CN104783122A - Preparation method of sea-buckthorn health salt - Google Patents
Preparation method of sea-buckthorn health salt Download PDFInfo
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- CN104783122A CN104783122A CN201410384179.5A CN201410384179A CN104783122A CN 104783122 A CN104783122 A CN 104783122A CN 201410384179 A CN201410384179 A CN 201410384179A CN 104783122 A CN104783122 A CN 104783122A
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Abstract
The invention discloses a preparation method of sea-buckthorn health salt. The preparation method comprises the following steps: 1) sea-buckthorn pre-treatment, 2) supercritical CO2 extraction, and 3) recrystallization. The step of supercritical CO2 extraction comprises extracting sea-buckthorn powder obtained in the step 1) through supercritical CO2 to obtain a sea-buckthorn functional component. The step of recrystallization comprises: dissolving the sea-buckthorn functional component into a pure water solution at a normal temperature and a normal pressure, adding sodium chloride and dissolving sodium chloride till the solution is saturated; and performing vacuum evaporation at a pressure of 0.5*10<5>Pa-1*10<5>Pa and at a temperature of 4-35 DEG C to obtain a sea-buckthorn health salt crystal.
Description
Technical field
The invention belongs to food dressing field, health-care salt relating to vegetable ingredients and preparation method thereof, be in particular a kind of by sea buckthorn fruit through certain PROCESS FOR TREATMENT, prepare a kind of preparation method realizing the edible salt of health-care effect while ensureing seasoning.
Background technology
Salt is the necessity that people live, it is one of most important material of human survival, also be flavoring the most frequently used in culinary art, suitably put in dish and order salt, not only seasoning but also favourable health, but traditional salt only has seasoning effect usually, function ratio is more single, and sodium content is higher, although sodium is the essential nutrient element of the mankind, takes in and too much easily cause human body to occur the chronic diseases such as hypertension, oedema, coronary heart disease, angiocardiopathy.Therefore, while the seasoning of guarantee salt, the study hotspot that its health-care efficacy has become food dressing field is increased.
At present, in salt, add the plant salt with the making of the specified plant composition of health-care efficacy, attract attention.Plant salt contains natural plant composition, and meet consumption fashion and the nutrition demand of modern society people, consumer is acceptant.China market there is at present the plant salt kind such as spirulina salt, mushroom salt.But the vegetable ingredients that this two a little salt adds is little, generally only has less than 1%, is difficult to play health-care efficacy.Have patent report to be added in commodity salt by green tea powder and prepare health-care salt, but this health-care salt also exists the defect of mouthfeel difference.
Sea-buckthorn (Hippophae rhamnoides L) is a kind of nutritious, plant that medical value is high.Greeks find that sea-buckthorn has therapeutic action very early.Ju is said, in ancient Greek, even the sick horse obtained terribly, after sea-buckthorn forest grazing a period of time, just plump and sturdy, fur is glittering.China Tibetan medicine, Mongolian medicine and the traditional Chinese medical science just treat various disease with sea-buckthorn in ancient times.Sea-buckthorn, by " Chinese Pharmacopoeia ", is classified as medicine-food two-purpose kind.According to motherland's traditional medical theory, the main favourable lung of sea-buckthorn, strong cloudy, rise sun, nourishing the stomach, invigorating the spleen, invigorate blood circulation, the pharmacological effect such as stagnation resolvation.
Modern times biologist, medical scholar is by studying discovery further, sea buckthorn fruit mainly contains hundred kinds of bioactivators such as vitamins, protein and amino acids, oil & fat acids, volatile oil, organic acid, carbohydrate, microelement kind, flavonoids, terpene and steroid, the content of its Vc, dimension A and dimension K, dimension E is the hat of fruit, it is 4 times of Kiwi berry, nearly 10 times of hawthorn, 80 times of tomato.The seed of sea-buckthorn and seabuckthorn seeds can be extracted oil, and in every 100 grams of Seabuckthorn Oils, vitamin content is up to more than 100 milligrams, and B-carrotene more than 10 milligrams, wherein exceedes Superoxide dismutase (SOD) 2746 units, is 4 times of ginseng.Just because of these functional components that sea-buckthorn is rich in, thus it has the appellation of " holy fruit " and " sub-gold ".Also make sea-buckthorn possess adjusting blood lipid, blood pressure, improve myocardial ischemia, antifatigue simultaneously, strengthen many effects such as memory.Medical research confirms that sea buckthorn fruit has anticancer swollen, anti-ageing, radioresistance, anti-inflammatory, enhancing body immunity, dispels effect of foxiness, beauty treatment especially.
