CN103350534B - A kind of nano-angle color-changing solar can control film and preparation method thereof - Google Patents
A kind of nano-angle color-changing solar can control film and preparation method thereof Download PDFInfo
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- CN103350534B CN103350534B CN201310164404.XA CN201310164404A CN103350534B CN 103350534 B CN103350534 B CN 103350534B CN 201310164404 A CN201310164404 A CN 201310164404A CN 103350534 B CN103350534 B CN 103350534B
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- sulfide
- angle color
- changing solar
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- 238000002360 preparation method Methods 0.000 title claims description 10
- 239000002052 molecular layer Substances 0.000 claims abstract description 36
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000000758 substrate Substances 0.000 claims abstract description 24
- 239000011521 glass Substances 0.000 claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 239000005083 Zinc sulfide Substances 0.000 claims description 5
- 229910052984 zinc sulfide Inorganic materials 0.000 claims description 5
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 5
- 229920002799 BoPET Polymers 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 3
- 238000002834 transmittance Methods 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 8
- 238000009413 insulation Methods 0.000 abstract description 8
- 239000012528 membrane Substances 0.000 abstract description 2
- 239000010408 film Substances 0.000 description 21
- 239000010409 thin film Substances 0.000 description 12
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium dioxide Chemical compound O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 description 4
- JPJALAQPGMAKDF-UHFFFAOYSA-N selenium dioxide Chemical compound O=[Se]=O JPJALAQPGMAKDF-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 3
- WUPHOULIZUERAE-UHFFFAOYSA-N 3-(oxolan-2-yl)propanoic acid Chemical compound OC(=O)CCC1CCCO1 WUPHOULIZUERAE-UHFFFAOYSA-N 0.000 description 2
- 230000006750 UV protection Effects 0.000 description 2
- CUGMJFZCCDSABL-UHFFFAOYSA-N arsenic(3+);trisulfide Chemical compound [S-2].[S-2].[S-2].[As+3].[As+3] CUGMJFZCCDSABL-UHFFFAOYSA-N 0.000 description 2
- CJDPJFRMHVXWPT-UHFFFAOYSA-N barium sulfide Chemical compound [S-2].[Ba+2] CJDPJFRMHVXWPT-UHFFFAOYSA-N 0.000 description 2
- 229910052980 cadmium sulfide Inorganic materials 0.000 description 2
- JGIATAMCQXIDNZ-UHFFFAOYSA-N calcium sulfide Chemical compound [Ca]=S JGIATAMCQXIDNZ-UHFFFAOYSA-N 0.000 description 2
- NNLOHLDVJGPUFR-UHFFFAOYSA-L calcium;3,4,5,6-tetrahydroxy-2-oxohexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(=O)C([O-])=O.OCC(O)C(O)C(O)C(=O)C([O-])=O NNLOHLDVJGPUFR-UHFFFAOYSA-L 0.000 description 2
- 229940119177 germanium dioxide Drugs 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 229910000464 lead oxide Inorganic materials 0.000 description 2
- 238000001755 magnetron sputter deposition Methods 0.000 description 2
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 229910052979 sodium sulfide Inorganic materials 0.000 description 2
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 2
- YPMOSINXXHVZIL-UHFFFAOYSA-N sulfanylideneantimony Chemical compound [Sb]=S YPMOSINXXHVZIL-UHFFFAOYSA-N 0.000 description 2
- CADICXFYUNYKGD-UHFFFAOYSA-N sulfanylidenemanganese Chemical compound [Mn]=S CADICXFYUNYKGD-UHFFFAOYSA-N 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- ALRFTTOJSPMYSY-UHFFFAOYSA-N tin disulfide Chemical compound S=[Sn]=S ALRFTTOJSPMYSY-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Abstract
A kind of nano-angle color-changing solar provided by the invention can control film, and including substrate (1) and the photochromic layer (2) be located in substrate (1), described nanochromics layer (2) is staggered is formed by sulfide nanometer layer (3) and oxidate nano layer (4)。It is simple, with low cost that this nano-angle color-changing solar can control membrane structure, and good heat-insulation effect, light transmittance are high, can be widely applied to the rupture pressure disc of automobile and building field and implosion guard, have huge application prospect。
Description
Technical field
The invention belongs to energy-conserving product field, film can be controlled particularly to a kind of nano-angle color-changing solar, the preparation method further relating to this thin film。
Background technology
The energy-conservation important topic having become people's concern with environmental conservation。Owing to simple glass is inadequate to ultrared isolation, hence in so that the glass door etc. of the large area window of skyscraper, motor-vehicle glass window and refrigerator-freezer needs to completely cut off the huge energy loss brought in thermal-radiating place, even cause environmental pollution。
