CN104759256A - Frangipani porous particle and application thereof - Google Patents
Frangipani porous particle and application thereof Download PDFInfo
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- CN104759256A CN104759256A CN201510078803.3A CN201510078803A CN104759256A CN 104759256 A CN104759256 A CN 104759256A CN 201510078803 A CN201510078803 A CN 201510078803A CN 104759256 A CN104759256 A CN 104759256A
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- frangipanis
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Abstract
The invention discloses a frangipani porous particle and application thereof, and 20-60 mesh frangipani porous particle is prepared from frangipani powder with the moisture content of 8-12% and particle size of 100 to 160 mesh and sucrose or mannitol as raw materials by fluidized bed top spray process by use of sodium carboxymethyl starch or / and hydroxypropyl methyl cellulose as a binder, frangipani contains not only volatile oil and other flavor components, also contains large amount of polysaccharides, the frangipani is prepared into a granule material for adding into a cigarette filter stick for effectively reducing the cigarette smoke stimulating, enriching cigarette aroma, increasing sweet returning feeling, and improving the moisturizing effect of the cigarette filter stick. The frangipani porous particle has a rough surface and a high specific surface area, the effective contact area of granular materials and cigarette smoke can be significantly improved, and ammonia and phenol in the cigarette smoke can be selectively adsorbed. The frangipani porous particle has the advantages of simple production process, raw materials easy to obtain, low cost, easy realization of industrial production and good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of frangipanis porous particle that can improve flavor quality of cigarette.Meanwhile, the invention still further relates to the application of this porous particle in Cigarette processing.
Background technology
Along with smoking and healthy problem more and more receive publicity, that how to improve cigarette sucks security, reduces the harmful components in cigarette smoke, improves the focus that the comfort of suction just becomes the research and development of each tobacco productive corporation.Cigarette material researcher utilizes natural plant material to develop some filter stick granular materials, the mode of main employing is the particle be directly ground into by vegetable material between 20 ~ 80 orders, or vegetable material is prepared into particle by extrusion, although at cigarette flavouring, harm reduction aspect achieves certain effect, but also there is the shortcoming of the following aspects: vegetable material is directly ground into particle by (1), grain shape is uneven, physical instability, when cigarette filter tip shaping, particle is easily made broken thus is produced a large amount of dust, stock utilization is not high, (2) particle is prepared by extrusion, the hole embedding that vegetable material itself easily has by the adhesive added, the contact area of granular materials and cigarette smoke is limited, its reducing tar and reducing harm limited use, particle is simultaneously comparatively tight, hardness is comparatively large, is unfavorable for the preparation of composite cigarette filter stick.For above-mentioned shortcoming, how to adopt suitable technology, preparation is applicable to the plant porous material of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Frangipanis, calls remote cape jasmine, yolk flower, India jasmine, great Ji Hua, belongs to Apocynaceae.Frangipanis corolla tubular, footpath is 5 ~ 6cm about, and 5 split; Outside milky, center foresythia, delicate fragrance is graceful.The main chemical compositions of frangipanis has the volatile oil such as squalene, linalool, citral, geranial, the iridoidses such as flavonoids and plumericin, plumieride, rich watt red eggs florigen such as mountain naphthalene element, mountain naphthalene element glycosides.Frangipanis has heat-clearing, moistening lung, removing toxic substances, dampness removing, the effects such as cough-relieving.But in the prior art about frangipanis being made honeycombed grain material and the research being applied to cigarette filter rod there is not yet relevant report.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide that a kind of resist processing is strong, uniform particles, security are high, flavouring successful, there is the frangipanis porous particle of certain harm reduction effect.
The present invention also aims to provide the described application of frangipanis porous particle in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of frangipanis porous particle, is obtained by the method for following steps:
(1) naturally being dried by frangipanis to moisture content is 8 ~ 12%, then to be ground into particle diameter be further 100 ~ 160 object powder, for subsequent use;
(2) sucrose or sweet mellow wine being pulverized is 100 ~ 160 object powder, for subsequent use;
(3) take 90 ~ 99 parts of frangipanis powder, 1 ~ 10 portion of sucrose or mannitol powder according to weight portion, mix, for subsequent use;
(4) take sodium carboxymethyl starch 4 ~ 8 parts, hydroxypropyl methylcellulose 0 ~ 4 part according to weight portion, then be mixed with distilled water the binder solution that concentration is 4 ~ 8%, for subsequent use;
(5) take mixed-powder 800 ~ 1100g for subsequent use and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) under fluidisation air pressure 0.12 ~ 0.15Bar, gas flow temperature 50 DEG C of conditions dry 5 ~ 10 minutes; B () is fluidisation air pressure 0.16 ~ 0.24Bar, gas flow temperature 50 ~ 60 DEG C, under atomisation pressure 0.08 ~ 0.12Bar, the hydrojet speed condition of 6 ~ 8g/ minute, employing top spray mode applies the binder solution that step (4) is prepared, and binder solution consumption is 20% ~ 40% of dry material weight; C () adhesive has applied after, repeat step (a), preparing moisture is 8 ~ 10%, and shaggy similar round particle is required frangipanis porous particle.
