CN104651955A - Preparation method of prefabricated palm fiber material for cotton/palm fiber blending - Google Patents
Preparation method of prefabricated palm fiber material for cotton/palm fiber blending Download PDFInfo
- Publication number
- CN104651955A CN104651955A CN201510087160.9A CN201510087160A CN104651955A CN 104651955 A CN104651955 A CN 104651955A CN 201510087160 A CN201510087160 A CN 201510087160A CN 104651955 A CN104651955 A CN 104651955A
- Authority
- CN
- China
- Prior art keywords
- monofilament
- decatize
- process vessel
- once
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C1/00—Treatment of vegetable material
Landscapes
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
The invention discloses a preparation method of a prefabricated palm fiber material for cotton/palm fiber blending. The preparation method comprises the following steps: performing primary boiling-off and primary steaming to water, palm fibers, sodium hydroxide solution, kerosene, camellia oil, refining agent MRN and JFC to obtain primarily steamed palm fibers; then performing secondary boiling-off and secondary steaming to the water, sodium hydroxide solution, refining agent MOL-201, new synthetic fiber refining agent AV-SCOUR-81, chelating agent EDTA, kerosene, camellia oil and the primarily steamed palm fibers to obtain secondarily steamed palm fibers; standing the secondarily steamed palm fibers; mixing with the sodium hydroxide, hydrogen peroxide, stabilizer LTP-S128 and water to obtain bleached palm fibers; and then washing and bleaching the palm fibers twice with water at different temperatures, draining off and drying to obtain the prefabricated palm fiber material for cotton/palm fiber blending.
Description
Technical field
The present invention relates to monofilament field of material technology, particularly relate to a kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending.
Background technology
Oil palm, also known as African oil palm, it is the woody oily section in Palmae torrid zone plant, main distribution tropical and subtropical region, in China mainly in Taiwan, Hainan, the ground such as Yunnan extensively cultivates, its fruit oil content up to more than 50%, after the brown oil refinement of squeezing out, can make cheap, nutritious edible oil and fat, be a kind of plant having economic worth.But, accessory substance---empty shell after oil palm fruit oil expression, because processing mode is limited, but serious negative effect and the wasting of resources are caused to environment, at present, industrially mainly empty shell is processed into monofilament, be pressed into sheet material again to sell, but, this sheet material purposes is limited so the amount of digestion monofilament is less, therefore, studies further monofilament, utilize its cheap, antibacterial mothproof, elasticity is better, content of cellulose is abundant, the fluffy advantage such as tiny of profile, expands its value very urgent.There are some researches show, by after monofilament preliminary treatment with cotton blending, the material that blending can be made to obtain is while possessing the above-mentioned advantage of monofilament, and also possessing the advantages such as cotton regularity is high, cohesive force is good, can deep processing be the textile products such as cloth further; But monofilament because quality is comparatively hard, pliability is poor, and containing a large amount of oil, wax and impurity, proposes high requirement to processing procedure.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending, the prefabricated monofilament material softness that the present invention obtains, elastic force is high, pliability good, and gas permeability, antibacterial mothproof effect are good, can be used in cotton/monofilament blending.
The preparation method of a kind of prefabricated monofilament material for cotton/monofilament blending that the present invention proposes, comprises following steps:
S1, once boil de-: be the sodium hydroxide solution of 44-47wt% by weight by 100-120 part water, 30-35 part monofilament, 15-18 part mass fraction, 4-6 part kerosene, 1.5-1.8 part tea oil, 3-5 part refining agent MRN, 0.7-1 part JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 55-60min, and once boiling de-temperature is 95-98 DEG C;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, a steam temperature is 110-115 DEG C, and a steaming time is 30-33min;
S3, secondary boil de-: be the sodium hydroxide solution of 44-47wt% by weight by 100-120 part water, 10-13 part mass fraction, 2-2.5 part refining agent MOL-201,1.8-2.2 part shin-gosen refining agent AV-SCOUR-81,3.2-3.5 part chelating agent EDTA, 1.6-2 part kerosene, 0.5-0.8 part tea oil drops into the 3rd process vessel, raise the 3rd process vessel and contents temperature thereof to after 85-90 DEG C, drop into monofilament after a decatize, continuation rising the 3rd process vessel and contents temperature thereof, to 97-100 DEG C, obtain secondary and boil de-rear monofilament after insulation 1.5-2h;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 115-120 DEG C, and secondary steaming time is 35-40min;
S5, placement: monofilament after secondary decatize is placed under 25-28 DEG C of environment 10-12h obtain placing after monofilament;
S6, bleaching: by weight 4-7 part sodium chlorate, 0.2-0.5 part hydrogen peroxide, 1-3 part stabilizing agent LTP-S128 and 100-110 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature thereof to 96-100 DEG C, obtain bleaching rear monofilament after insulation 1-1.5h;
S7, post processing: rinse after bleaching after monofilament 3-5min with 55-60 DEG C of water, then with 17-20 DEG C of water flushing 8-10min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 60-65 DEG C, and drying time is 30-35min.
