CN104804870A - Liquid essence with outstanding aroma amount and aroma quality and application of liquid essence to cigarettes - Google Patents
Liquid essence with outstanding aroma amount and aroma quality and application of liquid essence to cigarettes Download PDFInfo
- Publication number
- CN104804870A CN104804870A CN201510131226.XA CN201510131226A CN104804870A CN 104804870 A CN104804870 A CN 104804870A CN 201510131226 A CN201510131226 A CN 201510131226A CN 104804870 A CN104804870 A CN 104804870A
- Authority
- CN
- China
- Prior art keywords
- macroporous resin
- tobacco
- liquid
- liquid essence
- resin column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses liquid essence with the outstanding aroma amount and aroma quality. A mixture of various tobaccos is subjected to alcohol extraction and water precipitation, concentrated to be at certain alcoholic strength and then loaded onto a macroporous resin column, the macroporous resin column is eluted with 20% ethyl alcohol, 35-45% ethyl alcohol and 100% ethyl alcohol with volumes three times that of the macroporous resin column sequentially, a 100% ethyl alcohol eluent is collected and concentrated to be at the certain relative density and the certain refractive index, and the liquid essence with the outstanding aroma amount and aroma quality is obtained. The liquid essence is outstanding in aroma amount and aroma quality, can be used as necessary essence for stabilizing the style characteristic of cigarettes and can reduce quality fluctuations caused by the quality of the tobaccos to cigarette products.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, specifically, the present invention relates to a kind of perfume quantity of preparing from tobacco leaf and the outstanding liquid essence of aroma quality.Meanwhile, the invention still further relates to the application of described liquid essence in cigarette.
Background technology
The note impression that cigarette style characteristic brings to people when referring to cigarette smoking, good cigarette product all has oneself relatively unique and stable style and features.Two objective factors affecting cigarette style characteristic the most key are tobacco leaf and essence and flavoring agent.Tobacco leaf, owing to affecting by various extraneous factors such as region, illumination, moisture, temperature, makes the quality of tobacco of different year have larger fluctuation, controls its steady quality relatively difficult.Therefore from essence and flavoring agent angle, exploitation has the essence that style and features highlights, and reducing the change of cigarette style characteristic by quality of tobacco fluctuation, is extremely significant work.
Develop the tobacco flavour spices with specific style feature, and added to this specific style feature of outstanding cigarette in cigarette, be the important directions of tobacco enterprise spices research and development always.But there is the not strong problem of directive property in current research, the tobacco flavour spice product that the result that such research brings is developed often needs just can find suitable application product through a large amount of application tests, even cannot find the cigarette product of its feature applicable, cause the waste of research.
Macroporous resin is the polymkeric substance of a quasi-styrene, can realize the organic selective enrichment of difference according to polarity difference; Macroporous resin has certain pore size simultaneously, also can realize being separated by the volume-exclusion of molecular weight.
The present invention utilizes the selective separation feature of macroporous resin, adopt macroporous resin column in conjunction with solvent selectivity wash-out, the flavor components that specific organoleptic quality is outstanding can be obtained, effective removal, to the irrelevant even disadvantageous tobacco component of screening organoleptic quality, can highlight fragrance cigarette to exploitation and have great importance.
Summary of the invention
The object of the invention is to according to the steady demand of cigarette to style and features, develop the outstanding tobacco extractives of a kind of perfume quantity and aroma quality as liquid tobacco flavour.
This liquid tobacco flavour is the present invention also aims to be applied in cigarette.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, percentage ratio of the present invention is mass percent.
