CN104725525B - 一种魔芋胶的制备方法 - Google Patents
一种魔芋胶的制备方法 Download PDFInfo
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- CN104725525B CN104725525B CN201510177116.7A CN201510177116A CN104725525B CN 104725525 B CN104725525 B CN 104725525B CN 201510177116 A CN201510177116 A CN 201510177116A CN 104725525 B CN104725525 B CN 104725525B
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- Prior art keywords
- konjac
- rhizoma amorphophalli
- ethanol solution
- fine powder
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- 229920002752 Konjac Polymers 0.000 title claims abstract description 43
- 235000010485 konjac Nutrition 0.000 title claims abstract description 40
- 241001312219 Amorphophallus konjac Species 0.000 title claims abstract description 36
- 235000001206 Amorphophallus rivieri Nutrition 0.000 title claims abstract description 36
- 239000000252 konjac Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000003292 glue Substances 0.000 title abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 63
- 239000000843 powder Substances 0.000 claims abstract description 33
- 239000000126 substance Substances 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 17
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000005406 washing Methods 0.000 claims abstract description 10
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 6
- 229930195725 Mannitol Natural products 0.000 claims abstract description 6
- 239000000594 mannitol Substances 0.000 claims abstract description 6
- 235000010355 mannitol Nutrition 0.000 claims abstract description 6
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 239000001103 potassium chloride Substances 0.000 claims abstract description 4
- 235000011164 potassium chloride Nutrition 0.000 claims abstract description 4
- 239000000084 colloidal system Substances 0.000 claims description 20
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 16
- 229920002581 Glucomannan Polymers 0.000 claims description 15
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 229940046240 glucomannan Drugs 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 14
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 10
- 239000012065 filter cake Substances 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 9
- 238000010008 shearing Methods 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 239000007921 spray Substances 0.000 claims description 7
- 238000007654 immersion Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000002604 ultrasonography Methods 0.000 claims description 6
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical class [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 5
- 239000004227 calcium gluconate Substances 0.000 claims description 5
- 229960004494 calcium gluconate Drugs 0.000 claims description 5
- 235000013927 calcium gluconate Nutrition 0.000 claims description 5
- NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 claims description 5
- 230000014759 maintenance of location Effects 0.000 claims description 5
- 235000005074 zinc chloride Nutrition 0.000 claims description 5
- 239000011592 zinc chloride Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims 1
- 229930013930 alkaloid Natural products 0.000 abstract description 12
- 150000003797 alkaloid derivatives Chemical class 0.000 abstract description 12
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 2
- 238000009210 therapy by ultrasound Methods 0.000 abstract description 2
- 235000019441 ethanol Nutrition 0.000 abstract 3
- 238000005086 pumping Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 24
- 238000002137 ultrasound extraction Methods 0.000 description 5
- 238000000227 grinding Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 102000030523 Catechol oxidase Human genes 0.000 description 2
- 108010031396 Catechol oxidase Proteins 0.000 description 2
- 244000205754 Colocasia esculenta Species 0.000 description 2
- 235000006481 Colocasia esculenta Nutrition 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 235000018102 proteins Nutrition 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229960005069 calcium Drugs 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 210000003701 histiocyte Anatomy 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 229940025902 konjac mannan Drugs 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- -1 receive Chemical compound 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
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- Preparation Of Fruits And Vegetables (AREA)
Abstract
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CN201510177116.7A CN104725525B (zh) | 2015-04-15 | 2015-04-15 | 一种魔芋胶的制备方法 |
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105192627B (zh) * | 2015-09-29 | 2019-03-29 | 湖南大湘西魔芋有限公司 | 一种魔芋米及其生产方法 |
CN105175574A (zh) * | 2015-10-16 | 2015-12-23 | 吉林大学 | 啫喱状魔芋葡甘聚糖的制备方法和应用 |
CN107141368A (zh) * | 2017-06-21 | 2017-09-08 | 安康市巴山佳芋食品有限公司 | 一种魔芋中葡甘露聚糖的提取方法 |
CN108354103A (zh) * | 2018-02-09 | 2018-08-03 | 陕西巴山佳芋大健康产业开发有限公司 | 一种含有鲜魔芋活性物质的饮品、制备方法及其应用 |
CN110305372A (zh) * | 2019-07-06 | 2019-10-08 | 李光宽 | 一种魔芋葡甘聚糖耐高温食品包装薄膜及其制备方法 |
CN111345428A (zh) * | 2020-03-24 | 2020-06-30 | 河北喜之郎食品有限公司 | 一种魔芋胶及其制备方法 |
CN112369614A (zh) * | 2020-10-28 | 2021-02-19 | 黑龙江中医药大学 | 一种糖尿病临床营养组合物及其制备方法 |
CN113974202B (zh) * | 2021-10-25 | 2023-09-01 | 深圳市真味生物科技有限公司 | 一种环保型电子雾化液增稠剂及其制备方法 |
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JP2949049B2 (ja) * | 1995-03-28 | 1999-09-13 | 株式会社関越物産 | 脱臭したコンニャク粉の製造方法 |
CN101869231B (zh) * | 2010-06-04 | 2012-07-25 | 西南大学 | 消除魔芋粉中生物碱的方法 |
CN102090588B (zh) * | 2010-12-20 | 2012-10-03 | 湖南大湘西魔芋有限公司 | 一种魔芋脱毒及生产魔芋脆片的方法 |
CN103804510A (zh) * | 2012-11-05 | 2014-05-21 | 安康市龙飞魔芋食品有限公司 | 一种无硫魔芋胶的制备方法 |
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Inventor after: Zhang Zu Inventor before: Chen Zhonghui |
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TA01 | Transfer of patent application right |
Effective date of registration: 20170328 Address after: 362600 Fujian City, Quanzhou province Yongchun County, a town of Lushan Mountain village, No. 8 Applicant after: Zhang Zu Address before: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Effective date of registration: 20170328 Address after: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: 610000 Sichuan, Chengdu, Chenghua District No. 1 East Ring Road, No. two, No. 126 Applicant before: CHENGDU ZHENYING PRECISION INDUSTRY MECHANICAL AND ELECTRICAL EQUIPMENT CO.,LTD. |
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TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20181214 Address after: 442300 Jintongling Industrial Park, Zhuxi County, Shiyan City, Hubei Province Patentee after: HUBEI CURE THE ZITHER KONJAC TECHNOLOGY Co.,Ltd. Address before: 362600 Lushan Village No. 8, Yidu Town, Yongchun County, Quanzhou City, Fujian Province Patentee before: Zhang Zu |
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CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: Gold Ridge Industrial Park of Shiyan city in 442300 Hubei County of Zhuxi Province Patentee after: Hubei lizeyuan Food Co.,Ltd. Address before: Gold Ridge Industrial Park of Shiyan city in 442300 Hubei County of Zhuxi Province Patentee before: HUBEI CURE THE ZITHER KONJAC TECHNOLOGY Co.,Ltd. |