CN103876284A - Application of oak barks, functional filter stick additives, preparation method for functional filter stick additives and application on the functional filter stick additives - Google Patents
Application of oak barks, functional filter stick additives, preparation method for functional filter stick additives and application on the functional filter stick additives Download PDFInfo
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- CN103876284A CN103876284A CN201410076513.0A CN201410076513A CN103876284A CN 103876284 A CN103876284 A CN 103876284A CN 201410076513 A CN201410076513 A CN 201410076513A CN 103876284 A CN103876284 A CN 103876284A
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Abstract
The invention discloses application of oak barks, functional filter stick additives, a preparation method for the functional filter stick additives and application on the functional filter stick additives. The oak barks serve as cigarette filter stick adding ingredients, and are compounded with binding agents, tobacco leaves and/or tobacco stem powder and tobacco flavor to obtain cigarette filter stick additives which are used for enhancing aroma of smoke of cigarettes and reducing the content of tar in the smoke of the cigarettes. The preparation method for the cigarette filter stick additives comprises the following steps of uniformly mixing oak bark powder and tobacco leaves and/or tobacco stem powder to obtain mixture; further mixing the mixture and aqueous solution with the binding agents and the tobacco flavor; and performing spray drying and screening to obtain the cigarette filter stick additives. By using the cigarette filter stick additives, the content of the tar in the smoke of the cigarettes can be effectively reduced, compound aroma can be added to the smoke of cigarettes, and moreover, the processing and forming property of filter sticks of the cigarettes can be improved. The preparation method is simple; raw materials are easy to obtain; the production cost is low; and requirements on industrial production can be met.
Description
Technical field
The present invention is specifically related to the application of oak bark and a kind of functional form filter stick additive and its preparation method and application, belongs to production of cigarettes technical field,
Background technology
At present, make great efforts to improve sucking security and having become the common recognition of domestic and international tobacco business of cigarette, in order to reduce tar content in cigarette mainstream flue gas and other harmful components wherein, improve the security of sucking of cigarette, tobacco scientific and technical personnel have carried out a large amount of scientific researches, extensive use new technology, new technology, new material, doing a series of activities aspect research and production low tar, low hazard cigarette product.The particulate adsorbent material that is applied at present cigarette filter material mostly is inorganic material as diatomite, active carbon, silica gel etc., they have special configuration of surface and many cavity structures, cigarette smoke is produced to efficient selective adsorption capacity, but had the problem such as assorted gas, change cigarette smoking style of introducing.And adopt the technological means such as expanding tobacco particle to realize the object of reducing tar and reducing harm, but owing to containing a large amount of fragrance matters in coke tar in cigarette, along with reducing the reduction of tar, also lost a large amount of fragrance simultaneously, affect tobacco suction taste.Therefore, how in reducing tar content in tobacco, to guarantee that do not lose fragrance and taste is the problem that industry emphasis is considered as far as possible.
Oak bark, claim again cork, in prior art, have oak bark for making the report of cork flooring, as patent (publication number 101602220) discloses the cork flooring of a kind of comfortable, durable, environmental protection, attractive in appearance, sound insulation, the performance such as heat insulation, moistureproof, anti-skidding, fire-retardant.Patent (publication number 1344605A) discloses a kind of composite cork ornament materials, oak bark classification is processed into the cork ornament of the characteristic such as few containing sand, tomography area is large, but in the prior art, never crosses oak bark is applied to the report in cigarette.
Summary of the invention
For the deficiencies in the prior art, first object of the present invention is to be to provide oak bark to be added in cigarette filter rod as cigarette filter rod adding ingredient, can effectively reduce tar content and the machine-shaping property that improves filter stick in cigarette smoke.
Second object of the present invention is to be to provide one can effectively reduce tar content and flue gas flavouring in cigarette smoke, can improve the additive of cigarette filter stick of cigarette filter rod machine-shaping property simultaneously.