Sea buckthorn fruit is delicious, sweet and sour taste, nutritious, both can pluck to eat also to can be made into drink.Sea-buckthorn is the plant of traditional integration of drinking and medicinal herbs, is the important component of Chinese herbal medicine, in clinical practice or health-related food development, all have wide prospect.Health-care hippophae rhamnoide food is not only good to eat, also has natural health effect of sea-buckthorn.The multiple products such as seabuckthorn yogurt, sea buckthorn juice, Seabuckthorm Seed Oil, sea-buckthorn tea have been had to sell in the market.Sea-buckthorn taste is sour-sweet can well arrange in pairs or groups with cake, staple food, teas etc., and therefore, the development of health-care hippophae rhamnoide food has become a large focus in this field.
According to the inventors knowledge, there is no report at present and sea-buckthorn is added in salt, or prepare Patents and the document of mouthfeel and all excellent vegetalitas edible salt of health-care effect.
Summary of the invention
The object of the invention is to provide a kind of health-care hippophae rhamnoide salt and preparation method thereof, the sea buckthorn fruit of maturation or seed powder or extract are added in commodity salt.
The present invention solves the problems of the technologies described above adopted technical scheme:
1, a preparation method for health-care hippophae rhamnoide salt, comprises the steps:
1) sea-buckthorn pretreatment: sea-buckthorn is dried 4 ~ 6hr at 60 ~ 100 DEG C, controlling water content is 5 ~ 10%, and stoning, is crushed to 60 ~ 100 orders, 75 ~ 100 DEG C of hot-water soak 30min ~ 3hr; Filter, washing, dry, obtain total sugar content and be less than 10%, the seabuckthorn fruit powder that water content is less than 10%;
2) supercritical CO
2extraction: by step 1) described in seabuckthorn fruit powder pass through supercritical CO
2extraction obtains the functional component of sea-buckthorn, comprises following extraction step:
A, pressure are 25 ~ 35MPa, temperature 25 ~ 40 DEG C, time 30 ~ 60min, remove residues of pesticides;
B, pressure are 25 ~ 35MPa, temperature 30 ~ 33 DEG C, time 30min ~ 6hr, obtain cAMP, colors;
C, pressure are 30 ~ 35MPa, temperature 30 ~ 37 DEG C, time 2 ~ 5hr, obtain vitamin and triterpenic acid;
D, pressure are 33 ~ 35MPa, temperature 35 ~ 45 DEG C, time 2 ~ 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the sea-buckthorn function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa ~ 1x10
5pa, temperature is 4 ~ 35 DEG C, and namely reduction vaporization obtains health-care hippophae rhamnoide salt crystal.
Preferably, in order to ensure that obtained health-care hippophae rhamnoide salt has less impurity, health-care hippophae rhamnoide salt is better prepared; The purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
Preferably, in order to the sea-buckthorn function component content that obtains and purity higher, described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
The nucleus of the health-care hippophae rhamnoide salt crystal prepared is the functional component of sea-buckthorn, and the nucleus of described health-care hippophae rhamnoide salt crystal is the functional component of sea-buckthorn, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described health-care hippophae rhamnoide salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
The invention has the beneficial effects as follows:
1, this invention proposes health-care components sea-buckthorn to be added in commodity salt first, has filled up this field in a way blank.
2, by adding health-care components in daily flavouring salt---sea-buckthorn, avoid taking in separately mouthfeel that sea-buckthorn produces single and be difficult to ensure successional drawback, in the long run, the edible health care of this health-care salt to human body more has continuation.The present invention sea-buckthorn used is that the dried powder of sea-buckthorn or the nutrients of extract to sea-buckthorn have inspissation, further increases its health-care efficacy.
3, hippophae rhamnoides nutrition enriches, and sea-buckthorn contains abundant vitamins, protein and amino acids, oil & fat acids, volatile oil, organic acid, carbohydrate, microelement kind, flavonoids, terpene and steroid etc.In addition, also containing a large amount of mineral elements, as potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc, selenium etc.Health-care hippophae rhamnoide salt of the present invention can not only regulate immunity of organisms, and have anticancer, antitumor, hypoglycemic, reducing blood lipid, protect the liver, the anti-ageing effect of waiting for a long time, long-term edible prevention and the treatment being particularly conducive to health and chronic disease, thus meet the idea that people more and more focus on nutritional need, reduce the risk that Excess free enthalpy sodium salt causes the disease such as hypertension, coronary heart disease.