Preferably, in S1, the weight ratio of kerosene, tea oil, refining agent MRN, JFC is 4.5-5:1.6-1.7:3.5-4:0.8-0.9.
Preferably, in S2, the weight ratio of refining agent MOL-201, shin-gosen refining agent AV-SCOUR-81, chelating agent EDTA, kerosene, tea oil is 2.2-2.3:1.9-2.1:3.3-3.4:1.8-1.9:0.6-0.7.
Preferably, in S1, S3, stir once every 10-15min, each mixing time 2-3min.
Preferably, following steps are comprised:
S1, once boil de-: be the sodium hydroxide solution of 45-46wt% by weight by 108-112 part water, 32-33 part monofilament, 16-17 part mass fraction, 4.5-5 part kerosene, 1.6-1.7 part tea oil, 3.5-4 part refining agent MRN, 0.8-0.9 part JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 56-58min, and once boiling de-temperature is 96-97 DEG C;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, a steam temperature is 112-113 DEG C, and a steaming time is 31-32min;
S3, secondary boil de-: be the sodium hydroxide solution of 45-46wt% by weight by 108-115 part water, 11-12 part mass fraction, 2.2-2.3 part refining agent MOL-201,1.9-2.1 part shin-gosen refining agent AV-SCOUR-81,3.3-3.4 part chelating agent EDTA, 1.8-1.9 part kerosene, 0.6-0.7 part tea oil drops into the 3rd process vessel, raise the 3rd process vessel and contents temperature thereof to after 86-88 DEG C, drop into monofilament after a decatize, continuation rising the 3rd process vessel and contents temperature thereof, to 98-99 DEG C, obtain secondary and boil de-rear monofilament after insulation 1.6-1.8h;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 116-118 DEG C, and secondary steaming time is 36-38min;
S5, placement: monofilament after secondary decatize is placed under 26-27 DEG C of environment 10.5-11h obtain placing after monofilament;
S6, bleaching: by weight 5-6 part sodium chlorate, 0.3-0.4 part hydrogen peroxide, 1.5-2 part stabilizing agent LTP-S128 and 104-108 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature thereof to 97-98 DEG C, obtain bleaching rear monofilament after insulation 1.2-1.4h;
S7, post processing: rinse after bleaching after monofilament 3.5-4min with 56-57 DEG C of water, then with 18-19 DEG C of water flushing 8.5-9min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 61-62 DEG C, and drying time is 32-33min.
Above-mentioned S5 places in step, and solar irradiation should be avoided to be mapped to monofilament after secondary decatize.
The present invention adopts the PROCESS FOR TREATMENT monofilament of " two boil two steamings one puts a bleaching ", makes prefabricated monofilament material soft
Soft, elastic force is high, pliability good, and gas permeability, antibacterial mothproof effect are good, can be used in cotton/monofilament blending; S1 once boils in de-process, and sodium hydroxide solution, kerosene, tea oil, refining agent MRN, JFC can be with the use of, removes oil, the impurity of monofilament remained on surface, impels monofilament to tend to soft, pliable and tough; Wherein, in the alkaline environment that refining agent MRN is formed in the interpolation of sodium hydroxide solution, wetting, emulsification, washing monofilament, improve the pre-treatment quality of its internal fiber cellulose fiber, ensure softening and other follow-up quality; And kerosene, tea oil and penetrating agent JFC can mating reactions, reduce monofilament surface tension, penetrate into monofilament inside, impel monofilament to soften, prevent monofilament from uniting, be easy to and cotton blending; During S3 boils for bis-times and takes off, sodium hydroxide solution, refining agent MOL-201, shin-gosen refining agent AV-SCOUR-81, chelating agent EDTA, kerosene, tea oil can soften monofilament further, make it possess the quality of excellent elasticity, pliability and softness; Wherein, refining agent MOL-201 can have excellent removal to oils and prevent it from polluting again, enhances the wettability on monofilament surface simultaneously, makes prefabricated monofilament material more be easy to cotton/monofilament blending, and the material gas permeable poisture-penetrability also making blending obtained is excellent; And shin-gosen refining agent AV-SCOUR-81 has efficient infiltration, emulsification and peptizaiton to the oil layer in monofilament, significantly reduce the content of oil, wax in monofilament, and then promote that monofilament possesses good elasticity and softness; And the interpolation of chelating agent EDTA, its surface can be used to have a large amount of carboxyls, amino chelating position, stable water soluble chelate compound is generated with heavy metal ion such as the iron contained in monofilament, calcium, magnesium, thus shelter each metal ion species contained in monofilament, impel soft, the easy blending of monofilament, avoid occurring spot on cotton/monofilament blended material surface; And after S1, S3 step, carry out a decatize and secondary decatize respectively, and place after secondary decatize, monofilament surface oil lipid layer and wax coat can be destroyed, monofilament is impelled at high temperature to soften, make the material added in S1, S3 infiltrate through monofilament inside further simultaneously, improve softness and the elasticity of monofilament, the whiteness of monofilament can also be increased, be convenient to the processing such as later stage dyeing; And sodium chlorate, hydrogen peroxide coordinate as bleaching agent and under the protection of stabilizing agent LTP-S128, can make that whiteness of the present invention is good, impurity is few, be convenient to post-production.