The 3rd object of the present invention is to be to provide described additive application in cigarette filter rod, can effectively reduce tar content and flue gas flavouring in cigarette smoke, simultaneously to improve cigarette filter rod machine-shaping property.
The 4th object of the present invention is to be to provide a kind of simple to operate, method that low cost is prepared described additive, and the method meets suitability for industrialized production.
The invention provides the application of oak bark, this application is to be applied to the tar content reducing in cigarette smoke using oak bark as cigarette filter rod adding ingredient.
Described application is to be applied to oak bark as cigarette filter rod adding ingredient improve the machine-shaping property of filter stick and reduce the tar content in cigarette smoke.
Described oak bark is ground into powder and tobacco leaf and/or offal powder, binding agent and flavouring essence for tobacco 100:(5～40 in mass ratio): (1～10): (0.1～1) granulation thing additive, is added in cigarette filter rod tow.
Described particle additive particle diameter is 20～80 orders; Be preferably 30～60 orders.
Described tobacco leaf and/or offal powder diameter are for being not more than 200 orders.
Described binding agent is one or more in modified starch, shitosan, sodium alginate, pectin.
Described flavouring essence for tobacco is one or more in tobacco extract, cloud and mist absolute oil, methyl cyclopentenyl ketone, Megastigmatrienone.
Described oak bark powder diameter is 80～120 orders.
Described oak bark powder is through oak bark removal of impurities, dry, mechanical disintegration, and the screening of sieving obtains.
Described tobacco leaf and/or offal be waste tobacco leaf and or offal obtain by screening through pulverizing, grind, sieving.
The present invention also provides a kind of functional form filter stick additive, this additive by following mass parts component by solution mix, dry composite forms:
100 parts, oak bark powder;
5～40 parts, tobacco leaf and/or offal powder;
1～10 part of binding agent;
0.1～1 part of flavouring essence for tobacco.
The present invention also provide a kind of as described in the application of additive, this application is that described additive is added on and in cigarette filter rod, is applied to the tar content and the flue gas flavouring that reduce in cigarette smoke.
Described application is that described additive is added in cigarette filter rod and is applied to and reduces tar content, the flue gas flavouring in cigarette smoke and improve filter stick machine-shaping property.
Described additive is added in cigarette filter rod tow.
Described additive addition in the tow base material of cigarette filter rod is 1mg/mm～3mg/mm.
The present invention has added described additive and has been added on cigarette in tow and becomes unit filter stick, is more further combined into binary or polynary cigarette filter rod with common acetate fiber unit filter stick.
The present invention also provides a kind of preparation method of described additive, this preparation method is to be after 80～120 object oak bark powder and granularity are not more than 200 object tobacco leaves and/or offal powder and mix by granularity, again further and be dissolved with the aqueous solution of binding agent and flavouring essence for tobacco, obtain slurry; By gained slurry spray dry after, the sieve that sieves is got sieve 20～80 order particles, to obtain final product.
The described sieve that sieves is got grain graininess and is preferably 30～60 orders.
Described spray drying control system pellet moisture mass content is 6%～12%.
Beneficial effect of the present invention: the present invention is applied to oak bark in cigarette filter rod first, utilizes binding agent that oak bark, tobacco leaf and/or offal powder and flavouring essence for tobacco are combined into filter stick additive well.On the one hand, this filter stick additive has kept the outstanding mechanical performance of oak bark, heat-insulating property, the filter stick tow base material that has added this filter stick additive has suitable hardness and toughness, be conducive to machine-shaping and become filter stick, can reduce the wearing and tearing to equipment in filter stick process, temperature, especially cigarette that good thermal insulation simultaneously can reduce flue gas and enter oral cavity burn and suck while approaching filter end, may provide better suction impression to smoker.On the other hand, binding agent is by oak bark and tobacco leaf and/or offal powder bonding, and seal well flavouring essence for tobacco up for safekeeping enriching in fiber hole at oak bark and tobacco leaf and/or offal powder, not only effectively utilize the pore structure filter of additive to hold back flue gas, also can utilize the elasticity of oak bark to make to aspirate time, in filter stick, form moment cavity to change flow of flue gas mode and to increase filter end air permeability, reach unexpected effect, not only can effectively reduce the tar content in cigarette smoke, and flavouring essence for tobacco energy Stable Release in additive, make fragrance fuller abundant, lastingly, solve filter stick in prior art and fallen Jiao but the shortcoming of impact suction taste.In addition, additive raw material of the present invention source is wide, and preparation method is simple, greatly reduces production cost, meets suitability for industrialized production.
