙烯组合物 |
CN103626796A (zh) * | 2012-08-28 | 2014-03-12 | 杨晓林 | 一种硅橡胶的回收方法 |
CN102816405A (zh) * | 2012-08-30 | 2012-12-12 | 宁波聚泰新材料科技有限公司 | 一种低烟无卤阻燃热塑性弹性体及其制备方法 |
CN103319748A (zh) * | 2013-06-03 | 2013-09-25 | 公安部四川消防研究所 | 磷氮复合型阻燃剂及其制备方法 |
CN103665870A (zh) * | 2013-11-09 | 2014-03-26 | 国家电网公司 | 一种废弃复合绝缘子硅橡胶材料的回收再利用方法 |
CN104130505A (zh) * | 2014-08-15 | 2014-11-05 | 广州市海弘塑料科技有限公司 | 一种无卤阻燃交联聚丙烯及其制备方法与应用 |
CN105038241A (zh) * | 2015-07-03 | 2015-11-11 | 东至绿洲环保化工有限公司 | 一种回收有机硅橡胶废料再加工的有机硅阻燃剂及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN107501940A (zh) | 2017-12-22 |
CN107474387A (zh) | 2017-12-15 |
CN104893299A (zh) | 2015-09-09 |
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