CN104693833A - Preparation method of onion skin vegetable dye - Google Patents

Preparation method of onion skin vegetable dye Download PDF

Info

Publication number
CN104693833A
CN104693833A CN201510140693.9A CN201510140693A CN104693833A CN 104693833 A CN104693833 A CN 104693833A CN 201510140693 A CN201510140693 A CN 201510140693A CN 104693833 A CN104693833 A CN 104693833A
Authority
CN
China
Prior art keywords
dye
onion skin
onion
powder
skin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510140693.9A
Other languages
Chinese (zh)
Inventor
姚红亮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201510140693.9A priority Critical patent/CN104693833A/en
Publication of CN104693833A publication Critical patent/CN104693833A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources

Abstract

The invention provides a preparation method of an onion skin vegetable dye. The preparation method of the onion skin vegetable dye comprises the steps that firstly, onion skin is selected, cleaned and dried, and then the onion skin is crushed into plant powder of 30-80 meshes through a medicinal herb grinder; secondly, the plant powder is placed into an extraction pot, absolute ethyl alcohol is added into the extraction pot, the plant powder and the absolute ethyl alcohol are stirred for three hours to extract natural dye liquor, the proportion between the onion skin and the absolute ethyl alcohol is 1 to 10-20, and a dye liquid is obtained after filtering and slag removal are conducted; thirdly, the dye liquid is heated to reach 65-70 DEG C, the dye liquid is concentrated and the dye concentrated liquid with the concentration being 40%-50% is obtained; fourthly, reduction vaporization is conducted on the dye concentrated liquid through a rotary evaporator, and the dye concentrated liquid is volatilized and dried into natural dye powder. Raw materials of the onion skin vegetable dye are conveniently obtained, and the production process is simple. The prepared powder dye is convenient to transport, store and produce and high in production efficiency.

Description

A kind of preparation method of onion-skin vegetable dye
[technical field]
The present invention relates to chemical dyestuff technical field, be specifically related to a kind of preparation method of onion-skin vegetable dye.
[background technology]
Along with the raising of people's living standard, quality of life and living environment are more and more paid attention to, the biological degradation of natural plant dye self energy, do not affect environment, vegetable dye originating species, can expand plantation, continuous production, and it is applied to textile dyeing, there is significant Social benefit and economic benefit.Onion-skin contains pigment, is a kind of well Pure natural dye.
[summary of the invention]
The invention provides a kind of preparation method of onion-skin vegetable dye, make its technique simple, production efficiency is high, easily extracts the natural plant dye with dyeing function.
The technical scheme that the preparation method of a kind of onion-skin of the present invention vegetable dye adopts is: a kind of preparation method of onion-skin vegetable dye, comprise the following steps: step 1: choose onion-skin, clean, dry, then be ground into 30-80 object plant powder with medicinal herb grinder; Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue; Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%; Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder.
Further, Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
The invention has the beneficial effects as follows: raw material sources are convenient, and production technique is simple; Be prepared into powder dye, be convenient to transport, store and produce, production efficiency is high.
[embodiment]
Below in conjunction with specific embodiment, the invention will be further described.
The preparation method of a kind of onion-skin vegetable dye of the present invention, comprises the following steps:
Step 1: choose onion-skin, cleans, and dries, then is ground into 30-80 object plant powder with medicinal herb grinder;
Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue;
Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%;
Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder, wherein, Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
In sum, the invention has the beneficial effects as follows: raw material sources are convenient, and production technique is simple; Be prepared into powder dye, be convenient to transport, store and produce, production efficiency is high.

Claims (2)

1. a preparation method for onion-skin vegetable dye, is characterized in that comprising the following steps:
Step 1: choose onion-skin, cleans, and dries, then is ground into 30-80 object plant powder with medicinal herb grinder;
Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue;
Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%;
Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder.
2. the mixed planting method of a kind of cassava as claimed in claim 1 and soya bean, is characterized in that: Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
CN201510140693.9A 2015-03-30 2015-03-30 Preparation method of onion skin vegetable dye Pending CN104693833A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510140693.9A CN104693833A (en) 2015-03-30 2015-03-30 Preparation method of onion skin vegetable dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510140693.9A CN104693833A (en) 2015-03-30 2015-03-30 Preparation method of onion skin vegetable dye

Publications (1)

Publication Number Publication Date
CN104693833A true CN104693833A (en) 2015-06-10

Family

ID=53341402

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510140693.9A Pending CN104693833A (en) 2015-03-30 2015-03-30 Preparation method of onion skin vegetable dye

Country Status (1)