The present invention relates to the liquid essence that a kind of perfume quantity and aroma quality are outstanding, it is by the preparation of the method that comprises the following steps: (1) by the mixture of multiple tobacco leaf with 100% extraction using alcohol, obtain the ethanolic soln containing leaf tobacco extract, in above-mentioned ethanolic soln, add the water of its 1/3 volume and leave standstill 8-12 hour at 0-6 DEG C; Ethanolic soln removing insolubles after filtering and standing, filtrate being concentrated into its alcoholic strength is 10-15%, obtains tobacco just cream liquid;
(2) according to the mass ratio of the first cream liquid of described tobacco and macroporous resin filler 1:5-1:8, first for described tobacco cream liquid is imported the macroporous resin column injection port being filled with macroporous resin, and the liquid take-off rate controlling described macroporous resin column outlet is every 2s-4s mono-;
(3) use macroporous resin column described in the 35-45% ethanol of 20% ethanol of 3 times of described macroporous resin column volumes, 3 times of described macroporous resin column volumes and 100% ethanol elution of 3 times of described macroporous resin column volumes successively, collect the elutriant of 100% ethanol;
(4) elutriant of described 100% ethanol is concentrated into relative density (d
20 20) be 1.170-1.182, refractive index (n
d 20) for 1.446-1.468 time, obtain the liquid essence that described perfume quantity and aroma quality are outstanding.Wherein said relative density refers to the density of material and the density of the reference material ratio under respective defined terms.Described relative density in the present invention refers to 20 DEG C time, the quality of the liquid essence that the described perfume quantity of certain volume and aroma quality are given prominence to and the mass ratio of same volume distilled water.Described refractive index is defined as light velocity of propagation in a vacuum and the ratio in certain Propagation speed, described refractive index in the present invention refers to 20 DEG C time, has the aerial velocity of propagation of light of certain wavelength and the ratio of the velocity of propagation in the liquid essence given prominence in described perfume quantity and aroma quality; Also the light with certain wavelength can be expressed as when injecting flavouring essence for tobacco from air, the ratio of the sine of input angle and the sine at refraction angle.(note: wavelength is defined as (589.3 ± 0.3) nm, is equivalent to the D line in sodium spectrum.)
In preferred embodiments, the mixture of multiple tobacco leaf described in step (1) is the arbitrary combination of in the Argentinian tobacco leaf of Zimbabwe's tobacco leaf of different varieties, the Brazilian tobacco leaf of different varieties or different varieties at least two kinds.Usually, the tobacco leaf of place of production Zimbabwe is called Zimbabwe's tobacco leaf; Be that Brazilian tobacco leaf is called Brazilian tobacco leaf by the place of production; Be that Argentine tobacco leaf is called Argentinian tobacco leaf by the place of production.
In preferred embodiments, described in step (2), macroporous resin filler is non-polar macroporous resin.Preferably, described macroporous resin filler is HPD100 type macroporous resin or AB-8 type macroporous resin.
Second aspect present invention relates to the purposes of the liquid essence described in first aspect present invention as spices.
Third aspect present invention relates to the purposes in cigarette of the liquid essence described in first aspect present invention as tobacco spice.
Fourth aspect present invention relates to a kind of cigarette comprising liquid essence described in first aspect present invention.
Compared with prior art, the present invention has following beneficial effect:
(1) liquid essence of the present invention comes from tobacco leaf, safe and reliable; And it is liquid tobacco flavour, be more conducive to add in cigarette; Flow process is simple, is applicable to large-scale production;
(2) in the present invention, the directive property that is prepared as of liquid essence is separated, and the composition that targetedly enrichment perfume quantity and aroma quality are given prominence to not only reduces the useless technique in preparation process, and also more targeted in subsequent applications;
(3) liquid essence prepared by the present invention is to highlighting cigarette flavor amount and aroma quality, and stable prod quality plays an important role.
(4) in preparation process of the present invention, without the need to using any hazardous solvent, the security of gained liquid essence is improved.
Accompanying drawing explanation
The liquid essence that Fig. 1 is preparation in the embodiment of the present invention 1 adds the network diagramming of score value shared by various odor type style and features when aspirating in cigarette to.
The liquid essence that Fig. 2 is preparation in the embodiment of the present invention 2 adds the network diagramming of score value shared by various odor type style and features when aspirating in cigarette to.
The liquid essence that Fig. 3 is preparation in the embodiment of the present invention 3 adds the network diagramming of score value shared by various odor type style and features when aspirating in cigarette to.
Embodiment
Be described in further details the present invention below in conjunction with embodiment, embodiment is only limitted to the present invention is described, but not limitation of the invention.