The specific embodiment
Following examples are intended to illustrate the present invention, rather than further restriction to protection domain of the present invention.
Embodiment 1
First prepare filter stick particulate additive: get the dry rear physical mechanical of 5KG oak bark removal of impurities and pulverize, screening is got 80～120 object particles and obtained oak bark powder; Getting 3KG waste tobacco leaf pulverizing grinding gets lower than 200 order fine powders for subsequent use; Oak bark particle and Discarded Tobacco powder are mixed to obtain to dry mixed powder according to a certain weight ratio; Get suitable quantity of water soluble chitosan and tobacco extract and be dissolved in suitable quantity of water and be configured to the certain density aqueous solution, wherein, the mass ratio of oak bark powder, waste tobacco leaf powder, shitosan, tobacco extract is 100:20:3:0.5; Powder and aqueous solution are stirred and be configured to slurry; The slurry preparing is entered to spray dryer and spray dryly, control pellet moisture 6～12wt%, the particle screening obtaining is got to 30～60 order particles and obtain required functional form filter stick additive.The filter stick additive of preparation is propped up and evenly made an addition in cigarette filter rod tow with 2mg/, make after unit filter stick, be more further combined into binary compound bar and be prepared into cigarette with acetate fiber unit filter stick.Detect analysis and show, this additive has filter stick and processes suitable hardness and toughness, reduces tar content 1.0mg/ in cigarette mainstream flue gas and props up, and has obvious flavouring effect simultaneously.
Cigarette and common fiber tow filter rods cigarette that the binary compound filter candle that adopts the present embodiment to prepare is made, transfer to specialized review person to smoke panel test, and it is as shown in the table for evaluation and analysis result:
Embodiment 2
First prepare filter stick particulate additive: get the removal of impurities of 5KG oak bark dry after physical mechanical pulverize, 80～120 object particles are got in screening, and to obtain required oak bark powder for subsequent use; Getting 3KG waste tobacco stem pulverizing grinding gets lower than 200 order fine powders for subsequent use; Oak bark particle and Discarded Tobacco powder are mixed to obtain to dry mixed powder according to a certain weight ratio; Get appropriate sodium alginate and cloud and mist absolute oil and be dissolved in suitable quantity of water and be configured to the certain density aqueous solution, wherein, the mass ratio of oak bark powder, Discarded Tobacco powder, sodium alginate, cloud and mist absolute oil is 100:30:5:0.8; Powder and aqueous solution are stirred and be configured to certain density slurry; The slurry preparing is entered to spray dryer and spray dryly, control pellet moisture 6～12wt%, the particle screening obtaining is got to 30～60 order particles and obtain required functional form filter stick additive.The filter stick additive of preparation is propped up and evenly made an addition in cigarette filter rod tow with 3mg/, make after filter stick, be more further combined into binary filter stick with cellulose acetate filter rod, then make cigarette.Detect analysis and show, this additive has filter stick and processes suitable hardness and toughness, reduces tar content 1.5mg/ in cigarette mainstream flue gas and props up, and has obvious flavouring effect simultaneously.