Country Link
CN (1) CN104693833A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312355A (en) * 2017-06-12 2017-11-03 暨南大学 The preparation and its application of purple skin Onion pigment
PL424683A1 (en) * 2018-02-26 2019-09-09 Geecs Spółka Akcyjna Method for obtaining extract from onion peel and the extract from onion peel obtained by this method
CN110791120A (en) * 2019-10-09 2020-02-14 五邑大学 Extraction method of onion skin dye liquor, onion skin dye liquor and application of onion skin dye liquor in protein textiles
CN113462192A (en) * 2021-07-01 2021-10-01 上海禧蓝纺织品有限公司 Extraction and dyeing method of plant dye and plant mordant

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01179666A (en) * 1988-01-06 1989-07-17 Binshiyoo:Kk Use of pigment extracted from onion skin
JPH01269470A (en) * 1988-04-21 1989-10-26 San Ei Chem Ind Ltd Coloring of seasoning and sauce in yellowish brown color
RU2001072C1 (en) * 1992-04-21 1993-10-15 Лариса Михайловна Ильина Method for obtaining dye from onion husks
CN102119993A (en) * 2011-03-07 2011-07-13 天津科技大学 Preparation method of onion extract, application of onion extract for prolonging life of Caenorhabditis elegans and food containing onion extract
CN103131207A (en) * 2011-11-25 2013-06-05 宋德臣 Ecological dye
CN104073022A (en) * 2014-06-26 2014-10-01 南通润启时装有限公司 Preparation and application of onion-skin natural dye

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01179666A (en) * 1988-01-06 1989-07-17 Binshiyoo:Kk Use of pigment extracted from onion skin
JPH01269470A (en) * 1988-04-21 1989-10-26 San Ei Chem Ind Ltd Coloring of seasoning and sauce in yellowish brown color
RU2001072C1 (en) * 1992-04-21 1993-10-15 Лариса Михайловна Ильина Method for obtaining dye from onion husks
CN102119993A (en) * 2011-03-07 2011-07-13 天津科技大学 Preparation method of onion extract, application of onion extract for prolonging life of Caenorhabditis elegans and food containing onion extract
CN103131207A (en) * 2011-11-25 2013-06-05 宋德臣 Ecological dye
CN104073022A (en) * 2014-06-26 2014-10-01 南通润启时装有限公司 Preparation and application of onion-skin natural dye

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吴素玲等: "洋葱黄酮类物质不同提取工艺的比较研究", 《安徽农业科学》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312355A (en) * 2017-06-12 2017-11-03 暨南大学 The preparation and its application of purple skin Onion pigment
PL424683A1 (en) * 2018-02-26 2019-09-09 Geecs Spółka Akcyjna Method for obtaining extract from onion peel and the extract from onion peel obtained by this method
CN110791120A (en) * 2019-10-09 2020-02-14 五邑大学 Extraction method of onion skin dye liquor, onion skin dye liquor and application of onion skin dye liquor in protein textiles
CN113462192A (en) * 2021-07-01 2021-10-01 上海禧蓝纺织品有限公司 Extraction and dyeing method of plant dye and plant mordant

Similar Documents

Publication Publication Date Title
CN104693833A (en) Preparation method of onion skin vegetable dye
CN103451022A (en) Method for integrally extracting volatile oil, polysaccharide and flavone from elsholtzia haichowensis sun
CN104164302A (en) Extraction method of gardenia jasminoides volatile oil
CN103665929A (en) Real silk dyeing process of pomegranate bark vegetable dye
CN105367679A (en) Green tea polysaccharide extraction method
CN102964866A (en) Method for extracting perilla color from perilla leaves
CN106176878A (en) The extracting method of Radix Codonopsis extract
CN103789086A (en) Luffa cylindrica seed oil and preparation method thereof
CN102911520A (en) Henna vegetable dye preparation method
CN103665928A (en) Method for preparing safflower plant dyestuff
CN102911521A (en) Preparation method of walnut skin vegetable dye
CN104861737B (en) A kind of preparation method of sophora flower vegetable colour
CN106977307A (en) A kind of chrysanthemum dedicated fertilizer
CN104120028A (en) Method for extracting passion fruit seed oil
CN105272824A (en) Preparation method of natural cinnamomum camphora aromatic material
CN110283153A (en) A kind of anthocyanidin of pomegranate and the extracting method of polyphenol
CN103756356A (en) Method for preparing madder vegetable dye
CN103756355A (en) Method for preparing pomegranate-bark vegetable dye
CN104367622A (en) Method for extracting alkaloids from herba leonuri
CN102516800A (en) Preparation method for walnut peel vegetable dye
CN103103812A (en) Natural green cotton fabric
CN106349737A (en) Preparation method of Salvia japonica Thunb. vegetable dye
CN106279455B (en) A kind of comprehensive method for extracting cordycepin and Cordyceps sinensis polysaccharide in Cordyceps militaris of aqueous two-phase
CN102516801A (en) Arnebia euchroma dye preparation method
CN106147287A (en) A kind of preparation method of leaf of Chinese ilex vegetable colour

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20150610