Embodiment 1
(1) Zimbabwe's tobacco leaf, Brazilian tobacco leaf and Argentinian tobacco leaf three kinds of tobacco leaf specifications are pressed 1:1:1 mass ratio combine and use the extraction using alcohol of 100%, obtain the ethanolic soln containing leaf tobacco extract, in above-mentioned ethanolic soln, add the water of its 1/3 volume and leave standstill 12 hours at 0 DEG C; Ethanolic soln removing insolubles after filtering and standing, filtrate being concentrated into its alcoholic strength is 10%, obtains tobacco just cream liquid;
(2) according to the mass ratio of the first cream liquid of described tobacco and macroporous resin filler 1:5, first for described tobacco cream liquid is imported the macroporous resin column injection port being filled with macroporous resin, and the liquid take-off rate controlling described macroporous resin column outlet is every 2s mono-;
(3) use macroporous resin column described in 35% ethanol of 20% ethanol of 3 times of described macroporous resin column volumes, 3 times of described macroporous resin column volumes and 100% ethanol elution of 3 times of described macroporous resin column volumes successively, collect the elutriant of 100% ethanol;
(4) elutriant of described 100% ethanol being concentrated into relative density is 1.170, when refractive index is 1.446, obtains the liquid essence that described perfume quantity and aroma quality are outstanding.
Choose a kind of cigarette A not adding any essence and flavoring agent, and to be added in the present embodiment 1 the described perfume quantity of preparation and the outstanding liquid essence of aroma quality wherein according to the adding proportion of its pipe tobacco weight 0.01%, obtain cigarette A1.The cigarette A embodiment as a comparison of any essence and flavoring agent is not added with this.
The Analyses Methods for Sensory Evaluation Results of cigarette A1 and cigarette A is in table 1.
Embodiment 2
(1) Zimbabwe's tobacco leaf, Brazilian tobacco leaf and Argentinian tobacco leaf three kinds of tobacco leaf specifications are pressed 2:1:1 mass ratio combine and use the extraction using alcohol of 100%, obtain the ethanolic soln containing leaf tobacco extract, in above-mentioned ethanolic soln, add the water of its 1/3 volume and leave standstill 8 hours at 2 DEG C; Ethanolic soln removing insolubles after filtering and standing, filtrate being concentrated into its alcoholic strength is 15%, obtains tobacco just cream liquid;
(2) according to the mass ratio of the first cream liquid of described tobacco and macroporous resin filler 1:8, first for described tobacco cream liquid is imported the macroporous resin column injection port being filled with macroporous resin, and the liquid take-off rate controlling described macroporous resin column outlet is every 4s mono-;
(3) use macroporous resin column described in 45% ethanol of 20% ethanol of 3 times of described macroporous resin column volumes, 3 times of described macroporous resin column volumes and 100% ethanol elution of 3 times of described macroporous resin column volumes successively, collect the elutriant of 100% ethanol;
(4) elutriant of described 100% ethanol being concentrated into relative density is 1.182, when refractive index is 1.468, obtains the liquid essence that described perfume quantity and aroma quality are outstanding.
Choose a kind of cigarette A not adding any essence and flavoring agent, and to be added in the present embodiment 2 the described perfume quantity of preparation and the outstanding liquid essence of aroma quality wherein according to the adding proportion of its pipe tobacco weight 0.01%, obtain cigarette A2.
The Analyses Methods for Sensory Evaluation Results of cigarette A2 is in table 1.
Embodiment 3
(1) just Zimbabwe's tobacco leaf, Brazilian tobacco leaf and Argentinian tobacco leaf three kinds of tobacco leaf specifications are pressed 2:2:1 mass ratio and are combined and use the extraction using alcohol of 100%, obtain the ethanolic soln containing leaf tobacco extract, in above-mentioned ethanolic soln, add the water of its 1/3 volume and leave standstill 16 hours at 6 DEG C; Ethanolic soln removing insolubles after filtering and standing, filtrate being concentrated into its alcoholic strength is 12%, obtains tobacco just cream liquid;
(2) according to the mass ratio of the first cream liquid of described tobacco and macroporous resin filler 1:6, first for described tobacco cream liquid is imported the macroporous resin column injection port being filled with macroporous resin, and the liquid take-off rate controlling described macroporous resin column outlet is every 3s mono-;
(3) use macroporous resin column described in 40% ethanol of 20% ethanol of 3 times of described macroporous resin column volumes, 3 times of described macroporous resin column volumes and 100% ethanol elution of 3 times of described macroporous resin column volumes successively, collect the elutriant of 100% ethanol;
(4) elutriant of described 100% ethanol being concentrated into relative density is 1.174, when refractive index is 1.454, obtains the liquid essence that described perfume quantity and aroma quality are outstanding.