The binary compound filter candle that adopts the present embodiment to prepare is made to cigarette and the common fiber tow filter rods cigarette of filter, transfer to specialized review person to smoke panel test, it is as shown in the table for evaluation and analysis result:
Embodiment 3
First prepare filter stick particulate additive: get the removal of impurities of 5KG oak bark dry after physical mechanical pulverize, 80～120 object particles are got in screening, and to obtain oak bark powder for subsequent use; Getting 3KG waste tobacco leaf and offal (each 1.5KG) pulverizing grinding gets lower than 200 order fine powders for subsequent use; Oak bark particle and Discarded Tobacco powder are mixed to obtain to dry mixed powder according to a certain weight ratio; Get appropriate modified starch and cloud and mist absolute oil, Megastigmatrienone and be dissolved in suitable quantity of water and be configured to the certain density aqueous solution, wherein the mass ratio of oak bark powder, Discarded Tobacco powder, modified starch, cloud and mist absolute oil, Megastigmatrienone is 100:10:8:0.5:0.1; Powder and aqueous solution are stirred and be configured to certain density slurry; The slurry preparing is entered to spray dryer and spray dryly, control pellet moisture 6～12wt%, the particle screening obtaining is got to 30～60 order particles and obtain required functional form filter stick additive.The filter stick additive of preparation is propped up and evenly made an addition in cigarette filter rod tow with 1mg/, make after filter stick, further with the compound binary filter stick of cellulose acetate filter rod, then make cigarette.Detect analysis and show, this additive has filter stick and processes suitable hardness and toughness, reduces tar content 1.2mg/ in cigarette mainstream flue gas and props up, and has obvious flavouring effect simultaneously.
The binary compound filter candle that adopts the present embodiment to prepare is made to cigarette and common fiber tow filter rods cigarette, transfer to specialized review person to smoke panel test, it is as shown in the table for evaluation and analysis result:
Claims (17)
1. the application of oak bark, is characterized in that, is applied to the tar content reducing in cigarette smoke using oak bark as cigarette filter rod adding ingredient.
2. application as claimed in claim 1, it is characterized in that, described oak bark is ground into powder and tobacco leaf and/or offal powder, binding agent and flavouring essence for tobacco 100:(5～40 in mass ratio): (1～10): (0.1～1) granulation thing additive, is added in cigarette filter rod tow.
3. application as claimed in claim 2, is characterized in that, described particle additive particle diameter is 20～80 orders.
4. application as claimed in claim 3, is characterized in that, described particle additive particle diameter is 30～60 orders.
5. application as claimed in claim 2, is characterized in that, described tobacco leaf and/or offal powder diameter are for being not more than 200 orders.
6. application as claimed in claim 2, is characterized in that, described binding agent is one or more in modified starch, shitosan, sodium alginate, pectin.
7. application as claimed in claim 2, is characterized in that, described flavouring essence for tobacco is one or more in tobacco extract, cloud and mist absolute oil, methyl cyclopentenyl ketone, Megastigmatrienone.
8. the application as described in claim 2～5 any one, is characterized in that, described oak bark powder diameter is 80～120 orders.
9. a functional form filter stick additive, is characterized in that, by following mass parts component by solution mix, dry composite forms:
100 parts, oak bark powder;
5～40 parts, tobacco leaf and/or offal powder;
1～10 part of binding agent;
0.1～1 part of flavouring essence for tobacco.
10. additive as claimed in claim 9, is characterized in that, described binding agent is one or more in modified starch, shitosan, sodium alginate, pectin.
11. additives as claimed in claim 9, is characterized in that, described flavouring essence for tobacco is one or more in tobacco extract, cloud and mist absolute oil, methyl cyclopentenyl ketone, Megastigmatrienone.
The application of 12. 1 kinds of additives as described in claim 9～11 any one, is characterized in that, described additive is added on and in cigarette filter rod, is applied to the tar content reducing in cigarette smoke flavouring and flue gas.
13. application as claimed in claim 12, is characterized in that, described additive is added in cigarette filter rod tow.