Wherein, obtained its particle diameter of frangipanis porous particle is 20 ~ 60 orders.
Described adhesive is food-grade.
Described fluid bed is preferably Midi Glatt fluid bed.
Described frangipanis porous particle is applied in cigarette, it is characterized in that: the frangipanis porous particle adding 1 ~ 2mg in every millimeter of composite cigarette filter stick.
Compared with prior art, the present invention has the following advantages:
1. not only contain volatilization wet goods flavor component in frangipanis, also containing a large amount of polysaccharide components, be prepared into corresponding granular materials, add in cigarette filter rod, effectively can reduce cigarette smoke excitant, enrich cigarette flavor, increase cigarette and return sweet sense, and promote the humectation effect of cigarette filter rod.
2. the frangipanis porous particle size prepared by the present invention is even, stable in physicochemical property, there is good resist processing, what avoid that granular materials in filter stick formation process produces because of machining makes broken and dust, and granular materials can be uniformly distributed in filter stick tow.
3. gained frangipanis porous particle rough surface, has higher specific area, significantly improves effective contact area of granular materials and cigarette smoke, can ammonia in selective absorption cigarette smoke and phenol.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has application prospect well.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Getting Fresh Egg spends nature to dry to moisture 12%, then raw meal to be broken into particle diameter be 100 object powder, pulverizes sucrose for particle diameter 100 object powder in addition, take the frangipanis powder of 950g, 50g sucrose powder, mix; Made mixed-powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.12Bar, gas flow temperature is under 50 DEG C of conditions dry 10 minutes; Then sodium carboxymethyl starch distilled water is mixed with the binder solution that concentration is 8%, fluidisation air pressure be 0.18Bar, gas flow temperature is 50 DEG C, atomisation pressure is 0.08Bar, hydrojet speed is under 8g/ minute condition, adopts top spray mode to spray 300g binder solution; After adhesive has applied, setting fluidisation air pressure 0.12Bar, gas flow temperature are under 50 DEG C of conditions dry 8 minutes, moisture is adjusted to 10%, crosses 60 mesh sieves and namely obtain cigarette filter rod frangipanis porous particle.
Embodiment 2
Getting Fresh Egg spends nature to dry to moisture 10%, then raw meal to be broken into particle diameter be 120 object powder, pulverizes sucrose for particle diameter 120 object powder in addition, take the frangipanis powder of 980g, 20g sucrose powder, mix; Made mixed-powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.15Bar, gas flow temperature is under 60 DEG C of conditions dry 6 minutes; Then sodium carboxymethyl starch 3 parts, hydroxypropyl methylcellulose 3 parts is taken by weight, the binder solution that concentration is 6% is mixed with distilled water, be 0.22Bar, gas flow temperature 60 DEG C at fluidisation air pressure, atomisation pressure is 0.12Bar, hydrojet speed is under 7g/ minute condition, adopts top spray mode to spray 280g binder solution; After adhesive has applied, setting fluidisation air pressure 0.15Bar, gas flow temperature are under 60 DEG C of conditions dry 10 minutes, moisture is adjusted to 11%, crosses 40 mesh sieves and namely obtain cigarette filter rod frangipanis porous particle.
Embodiment 3
Getting Fresh Egg spends nature to dry to moisture 9%, then raw meal to be broken into particle diameter be 160 object powder, pulverizes sweet mellow wine for particle diameter 160 object powder in addition, take the frangipanis powder of 900g, 100g mannitol powder, mix; Made mixed-powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.14Bar, gas flow temperature is under 55 DEG C of conditions dry 10 minutes; Then sodium carboxymethyl starch 2 parts, hydroxypropyl methylcellulose 3 parts is taken by weight, the binder solution that concentration is 5% is mixed with distilled water, be 0.20Bar, gas flow temperature 60 DEG C at fluidisation air pressure, atomisation pressure is 0.12Bar, hydrojet speed is under 6g/ minute condition, adopts top spray mode to spray 320g binder solution; After adhesive has applied, setting fluidisation air pressure 0.15Bar, gas flow temperature are under 55 DEG C of conditions dry 10 minutes, moisture is adjusted to 11%, crosses 20 mesh sieves and namely obtain cigarette filter rod frangipanis porous particle.
Application Example 1
Gained frangipanis porous particle being prepared by embodiment 1 is applied in composite cigarette filter stick, and every millimeter of cigarette filter rod adds 1mg granular materials, is prepared into experiment cigarette, carries out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter, and the sweet sense of flue gas is obvious; Harmful ingredients in flue gas detects and shows: ammonia reduced rate is 14.3%, phenol reduced rate is 16.6%, and this porous particle can ammonia in selective absorption cigarette smoke and phenol.
