CN104875442A - High thermal-insulation energy-saving explosion-proof membrane - Google Patents
High thermal-insulation energy-saving explosion-proof membrane Download PDFInfo
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- CN104875442A CN104875442A CN201510232389.7A CN201510232389A CN104875442A CN 104875442 A CN104875442 A CN 104875442A CN 201510232389 A CN201510232389 A CN 201510232389A CN 104875442 A CN104875442 A CN 104875442A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
- B32B15/04—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B15/08—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
- B32B15/09—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin comprising polyesters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
- B32B15/04—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B15/043—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/12—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
- B32B37/1284—Application of adhesive
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
- B32B7/04—Interconnection of layers
- B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/14—Metallic material, boron or silicon
- C23C14/20—Metallic material, boron or silicon on organic substrates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/35—Sputtering by application of a magnetic field, e.g. magnetron sputtering
- C23C14/352—Sputtering by application of a magnetic field, e.g. magnetron sputtering using more than one target
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2250/00—Layers arrangement
- B32B2250/04—4 layers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/304—Insulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/40—Properties of the layers or laminate having particular optical properties
- B32B2307/416—Reflective
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/714—Inert, i.e. inert to chemical degradation, corrosion
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2311/00—Metals, their alloys or their compounds
- B32B2311/02—Noble metals
- B32B2311/08—Silver
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2311/00—Metals, their alloys or their compounds
- B32B2311/24—Aluminium
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Laminated Bodies (AREA)
- Physical Vapour Deposition (AREA)
Abstract
The invention discloses a high thermal-insulation energy-saving explosion-proof membrane. The explosion-proof membrane comprises a thermal-stability polyester film layer, a first metal indium layer is formed on one surface of the thermal-stability polyester film layer in a magnetron sputtering manner; a polyester film with the thickness of 40 microns is prepared, the polyester film is a thermal-stability polyester film; the first metal indium layer as anti-oxidation protection is deposited on the thermal-stability polyester film in the magnetron sputtering manner, the working pressure is set as 0.7Pa, the target distance is fixed at 75mm, the flow of the argon is 22sccm, the sputtering power of the indium is 40W, the sputtering rate is respectively 4.0nm/min, and the thickness of the first metal indium layer is 5nm. The explosion-proof membrane disclosed by the invention is in favor of reflecting and obstructing infrared ray in solar ray, the thermal-insulation effect is obvious, and the magnetron sputtered metal layer can be well protected, the metal oxidation is prevented, the product performance and the service life are improved and guaranteed, so that the explosion-proof membrane is suitable for occasions with higher requirement.
Description
Technical field
The present invention relates to a kind of energy-saving explosion-proof film, belong to adhesive material technical field.
Background technology
The glass that the glass that current building and general place use and body of a motor car use is all generally simple glass, although simple glass has good transmittance, be convenient to observe extraneous circumstance and be convenient to driver and observe passenger in road traffic condition and car and observe situation outside car, on the one hand, the sunshine but outside glass and other light often affect eyes and the vision of glass inner face personnel and driver; On the other hand, sunlight outside glass can shine hot glass inner face and automotive interior through glass, glass inner face and automotive interior temperature are increased, when more seriously causing glass breaking when meeting accident, broken glass disperses and can injure periphery personnel, therefore, often the door curtain made of cloth is installed after glass He in automobile, to keep the sun off with heat insulation, then adopt the method for pasting plastic sheeting at present, but those skilled in the art fail to give enough attention in heat-proof quality.Therefore, how improving heat-insulating efficiency, can ensure again the transmitance of very high visible ray, is the direction that those skilled in the art make great efforts to reach not only energy-conservation but also high transparency.Meanwhile, producing the high heat insulation rupture pressure disc of high transparency at flexible parent metal (plastic sheeting) magnetron sputtering is also the direction that those skilled in the art make great efforts.
Summary of the invention
The object of the invention is to provide a kind of high heat-insulating and energy-saving rupture pressure disc, this high heat-insulating and energy-saving rupture pressure disc had both been conducive to the infrared ray in reflection and obstruct sunray, effect of heat insulation is remarkable, magnetron sputtering metal level can better be protected again, prevent burning, improve and ensure that the performance and used life of product, thus be applicable to the higher place of requirement; The present invention provides the preparation technology of the saturating high heat-insulating and energy-saving rupture pressure disc of above-mentioned height simultaneously.