4, traditional sea buckthorn resources of China is combined with salt product the health-care salt developed, on the basis keeping salt outward appearance, highlight peculiar taste and the color and luster of sea-buckthorn, taste is sour-sweet suitable, greatly can meet the diversified demand of consumer in culinary art, promote the mouthfeel of dish, for the effect of fishlike smell and meat fishy smell can also be removed in the culinary art of meat dish, accomplish " hyperchromic increase taste again ".
5, too much eat as the acid foods such as meat, poultry, fish, dairy products are easy to cause acidic constitution, we are mostly acidic food for usually edible commodity salt, and contain the metallic elements such as more potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc in sea buckthorn fruit and seed, its powder and extract are base-forming food, and the health-care salt made with this is also base-forming food.Acid-base balance in human body depends on the Acidity of Aikalinity of institute's dietary intake, and long-term this health-care salt edible contributes to the unnecessary acidic materials of neutralization in body, to maintain the acid-base balance of human body, is conducive to the permanent health of consumer.
The invention has the beneficial effects as follows the preparation method providing the sub-health-care salt of a kind of sea-buckthorn, the extract of sub-for sea-buckthorn powder is added in commercial salt, farthest can play the health-care effect of sea-buckthorn, make people while use salt reaches seasoning object, facilitate the health of self.
Detailed description of the invention
Following examples are used for the present invention is described, but are not used for limiting the scope of the invention.
The preparation of embodiment 1, a kind of health-care hippophae rhamnoide salt
A preparation method for health-care hippophae rhamnoide salt, comprises the steps:
1) sea-buckthorn pretreatment: sea-buckthorn is dried 4hr at 100 DEG C, controlling water content is 5%, and stoning, is crushed to 60 orders, 75 DEG C of hot-water soak 3hr; Filter, washing, dry, obtain total sugar content and be less than 8%, the seabuckthorn fruit powder that water content is less than 5%;
2) supercritical CO
2extraction: by step 1) described in seabuckthorn fruit powder pass through supercritical CO
2extraction obtains the functional component of sea-buckthorn, comprises following extraction step:
A, pressure are 25MPa, temperature 40 DEG C, time 60min, remove residues of pesticides;
B, pressure are 25MPa, temperature 33 DEG C, time 3hr, obtain cAMP, colors;
C, pressure are 30MPa, temperature 37 DEG C, time 3hr, obtain vitamin and triterpenic acid;
D, pressure are 33MPa, temperature 45 C, time 3hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the sea-buckthorn function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa, temperature is 10 DEG C, and namely reduction vaporization obtains health-care hippophae rhamnoide salt crystal.
The purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
Described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
The nucleus of described health-care hippophae rhamnoide salt crystal is the functional component of sea-buckthorn, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described health-care hippophae rhamnoide salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
The preparation of embodiment 2, a kind of health-care hippophae rhamnoide salt
A preparation method for health-care hippophae rhamnoide salt, comprises the steps:
1) sea-buckthorn pretreatment: sea-buckthorn is dried 6hr at 60 DEG C, controlling water content is 10%, and stoning, is crushed to 100 orders, 100 DEG C of hot-water soak 3hr; Filter, washing, dry, obtain total sugar content and be less than 5%, the seabuckthorn fruit powder that water content is less than 5%;
2) supercritical CO
2extraction: by step 1) described in seabuckthorn fruit powder pass through supercritical CO
2extraction obtains the functional component of sea-buckthorn, comprises following extraction step:
A, pressure are 25MPa, temperature 25 DEG C, time 60min, remove residues of pesticides;
B, pressure are 35MPa, temperature 30 DEG C, time 6hr, obtain cAMP, colors;
C, pressure are 35MPa, temperature 30 DEG C, time 5hr, obtain vitamin and triterpenic acid;
D, pressure are 35MPa, temperature 35 DEG C, time 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the sea-buckthorn function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 1x10 at pressure
5pa, temperature is 30 DEG C, and namely reduction vaporization obtains health-care hippophae rhamnoide salt crystal.