For solving the transparent heat-insulated problem in the place such as building, vehicle glass, conduct extensive research both at home and abroad and attempt, invent multiple thermal insulation film, common in the market mainly have the product such as metal coating heat-reflecting glass and various heat reflection pad pastings, and these products are for increasing to ultrared reflection, isolate radiant heat, yet with these films in use, the light transmittance of visible ray is not high yet, have impact on daylighting and visibility, even has influence on personal safety。Also have and adopt the metallic film including the layers such as titanium oxide, there is the light transmittance of higher visible ray, however relatively costly, it is difficult to promote on a large scale。
Summary of the invention
Goal of the invention: the nano-angle color-changing solar that the first object of the present invention is to provide a kind of good heat-insulation effect, light transmittance is good can control film。
The preparation method that the second object of the present invention is to provide above-mentioned thin film。
Technical scheme: a kind of nano-angle color-changing solar provided by the invention can control film, including substrate (1) and the photochromic layer (2) be located in substrate (1), described nanochromics layer (2) is staggered is formed by sulfide nanometer layer (3) and oxidate nano layer (4)。
As preferably, described substrate (1) is PET film, plastics or glass。
Preferred as another kind, the thickness of described sulfide nanometer layer (3) is 2～500nm。
Preferred as another kind, described sulfide nanometer layer (3) is zinc sulfide nano layer, sodium sulfide nanometer layer, calcium sulfide nanometer layer, barium sulfide nanometer layer, manganese sulfide nano layer, cadmium sulfide nano layer, arsenic sulfide nanometer layer, Tin disulfide nanometer layer, antimony sulfide nano layer, bismuth sulfide nano layer。
Preferred as another kind, the thickness of described oxidate nano layer (4) is 2～500nm。
Preferred as another kind, described nano oxide layer (4) is silica nanometer layer, germanium dioxide nanometer layer, selenium dioxide nanometer layer, Lead oxide brown nanometer layer。,
Present invention also offers the preparation method that above-mentioned nano-angle color-changing solar can control film, comprise the following steps: comprise the following steps: interlocking at substrate surface sputters sulfide nanometer layer and oxidate nano layer and get final product。
Beneficial effect: it is simple, with low cost that nano-angle color-changing solar provided by the invention can control membrane structure, good heat-insulation effect, light transmittance are high, can be widely applied to the rupture pressure disc of automobile and building field and implosion guard, have huge application prospect。
Specifically, nano-angle color-changing solar provided by the invention can control film relative to prior art, has advantage highlighted below:
First, good heat-insulation effect, light transmittance are high。This thin film is by being crisscross arranged sulfurized layer and oxide skin(coating), utilize sulfide and the oxide intrinsic refractive index to light, by the superposition of sulfurized layer and oxide skin(coating), incident illumination is carried out superposition repeatedly to reflect, refraction light is utilized to carry out the multipath interference of light, thus greatly reducing infrared ray and ultraviolet radiation, and then substantially increase effect of heat insulation；Simultaneously, sulfide and oxide self possess transparent character, it is ensured that the light transmittance of this thin film, and thin film of the present invention has the light transmittance every infrared capable, 60～95% every UV resistance, 65～90% of 60～80%, good heat-insulation effect, light transmittance are high, meet the policy of energy-saving and emission-reduction。
Second, with low cost。This thin film adopts nanometer sulfide and nano-oxide as stratiform coating, and raw material sources are extensive, with low cost。
3rd, this thin film has good privacy。Incident illumination is carried out superposition repeatedly by the superposition of sulfurized layer and oxide skin(coating) and reflects by this thin film, refraction light is utilized to carry out the multipath interference of light, thus being formed under the observation of different visual angles, make the former film of original transparent PET or conventional clear glass has different color effects, so that thin film has good privacy。