Application Example 2
Gained frangipanis porous particle being prepared by embodiment 2 is applied in composite cigarette filter stick, and every millimeter of cigarette filter rod adds 2mg granular materials, is prepared into experiment cigarette, carries out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter, and the sweet sense of flue gas is obvious; Harmful ingredients in flue gas detects and shows: ammonia reduced rate is 15.6%, phenol reduced rate is 17.3%, and this porous particle can ammonia in selective absorption cigarette smoke and phenol.
Application Example 3
Gained frangipanis porous particle being prepared by embodiment 3 is applied in composite cigarette filter stick, every millimeter of cigarette filter rod adds 1.5mg granular materials, being prepared into experiment cigarette, carrying out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter, and the sweet sense of flue gas is obvious; Harmful ingredients in flue gas detects and shows: ammonia reduced rate is 16.3%, phenol reduced rate is 18.1%, and this porous particle can ammonia in selective absorption cigarette smoke and phenol.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a frangipanis porous particle, is obtained by the method for following steps:
(1) naturally being dried by frangipanis to moisture content is 8 ~ 12%, then to be ground into particle diameter be further 100 ~ 160 object powder, for subsequent use;
(2) sucrose or sweet mellow wine being pulverized is 100 ~ 160 object powder, for subsequent use;
(3) take 90 ~ 99 parts of frangipanis powder, 1 ~ 10 portion of sucrose or mannitol powder according to weight portion, mix, for subsequent use;
(4) take sodium carboxymethyl starch 4 ~ 8 parts, hydroxypropyl methylcellulose 0 ~ 4 part according to weight portion, then be mixed with distilled water the binder solution that concentration is 4 ~ 8%, for subsequent use;
(5) take mixed-powder 800 ~ 1100g for subsequent use and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) under fluidisation air pressure 0.12 ~ 0.15Bar, gas flow temperature 50 DEG C of conditions dry 5 ~ 10 minutes; B () is fluidisation air pressure 0.16 ~ 0.24Bar, gas flow temperature 50 ~ 60 DEG C, under atomisation pressure 0.08 ~ 0.12Bar, the hydrojet speed condition of 6 ~ 8g/ minute, employing top spray mode applies the binder solution that step (4) is prepared, and binder solution consumption is 20% ~ 40% of dry material weight; C () adhesive has applied after, repeat step (a), preparing moisture is 8 ~ 10%, and shaggy similar round particle is required frangipanis porous particle.
2. frangipanis porous particle according to claim 1, is characterized in that: obtained its particle diameter of frangipanis porous particle is 20 ~ 60 orders.
3. frangipanis porous particle according to claim 1, is characterized in that: use adhesive to be food-grade.
4. frangipanis porous particle according to claim 1, is characterized in that: described fluid bed is preferably Midi Glatt fluid bed.
5. frangipanis porous particle according to claim 1 is applied in cigarette, it is characterized in that: the frangipanis porous particle adding 1 ~ 2mg in every millimeter of composite cigarette filter stick.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510078803.3A CN104759256A (en) | 2015-02-13 | 2015-02-13 | Frangipani porous particle and application thereof |
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| CN201510078803.3A CN104759256A (en) | 2015-02-13 | 2015-02-13 | Frangipani porous particle and application thereof |
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| CN104759256A true CN104759256A (en) | 2015-07-08 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108323804A (en) * | 2018-01-24 | 2018-07-27 | 云南中烟工业有限责任公司 | A kind of cigarette filter rod Yunnan olive porous particle and its application |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101044918A (en) * | 2007-04-30 | 2007-10-03 | 温纯青 | Frangipani shaped Cigarette with egg extraction for reducing |
| CN102318898A (en) * | 2011-08-20 | 2012-01-18 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing natural plant granular materials for filter tips |
| CN103689795A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Peony porous particle and application thereof in cigarette |
| CN103689796A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Lemon grass porous particle and application thereof in cigarettes |
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- 2015-02-13 CN CN201510078803.3A patent/CN104759256A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101044918A (en) * | 2007-04-30 | 2007-10-03 | 温纯青 | Frangipani shaped Cigarette with egg extraction for reducing |
| CN102318898A (en) * | 2011-08-20 | 2012-01-18 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing natural plant granular materials for filter tips |
| CN103689795A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Peony porous particle and application thereof in cigarette |
| CN103689796A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Lemon grass porous particle and application thereof in cigarettes |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108323804A (en) * | 2018-01-24 | 2018-07-27 | 云南中烟工业有限责任公司 | A kind of cigarette filter rod Yunnan olive porous particle and its application |
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Application publication date: 20150708 |