Claims (5)
1. a preparation method for health-care hippophae rhamnoide salt, comprises the steps:
1) sea-buckthorn pretreatment: sea-buckthorn is dried 4 ~ 6hr at 60 ~ 100 DEG C, controlling water content is 5 ~ 10%, and stoning, is crushed to 60 ~ 100 orders, 75 ~ 100 DEG C of hot-water soak 30min ~ 3hr; Filter, washing, dry, obtain total sugar content and be less than 10%, the seabuckthorn fruit powder that water content is less than 10%;
2) supercritical CO
2extraction: by step 1) described in seabuckthorn fruit powder pass through supercritical CO
2extraction obtains the functional component of sea-buckthorn, comprises following extraction step:
A, pressure are 25 ~ 35MPa, temperature 25 ~ 40 DEG C, time 30 ~ 60min, remove residues of pesticides;
B, pressure are 25 ~ 35MPa, temperature 30 ~ 33 DEG C, time 30min ~ 6hr, obtain cAMP, colors;
C, pressure are 30 ~ 35MPa, temperature 30 ~ 37 DEG C, time 2 ~ 5hr, obtain vitamin and triterpenic acid;
D, pressure are 33 ~ 35MPa, temperature 35 ~ 45 DEG C, time 2 ~ 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the sea-buckthorn function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa ~ 1x10
5pa, temperature is 4 ~ 35 DEG C, and namely reduction vaporization obtains health-care hippophae rhamnoide salt crystal.
2. the preparation method of health-care hippophae rhamnoide salt as claimed in claim 1, is characterized in that: the purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
3. the preparation method of health-care hippophae rhamnoide salt as claimed in claim 1, is characterized in that: described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
4. the preparation method of health-care hippophae rhamnoide salt as claimed in claim 1, is characterized in that: the nucleus of described health-care hippophae rhamnoide salt crystal is the functional component of sea-buckthorn, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described health-care hippophae rhamnoide salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
5. a health-care hippophae rhamnoide salt, the preparation method of the health-care hippophae rhamnoide salt as described in as arbitrary in Claims 1 to 4 obtains.
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| CN201410384179.5A CN104783122A (en) | 2014-08-06 | 2014-08-06 | Preparation method of sea-buckthorn health salt |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106858519A (en) * | 2017-01-16 | 2017-06-20 | 中盐新干盐化有限公司 | A kind of health-care hippophae rhamnoide edible salt and preparation method thereof |
| CN108283306A (en) * | 2017-12-27 | 2018-07-17 | 天津佰亿达企业管理股份有限公司 | A kind of health-care hippophae rhamnoide edible salt and preparation method thereof |
| CN108635383A (en) * | 2018-08-01 | 2018-10-12 | 中国科学院青海盐湖研究所 | Sea-buckthorn salt cream and preparation method thereof |
| CN113080428A (en) * | 2021-04-19 | 2021-07-09 | 云南省盐业有限公司 | Edible health-care salt and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101331938A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Natural green tea health edible salt |
| CN102342482A (en) * | 2011-09-28 | 2012-02-08 | 四川久大品种盐有限责任公司 | Iodized tea salt and preparation method thereof |
| CN102960706A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Re-crystallization preparation method of bamboo salt |
-
2014
- 2014-08-06 CN CN201410384179.5A patent/CN104783122A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101331938A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Natural green tea health edible salt |
| CN102342482A (en) * | 2011-09-28 | 2012-02-08 | 四川久大品种盐有限责任公司 | Iodized tea salt and preparation method thereof |
| CN102960706A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Re-crystallization preparation method of bamboo salt |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106858519A (en) * | 2017-01-16 | 2017-06-20 | 中盐新干盐化有限公司 | A kind of health-care hippophae rhamnoide edible salt and preparation method thereof |
| CN108283306A (en) * | 2017-12-27 | 2018-07-17 | 天津佰亿达企业管理股份有限公司 | A kind of health-care hippophae rhamnoide edible salt and preparation method thereof |
| CN108635383A (en) * | 2018-08-01 | 2018-10-12 | 中国科学院青海盐湖研究所 | Sea-buckthorn salt cream and preparation method thereof |
| CN113080428A (en) * | 2021-04-19 | 2021-07-09 | 云南省盐业有限公司 | Edible health-care salt and preparation method thereof |
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Application publication date: 20150722 |