4th, it is widely used。This thin film can be widely applied to rupture pressure disc and the implosion guard of automobile and building field, has huge application prospect。
Accompanying drawing explanation
Fig. 1 is the structural representation that the nano-angle color-changing solar of the embodiment of the present invention 1 can control film。
Detailed description of the invention
According to following embodiment, it is possible to be more fully understood that the present invention。But, as it will be easily appreciated by one skilled in the art that the concrete material proportion described by embodiment, process conditions and result thereof are merely to illustrate the present invention, and should without the present invention described in detail in restriction claims。
Embodiment 1
Nano-angle color-changing solar can control film, sees Fig. 1, and including substrate 1 and the nanochromics layer 2 being located in substrate 1, nanochromics layer 2 is staggered is formed by sulfide nanometer layer 3 and oxidate nano layer 4, and nanochromics layer 2 includes 12 layers。The thickness of sulfide nanometer layer 3 respectively 100nm, 70nm, 50nm, 200nm, 300nm, 60nm；The thickness of oxidate nano layer 4 respectively 200nm, 80nm, 120nm, 200nm, 300nm, 120nm。
Substrate 1 is PET film；Sulfide nanometer layer 3 is zinc sulfide nano layer；Oxidate nano layer 4 is silica nanometer layer。
Its preparation method, comprises the following steps: the first zinc sulfide nano layer of magnetron sputtering 100nm in the PET film of substrate 1, then on the zinc sulfide nano layer of 100nm the silica nanometer layer of magnetron sputtering 200nm；By that analogy, staggered sputtering sulfide nanometer layer 3 and the oxidate nano layer 4 and get final product on substrate 1 surface。
Embodiment 2
Nano-angle color-changing solar can control film, and including substrate 1 and the nanochromics layer 2 being located in substrate 1, nanochromics layer 2 is staggered is formed by sulfide nanometer layer 3 and oxidate nano layer 4, and nanochromics layer 2 includes 15 layers。The thickness of sulfide nanometer layer 3 respectively 100nm, 70nm, 50nm, 200nm, 300nm, 60nm, 150nm, 500nm；The thickness of oxidate nano layer 4 is 200nm, 80nm, 120nm, 200nm, 300nm, 120nm, 500nm。
Substrate 1 is plastics；Sulfide nanometer layer 3 is sodium sulfide nanometer layer；Oxidate nano layer 4 is germanium dioxide nanometer layer。
Its preparation method is with embodiment 1。
Embodiment 3
Nano-angle color-changing solar can control film, and including substrate 1 and the photochromic layer 2 being located in substrate 1, nanochromics layer 2 is staggered is formed by sulfide nanometer layer 3 and oxidate nano layer 4, and nanochromics layer 2 includes 20 layers。The thickness of sulfide nanometer layer 3 respectively 100nm, 50nm, 20nm, 250nm, 350nm, 200nm, 300nm, 60nm, 150nm, 500nm；The thickness of oxidate nano layer 4 is 150nm, 200nm, 80nm, 250nm, 350nm, 120nm, 200nm, 300nm, 120nm, 500nm。
Substrate 1 is glass；Sulfide nanometer layer 3 is calcium sulfide nanometer layer；Oxidate nano layer 4 is stannic oxide nanometer layer。
Its preparation method is with embodiment 1。
Embodiment 4
Nano-angle color-changing solar can control film, and including substrate 1 and the photochromic layer 2 being located in substrate 1, nanochromics layer 2 is staggered is formed by sulfide nanometer layer 3 and oxidate nano layer 4, and nanochromics layer 2 includes 600 layers。The thickness of sulfide nanometer layer 3 is between 20-500nm；The thickness of oxidate nano layer 4 is between 20-500nm。
Substrate 1 is glass；Sulfide nanometer layer 3 is barium sulfide nanometer layer；Oxidate nano layer 4 is selenium dioxide nanometer layer。
Its preparation method is with embodiment 1。
Embodiment 5
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: nanochromics layer 2 includes 300 layers；The thickness of sulfide nanometer layer 3 is between 20-500nm；The thickness of oxidate nano layer 4 is between 20-500nm；Sulfide nanometer layer 3 is manganese sulfide nano layer；Oxidate nano layer 4 is Lead oxide brown nanometer layer。
Embodiment 6
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: the thickness of sulfide nanometer layer 3 is between 20-500nm；The thickness of oxidate nano layer 4 is between 20-500nm；Sulfide nanometer layer 3 is cadmium sulfide nano layer。
Embodiment 7
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: sulfide nanometer layer 3 is arsenic sulfide nanometer layer。
Embodiment 8
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: sulfide nanometer layer 3 is Tin disulfide nanometer layer。
Embodiment 9
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: sulfide nanometer layer 3 is antimony sulfide nano layer。
Embodiment 10