For achieving the above object, the technical solution used in the present invention is: a kind of high heat-insulating and energy-saving rupture pressure disc, comprise a heat endurance laminated polyester film, this heat endurance laminated polyester film one surface magnetic control sputtering has the first metal indium layer, this another surface magnetic control sputtering of the first metal indium layer has metallic silver layer as thermal insulation layer or metallic aluminum, and this metallic silver layer or another surface magnetic control sputtering of metallic aluminum have the second metal indium layer; Described first indium metal layer thickness is 5nm, and described metallic silver layer or metallic aluminum thickness are 20nm, described second metal indium layer 8nm;
Described high heat-insulating and energy-saving rupture pressure disc is obtained by following technique:
Step one, prepare a polyester film, thickness is 40 μm, and described polyester film is heat endurance polyester film;
Step 2, on the heat endurance polyester film of step one magnetron sputtering deposition as the first metal indium layer of protection against oxidation; process conditions are: employing purity is the target of the indium of 99.99%; sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75 mm, and the flow of argon gas is 22sccm, and the sputtering power of indium is 40 W, and sputter rate is 4.0nm/min respectively, and the first indium metal layer thickness is 5nm;
Step 3, deposit a thermal insulation layer at first another surface magnetic control sputtering of metal indium layer, this thermal insulation layer metallic silver layer, process conditions are: purity is the target of 99.99% silver medal, and sputter gas is 99.999% high-purity argon gas, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and silver-colored target as sputter power is 40W, and sputter rate is 6.4 nm/min, and described insulation thickness is 20nm;
Step 4, then deposit the second metal indium layer at another surface magnetic control sputtering of thermal insulation layer of step 3, process conditions are: indium target purity is 99.99%, and sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6. 1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and the sputtering power of indium is all 40 W, and sputter rate is 4.0nm/min respectively, and described second indium metal layer thickness is 8nm; In described step 4 before the second metal indium layer sputtering, first indium target is carried out to the pre-sputtering of 5min, to remove oxide and the pollutant of target remained on surface.
In technique scheme, further improved plan is as follows:
1, in such scheme, before described heat endurance laminated polyester film magnetron sputtering, at 150 ~ 160 DEG C, preheating shrink process is carried out.
2, in such scheme, between described heat endurance laminated polyester film and the first metal indium layer, acrylic emulsion layer is coated with.
3, in such scheme, described heat endurance polyester film layer thickness is 15 ~ 70 μm.
4, in such scheme, described thermal insulation layer is metallic aluminum, and this metallic aluminum thickness is 20 ~ 50nm.
Because technique scheme is used, the present invention compared with prior art has following advantages and effect:
1, height heat-insulating and energy-saving rupture pressure disc of the present invention, its substrate layer one surface magnetic control sputtering has the first metal indium layer, this another surface magnetic control sputtering of metal indium layer has metallic silver layer as thermal insulation layer or metallic aluminum, this metallic silver layer or another surface magnetic control sputtering of metallic aluminum have the second metal indium layer, described first indium metal layer thickness is 2 ~ 15nm, described metallic silver layer or metallic aluminum thickness are 8 ~ 55nm, described second metal indium layer 5 ~ 20nm, both the infrared ray that magnetron sputtering metal level can be reflected and be intercepted in sunray had been conducive to, effect of heat insulation is remarkable, magnetron sputtering metal level can better be protected again, prevent burning, improve and ensure that the performance and used life of product, thus be applicable to the higher place of requirement.
2, height heat-insulating and energy-saving rupture pressure disc of the present invention, its plastic-based film carries out preheating shrink process at 150 ~ 160 DEG C, improve the molecularly oriented of plastic-based film, meanwhile, improve plastic-based film degree of crystallinity and improve lattice structure, thus improve plastic-based film heat endurance, concrete data, the thermal contraction of common plastics basement membrane is generally 1 ~ 3%, avoid plastic-based film thermal contraction and distortion when magnetron sputtering, substantially increases product.
3, height heat-insulating and energy-saving rupture pressure disc of the present invention, acrylic emulsion layer is coated with between its plastic-based film and the first metal indium layer, the metal level of plastic-based film and magnetron sputtering has better adhesive force, and product has higher visible light transmissivity, concrete data are as follows: the visible light transmissivity 88 ~ 90% of common plastics basement membrane, but the present invention, can reach 92 ~ 95%; Especially, between the first metal indium layer, be coated with acrylic emulsion layer again carry out preheating shrink process at 150 ~ 160 DEG C before substrate layer magnetron sputtering after, while improving light transmittance, also improve the adhesive force of the metal indium layer of PET film and magnetron sputtering; The present invention is preferred metal indium layer and insulation thickness, both achieved anticorrosion ability, in turn ensure that the transmitance of effect of heat insulation and visible ray.