14. application as claimed in claim 13, is characterized in that, the addition of described additive in cigarette filter rod tow is 1mg/mm～3mg/mm.
The preparation method of 15. 1 kinds of additives as described in claim 9～11 any one, it is characterized in that, be after 80～120 object oak bark powder and granularity are not more than 200 object tobacco leaves and/or offal powder and mix by granularity, again further and be dissolved with the aqueous solution of binding agent and flavouring essence for tobacco, obtain slurry; By gained slurry spray dry after, the sieve that sieves is got sieve 20～80 order particles, to obtain final product.
16. as the preparation method of claim 15, it is characterized in that, the described sieve that sieves is got 30～60 order particles.
17. as the preparation method of claim 15, it is characterized in that, described spray drying control system pellet moisture mass content is 6%～12%.
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| CN201410076513.0A CN103876284B (en) | 2014-03-04 | 2014-03-04 | The application and a kind of functional form filter stick additive and its preparation method and application of oak bark |
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| CN201410076513.0A CN103876284B (en) | 2014-03-04 | 2014-03-04 | The application and a kind of functional form filter stick additive and its preparation method and application of oak bark |
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| CN103876284A true CN103876284A (en) | 2014-06-25 |
| CN103876284B CN103876284B (en) | 2015-12-02 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105996123A (en) * | 2016-05-27 | 2016-10-12 | 阜阳卷烟材料厂 | Cigarette filter stick for reducing release quantity of crotonaldehyde in smoke gas |
| CN109123773A (en) * | 2017-06-28 | 2019-01-04 | 湖南中烟工业有限责任公司 | It is a kind of with mend Xiang Gong can cigarette filter rod, and its preparation method and application |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110250565A (en) * | 2019-06-10 | 2019-09-20 | 江西中烟工业有限责任公司 | A kind of plant granule perfume (or spice) pearl and the preparation method and application thereof |
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| US413036A (en) * | 1889-10-15 | William demuth | ||
| US2920629A (en) * | 1958-04-03 | 1960-01-12 | Wallace A Erickson & Co | Filtration of tobacco smoke |
| US3297041A (en) * | 1965-03-15 | 1967-01-10 | American Filtrona Corp | Tobacco smoke filter or the like |
| US3332427A (en) * | 1964-11-25 | 1967-07-25 | Istituto Chemioterapico | Product and process for filtering tobacco smoke |
| US20050076928A1 (en) * | 2003-10-10 | 2005-04-14 | Hu Peter H.L. | Cigarette filter |
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2014
- 2014-03-04 CN CN201410076513.0A patent/CN103876284B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US413036A (en) * | 1889-10-15 | William demuth | ||
| US2920629A (en) * | 1958-04-03 | 1960-01-12 | Wallace A Erickson & Co | Filtration of tobacco smoke |
| US3332427A (en) * | 1964-11-25 | 1967-07-25 | Istituto Chemioterapico | Product and process for filtering tobacco smoke |
| US3297041A (en) * | 1965-03-15 | 1967-01-10 | American Filtrona Corp | Tobacco smoke filter or the like |
| US20050076928A1 (en) * | 2003-10-10 | 2005-04-14 | Hu Peter H.L. | Cigarette filter |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105996123A (en) * | 2016-05-27 | 2016-10-12 | 阜阳卷烟材料厂 | Cigarette filter stick for reducing release quantity of crotonaldehyde in smoke gas |
| CN109123773A (en) * | 2017-06-28 | 2019-01-04 | 湖南中烟工业有限责任公司 | It is a kind of with mend Xiang Gong can cigarette filter rod, and its preparation method and application |
| CN109123773B (en) * | 2017-06-28 | 2020-01-31 | 湖南中烟工业有限责任公司 | cigarette filter stick with fragrance supplementing function, and preparation method and application thereof |
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| CN103876284B (en) | 2015-12-02 |
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