Nano-angle color-changing solar can control film, substantially the same manner as Example 1, the difference is that only: sulfide nanometer layer 3 is bismuth sulfide nano layer。
Embodiment 11
The thin film that detection embodiment 1 to embodiment 11 prepares, result is in Table 1。
The light transmittance of the thin film that table 1 embodiment 1 to embodiment 11 prepares and effect of heat insulation table
| Light transmittance (%) | Every UV resistance (%) | Every infrared capable (%) | |
| Embodiment 1 | 80 | 75 | 88 |
| Embodiment 2 | 85 | 78 | 90 |
| Embodiment 3 | 82 | 74 | 85 |
| Embodiment 4 | 81 | 80 | 90 |
| Embodiment 5 | 95 | 80 | 89 |
| Embodiment 6 | 79 | 75 | 86 |
| Embodiment 7 | 86 | 73 | 86 |
| Embodiment 8 | 80 | 78 | 87 |
| Embodiment 9 | 60 | 76 | 83 |
| Embodiment 10 | 85 | 60 | 81 |
| Embodiment 11 | 80 | 77 | 65 |
Claims (3)
1. a nano-angle color-changing solar can control film, it is characterized in that: including substrate (1) and the photochromic layer (2) being located in substrate (1), described nanochromics layer (2) is staggered is formed by sulfide nanometer layer (3) and oxidate nano layer (4)；Described nanochromics layer (2) includes 12 layers, and wherein, sulfide nanometer layer (3) is zinc sulfide nano layer, and thickness is 100nm, 70nm, 50nm, 200nm, 300nm, 60nm respectively；Oxidate nano layer (4) is silica nanometer layer, and thickness is 200nm, 80nm, 120nm, 200nm, 300nm, 120nm respectively。
2. a kind of nano-angle color-changing solar according to claim 1 can control film, it is characterised in that: described substrate (1) is PET film or glass。
3. the preparation method that the nano-angle color-changing solar described in a claim 1 or 2 can control film, it is characterised in that: comprise the following steps: interlocking at substrate surface sputters sulfide nanometer layer and oxidate nano layer and get final product。
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| CN201310164404.XA CN103350534B (en) | 2013-05-06 | 2013-05-06 | A kind of nano-angle color-changing solar can control film and preparation method thereof |
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| CN105227202A (en) * | 2015-09-01 | 2016-01-06 | 信阳师范学院 | A kind of electronic communication equipment based on Internet of Things |
| CN105128473B (en) * | 2015-09-04 | 2017-05-10 | 黑龙江科技大学 | Reflecting luminous film |
| CN106179750A (en) * | 2015-10-27 | 2016-12-07 | 浙江亿东环保科技有限公司 | One pole gold pin anion outdoor PM2.5 purifier |
| CN109111870A (en) * | 2018-06-07 | 2019-01-01 | 苏州袭麟光电科技产业有限公司 | A kind of improved heat-insulated solar control film of height of nano material |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100516145C (en) * | 2000-09-22 | 2009-07-22 | 弗莱克斯产品公司 | Optically variable pigments and foils with enhanced color shifting properties |
| CN101500833A (en) * | 2006-06-09 | 2009-08-05 | 埃克阿泰克有限责任公司 | Polycarbonate glazing system having solar reflecting properties |
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| US20050196623A1 (en) * | 2004-03-03 | 2005-09-08 | Mckown Clem S.Jr. | Solar control coated glass composition |
| US20060141265A1 (en) * | 2004-12-28 | 2006-06-29 | Russo David A | Solar control coated glass composition with reduced haze |
| JP2008151549A (en) * | 2006-12-14 | 2008-07-03 | Seiko Epson Corp | Dial plate for watch and the watch |
| CN203267331U (en) * | 2013-05-06 | 2013-11-06 | 苏州金海薄膜科技发展有限公司 | Nanometer angle discoloring solar control film |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100516145C (en) * | 2000-09-22 | 2009-07-22 | 弗莱克斯产品公司 | Optically variable pigments and foils with enhanced color shifting properties |
| CN101500833A (en) * | 2006-06-09 | 2009-08-05 | 埃克阿泰克有限责任公司 | Polycarbonate glazing system having solar reflecting properties |
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Address after: 215400, 8, Kai Xing Road, old gate area, pontoon bridge, Suzhou, Jiangsu, Taicang Applicant after: SUZHOU XILIN OPTOELECTRONICS TECHNOLOGY INDUSTRY CO., LTD. Address before: 215400, 8, Kai Xing Road, old gate area, pontoon bridge, Suzhou, Jiangsu, Taicang Applicant before: Suzhou Kinghigh Membrane Technology Development Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: SUZHOU KINGHIGH FILM TECHNOLOGY DEVELOPMENT CO., LTD. TO: SUZHOU XILIN OPTOELECTRONIC TECHNOLOGY INDUSTRY CO., LTD. |
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Effective date of registration: 20161101 Address after: 215434, Suzhou, Jiangsu Province, Taicang City Bridge Town, 8 old gate road, 8 Patentee after: Suzhou Xu Ze new Mstar Technology Ltd Address before: 215400, 8, Kai Xing Road, old gate area, pontoon bridge, Suzhou, Jiangsu, Taicang Patentee before: SUZHOU XILIN OPTOELECTRONICS TECHNOLOGY INDUSTRY CO., LTD. |
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