Accompanying drawing explanation
Accompanying drawing 1 is height heat-insulating and energy-saving rupture pressure disc structural representation one of the present invention;
Accompanying drawing 2 is height heat-insulating and energy-saving rupture pressure disc structural representation two of the present invention.
In above accompanying drawing: 1, substrate layer; 2, the first metal indium layer; 31, metallic silver layer; 32, metallic aluminum; 4, the second metal indium layer.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1: a kind of high heat-insulating and energy-saving rupture pressure disc, comprise a heat endurance laminated polyester film 1, this heat endurance laminated polyester film 1 one surface magnetic control sputtering has the first metal indium layer 2, this another surface magnetic control sputtering of the first metal indium layer 2 has metallic silver layer 31 as thermal insulation layer or metallic aluminum 32, and this metallic silver layer 31 or another surface magnetic control sputtering of metallic aluminum 32 have the second metal indium layer 4; Described first indium metal layer thickness is 5nm, and described metallic silver layer or metallic aluminum thickness are 20nm, described second metal indium layer 8nm;
Described high heat-insulating and energy-saving rupture pressure disc is obtained by following technique:
Step one, prepare a polyester film, thickness is 40 μm, and described polyester film is heat endurance polyester film;
Step 2, on the heat endurance polyester film of step one magnetron sputtering deposition as the first metal indium layer of protection against oxidation; process conditions are: employing purity is the target of the indium In of 99.99%; sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75 mm, and the flow of argon gas is 22sccm, and the sputtering power of indium In is 40 W, and sputter rate is 4.0nm/min respectively, and the first indium metal layer thickness is 5nm;
Step 3, deposit a thermal insulation layer at first another surface magnetic control sputtering of metal indium layer, this thermal insulation layer metallic silver layer, process conditions are: purity is the target of 99.99% silver medal, and sputter gas is 99.999% high-purity argon gas, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and silver-colored target as sputter power is 40W, and sputter rate is 6.4 nm/min, and described insulation thickness is 20nm;
Step 4, then deposit the second metal indium layer at another surface magnetic control sputtering of thermal insulation layer of step 3, process conditions are: indium target purity is 99.99%, and sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6. 1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and the sputtering power of indium is all 40 W, and sputter rate is 4.0nm/min respectively, and described second indium metal layer thickness is 8nm; In described step 4 before the second metal indium layer sputtering, first indium target is carried out to the pre-sputtering of 5min, to remove oxide and the pollutant of target remained on surface.
At 150 ~ 160 DEG C, preheating shrink process is carried out before above-mentioned heat endurance laminated polyester film magnetron sputtering.Described heat endurance polyester film layer thickness is 15 ~ 70 μm.
Embodiment 2: a kind of high heat-insulating and energy-saving rupture pressure disc, comprise a heat endurance laminated polyester film 1, this heat endurance laminated polyester film 1 one surface magnetic control sputtering has the first metal indium layer 2, this another surface magnetic control sputtering of the first metal indium layer 2 has metallic silver layer 31 as thermal insulation layer or metallic aluminum 32, and this metallic silver layer 31 or another surface magnetic control sputtering of metallic aluminum 32 have the second metal indium layer 4; Described first indium metal layer thickness is 5nm, and described metallic silver layer or metallic aluminum thickness are 20nm, described second metal indium layer 8nm;
Described high heat-insulating and energy-saving rupture pressure disc is obtained by following technique:
Step one, prepare a polyester film, thickness is 40 μm, and described polyester film is heat endurance polyester film;
Step 2, on the heat endurance polyester film of step one magnetron sputtering deposition as the first metal indium layer of protection against oxidation; process conditions are: employing purity is the target of the indium In of 99.99%; sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75 mm, and the flow of argon gas is 22sccm, and the sputtering power of indium In is 40 W, and sputter rate is 4.0nm/min respectively, and the first indium metal layer thickness is 5nm;
Step 3, deposit a thermal insulation layer at first another surface magnetic control sputtering of metal indium layer, this thermal insulation layer metallic silver layer, process conditions are: purity is the target of 99.99% silver medal, and sputter gas is 99.999% high-purity argon gas, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and silver-colored target as sputter power is 40W, and sputter rate is 6.4 nm/min, and described insulation thickness is 20nm;
Step 4, then deposit the second metal indium layer at another surface magnetic control sputtering of thermal insulation layer of step 3, process conditions are: indium target purity is 99.99%, and sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6. 1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and the sputtering power of indium is all 40 W, and sputter rate is 4.0nm/min respectively, and described second indium metal layer thickness is 8nm; In described step 4 before the second metal indium layer sputtering, first indium target is carried out to the pre-sputtering of 5min, to remove oxide and the pollutant of target remained on surface.