Choose a kind of cigarette A not adding any essence and flavoring agent, and to be added in the present embodiment 3 the described perfume quantity of preparation and the outstanding liquid essence of aroma quality wherein according to the adding proportion of its pipe tobacco weight 0.01%, obtain cigarette A3.
The Analyses Methods for Sensory Evaluation Results of cigarette A3 is in table 1.
Table 1: Analyses Methods for Sensory Evaluation Results
Remarks: in sensory evaluation, the maximum score value of each assessment item is 15 points, in embodiment 1-3, each assessment item score is all that benchmark is evaluated with comparative example.
With the addition of in corresponding table 1 embodiment 1-3 in the sensory evaluation of cigarette A1, A2, the A3 of the liquid essence that perfume quantity of the present invention and aroma quality are given prominence to, score value shared by various odor type style and features divides other network diagramming respectively as illustrated in the accompanying drawings from 1 to 3.
As can be seen from table 1 and accompanying drawing 1-3, the cigarette that with the addition of the liquid essence that perfume quantity of the present invention and aroma quality are given prominence to is particularly outstanding in perfume quantity and aroma quality in sensory evaluation relative to the cigarette of comparative example, and liquid essence perfume quantity of the present invention and aroma quality can given prominence to adds in the cigarette needing to strengthen perfume quantity and aroma quality targetedly.
Claims (6)
1. the liquid essence that a perfume quantity and aroma quality are outstanding, it is characterized in that, it is by the preparation of the method that comprises the following steps: (1) by the mixture of multiple tobacco leaf with 100% extraction using alcohol, obtain the ethanolic soln containing leaf tobacco extract, in above-mentioned ethanolic soln, add the water of its 1/3 volume and leave standstill 8-16 hour at 0-6 DEG C; Ethanolic soln removing insolubles after filtering and standing, filtrate being concentrated into its alcoholic strength is 10-15%, obtains tobacco just cream liquid;
(2) according to the mass ratio of the first cream liquid of described tobacco and macroporous resin filler 1:5-1:8, first for described tobacco cream liquid is imported the macroporous resin column injection port being filled with macroporous resin, and the liquid take-off rate controlling described macroporous resin column outlet is every 2s-4s mono-;
(3) use macroporous resin column described in the 35-45% ethanol of 20% ethanol of 3 times of described macroporous resin column volumes, 3 times of described macroporous resin column volumes and 100% ethanol elution of 3 times of described macroporous resin column volumes successively, collect the elutriant of 100% ethanol;
(4) elutriant of described 100% ethanol being concentrated into relative density is 1.170-1.182, when refractive index is 1.446-1.468, obtains the liquid essence that described perfume quantity and aroma quality are outstanding.
2. liquid essence according to claim 1, it is characterized in that, the mixture of multiple tobacco leaf described in step (1) is the arbitrary combination of in the Argentinian tobacco leaf of Zimbabwe's tobacco leaf of different varieties, the Brazilian tobacco leaf of different varieties or different varieties at least two kinds.
3. liquid essence according to claim 1, is characterized in that, the described macroporous resin filler used in step (2) is non-polar macroporous resin.
4. liquid essence according to claim 1 is as the purposes of spices.
5. liquid essence according to claim 1 is as the purposes of tobacco spice in cigarette.
6. one kind comprises the cigarette of liquid essence as claimed in claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510131226.XA CN104804870B (en) | 2015-03-24 | 2015-03-24 | The liquid essence and its application in cigarette that a kind of perfume quantity and aroma quality protrude |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510131226.XA CN104804870B (en) | 2015-03-24 | 2015-03-24 | The liquid essence and its application in cigarette that a kind of perfume quantity and aroma quality protrude |
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| Publication Number | Publication Date |
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| CN104804870A true CN104804870A (en) | 2015-07-29 |
| CN104804870B CN104804870B (en) | 2018-06-12 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105223303A (en) * | 2015-10-29 | 2016-01-06 | 云南中烟工业有限责任公司 | A kind of method adopting index to characterize cigarette fruital odor characteristic |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111035057A (en) * | 2019-11-27 | 2020-04-21 | 内蒙古昆明卷烟有限责任公司 | Method for preparing tar extract from waste cigarette butts and application of tar extract in cigarettes |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105223303A (en) * | 2015-10-29 | 2016-01-06 | 云南中烟工业有限责任公司 | A kind of method adopting index to characterize cigarette fruital odor characteristic |
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| CN104804870B (en) | 2018-06-12 |
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