At 150 ~ 160 DEG C, preheating shrink process is carried out before above-mentioned heat endurance laminated polyester film magnetron sputtering.
Acrylic emulsion layer is coated with between above-mentioned heat endurance laminated polyester film and the first metal indium layer.
Above-described embodiment, only for technical conceive of the present invention and feature are described, its object is to person skilled in the art can be understood content of the present invention and implement according to this, can not limit the scope of the invention with this.All equivalences done according to Spirit Essence of the present invention change or modify, and all should be encompassed within protection scope of the present invention.
Claims (4)
1. one kind high heat-insulating and energy-saving rupture pressure disc, it is characterized in that: comprise a heat endurance laminated polyester film (1), this heat endurance laminated polyester film (1) one surface magnetic control sputtering has the first metal indium layer (2), this the first metal indium layer (2) another surface magnetic control sputtering has metallic silver layer (31) as thermal insulation layer or metallic aluminum (32), and this metallic silver layer (31) or metallic aluminum (32) another surface magnetic control sputtering have the second metal indium layer (4); Described first indium metal layer thickness is 5nm, and described metallic silver layer or metallic aluminum thickness are 20nm, described second metal indium layer 8nm;
Described high heat-insulating and energy-saving rupture pressure disc is obtained by following technique:
Step one, prepare a polyester film, thickness is 40 μm, and described polyester film is heat endurance polyester film;
Step 2, on the heat endurance polyester film of step one magnetron sputtering deposition as the first metal indium layer of protection against oxidation; process conditions are: employing purity is the target of the indium (In) of 99.99%; sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75 mm, and the flow of argon gas is 22sccm, and the sputtering power of indium (In) is 40 W, and sputter rate is 4.0nm/min respectively, and the first indium metal layer thickness is 5nm;
Step 3, deposit a thermal insulation layer at first another surface magnetic control sputtering of metal indium layer, this thermal insulation layer metallic silver layer, process conditions are: purity is the target of 99.99% silver medal, and sputter gas is 99.999% high-purity argon gas, and the vacuum of inside cavity is 6.1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and silver-colored target as sputter power is 40W, and sputter rate is 6.4 nm/min, and described insulation thickness is 20nm;
Step 4, then deposit the second metal indium layer at another surface magnetic control sputtering of thermal insulation layer of step 3, process conditions are: indium target purity is 99.99%, and sputter gas is the high-purity argon gas of 99.999%, and the vacuum of inside cavity is 6. 1 × 10
-4pa, operating pressure is set to 0.7 Pa, and target distance is fixed on 75mm, and the flow of argon gas is 22sccm, and the sputtering power of indium is all 40 W, and sputter rate is 4.0nm/min respectively, and described second indium metal layer thickness is 8nm; In described step 4 before the second metal indium layer sputtering, first indium target is carried out to the pre-sputtering of 5min, to remove oxide and the pollutant of target remained on surface.
2. the saturating high heat-insulating and energy-saving rupture pressure disc of height according to claim 1, is characterized in that: at 150 ~ 160 DEG C, carry out preheating shrink process before described heat endurance laminated polyester film magnetron sputtering.
3. the saturating high heat-insulating and energy-saving rupture pressure disc of height according to claim 1, is characterized in that: be coated with acrylic emulsion layer between described heat endurance laminated polyester film and the first metal indium layer.
4. the saturating high heat-insulating and energy-saving rupture pressure disc of height according to claim 1, is characterized in that: described heat endurance polyester film layer thickness is 15 ~ 70 μm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510232389.7A CN104875442B (en) | 2012-12-18 | 2012-12-18 | High thermal-insulation energy-saving explosion-proof membrane |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510232389.7A CN104875442B (en) | 2012-12-18 | 2012-12-18 | High thermal-insulation energy-saving explosion-proof membrane |
| CN201210549980.1A CN103057211B (en) | 2012-12-18 | 2012-12-18 | Preparation technology of energy-saving explosion-proof film with high transmittance and obtained explosion-proof film |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210549980.1A Division CN103057211B (en) | 2012-12-18 | 2012-12-18 | Preparation technology of energy-saving explosion-proof film with high transmittance and obtained explosion-proof film |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104875442A true CN104875442A (en) | 2015-09-02 |
| CN104875442B CN104875442B (en) | 2017-04-19 |
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Family Applications (6)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510230304.1A Active CN104859224B (en) | 2012-12-18 | 2012-12-18 | Energy-saving explosion-proof film for building glass |
| CN201510226551.4A Active CN104890318B (en) | 2012-12-18 | 2012-12-18 | Constructional energy saving explosion-proof pasting pad |
| CN201510226760.9A Active CN104890319B (en) | 2012-12-18 | 2012-12-18 | Explosion-proof membrane |
| CN201210549980.1A Active CN103057211B (en) | 2012-12-18 | 2012-12-18 | Preparation technology of energy-saving explosion-proof film with high transmittance and obtained explosion-proof film |
| CN201510232389.7A Active CN104875442B (en) | 2012-12-18 | 2012-12-18 | High thermal-insulation energy-saving explosion-proof membrane |
| CN201510226311.4A Active CN104908559B (en) | 2012-12-18 | 2012-12-18 | High-transparency explosion-proof adhesive membrane for automobile glass |
Family Applications Before (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510230304.1A Active CN104859224B (en) | 2012-12-18 | 2012-12-18 | Energy-saving explosion-proof film for building glass |
| CN201510226551.4A Active CN104890318B (en) | 2012-12-18 | 2012-12-18 | Constructional energy saving explosion-proof pasting pad |
| CN201510226760.9A Active CN104890319B (en) | 2012-12-18 | 2012-12-18 | Explosion-proof membrane |
| CN201210549980.1A Active CN103057211B (en) | 2012-12-18 | 2012-12-18 | Preparation technology of energy-saving explosion-proof film with high transmittance and obtained explosion-proof film |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201510226311.4A Active CN104908559B (en) | 2012-12-18 | 2012-12-18 | High-transparency explosion-proof adhesive membrane for automobile glass |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108129686A (en) * | 2017-12-20 | 2018-06-08 | 江苏斯瑞达新材料科技有限公司 | The preparation method of high temperature resistant heat insulation energy-saving explosion-proof film |
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| CN104859224B (en) * | 2012-12-18 | 2017-03-08 | 苏州斯迪克新材料科技股份有限公司 | Energy-saving explosion-proof film for building glass |
| CN105369206A (en) * | 2015-12-03 | 2016-03-02 | 凯盛光伏材料有限公司 | Magnetron sputtering device for preparing flexible liner membrane |
| JP2021074978A (en) * | 2019-11-11 | 2021-05-20 | 尾池工業株式会社 | Layered film, metallic tone product, and metallic signage |
| CN113136556A (en) * | 2021-03-12 | 2021-07-20 | 先导薄膜材料（广东）有限公司 | Preparation method of indium film for acousto-optic modulator |
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Also Published As
| Publication number | Publication date |
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| CN104890318B (en) | 2017-04-19 |
| CN104859224B (en) | 2017-03-08 |
| CN104859224A (en) | 2015-08-26 |
| CN104908559B (en) | 2017-04-19 |
| CN104890319A (en) | 2015-09-09 |
| CN103057211B (en) | 2015-06-10 |
| CN104890318A (en) | 2015-09-09 |
| CN104890319B (en) | 2017-04-19 |
| CN104875442B (en) | 2017-04-19 |
| CN103057211A (en) | 2013-04-24 |
| CN104908559A (en) | 2015-09-16 |
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Address after: 223900 Sihong Province Economic Development Zone, Suqian, West Ocean West Road, No. 6 Applicant after: Jiangsu Stick new materials Polytron Technologies Inc Address before: 215400 Taicang, Suzhou, Taicang Economic Development Zone, Qingdao West Road, No. 11, No. Applicant before: Suzhou Sidike New Material Science & Technology Co., Ltd. |
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