Detailed description of the invention
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The preparation method of a kind of prefabricated monofilament material for cotton/monofilament blending that the present invention proposes, comprises following steps:
S1, once boil de-: be the sodium hydroxide solution of 44wt% by weight by 120 parts of water, 30 parts of monofilaments, 18 parts of mass fractions, 6 parts of kerosene, 1.5 parts of tea oil, 5 parts of refining agent MRN, 0.7 part of JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 60min, and once boiling de-temperature is 95 DEG C; Wherein, stir once every 15min, each mixing time 2min;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, one time steam temperature is 115 DEG C, and a steaming time is 30min;
S3, secondary boil de-: be the sodium hydroxide solution of 47wt% by 120 parts of water, 10 parts of mass fractions by weight, 2 parts of refining agent MOL-201,2.2 parts of shin-gosen refining agent AV-SCOUR-81,3.2 parts of chelating agent EDTA, 2 parts of kerosene, 0.5 part of tea oil drop into the 3rd process vessels, after raising the 3rd process vessel and contents temperature to 90 thereof DEG C, drop into monofilament after a decatize, continue rising the 3rd process vessel and contents temperature to 97 DEG C thereof, obtain secondary after insulation 2h and boil de-rear monofilament; Wherein, stir once every 10min, each mixing time 3min;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 115 DEG C, and secondary steaming time is 40min;
S5, placement: monofilament after secondary decatize is placed under 25 DEG C of environment 12h obtain placing after monofilament; , wherein, solar irradiation should be avoided to be mapped to monofilament after secondary decatize.
S6, bleaching: by weight 4 parts of sodium chlorate, 0.5 part of hydrogen peroxide, 1 part of stabilizing agent LTP-S128 and 110 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature to 96 DEG C thereof, obtain bleaching rear monofilament after insulation 1.5h;
S7, post processing: rinse after bleaching after monofilament 5min with 55 DEG C of water, then with 17 DEG C of water flushing 10min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 60 DEG C, and drying time is 35min.
Embodiment 2
The preparation method of a kind of prefabricated monofilament material for cotton/monofilament blending that the present invention proposes, comprises following steps:
S1, once boil de-: be the sodium hydroxide solution of 47wt% by weight by 100 parts of water, 35 parts of monofilaments, 15 parts of mass fractions, 4 parts of kerosene, 1.8 parts of tea oil, 3 parts of refining agent MRN, 1 part of JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 55min, and once boiling de-temperature is 98 DEG C; Wherein, stir once every 10min, each mixing time 3min;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, one time steam temperature is 110 DEG C, and a steaming time is 33min;
S3, secondary boil de-: be the sodium hydroxide solution of 44wt% by 100 parts of water, 13 parts of mass fractions by weight, 2.5 parts of refining agent MOL-201,1.8 parts of shin-gosen refining agent AV-SCOUR-81,3.5 parts of chelating agent EDTA, 1.6 parts of kerosene, 0.8 part of tea oil drop into the 3rd process vessels, after raising the 3rd process vessel and contents temperature to 85 thereof DEG C, drop into monofilament after a decatize, continue rising the 3rd process vessel and contents temperature to 100 DEG C thereof, obtain secondary after insulation 1.5h and boil de-rear monofilament; Wherein, stir once every 15min, each mixing time 2min;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 120 DEG C, and secondary steaming time is 35min;
S5, placement: monofilament after secondary decatize is placed under 28 DEG C of environment 10h obtain placing after monofilament; Wherein, solar irradiation should be avoided to be mapped to monofilament after secondary decatize;
S6, bleaching: by weight 7 parts of sodium chlorate, 0.2 part of hydrogen peroxide, 3 parts of stabilizing agent LTP-S128 and 100 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature to 100 DEG C thereof, obtain bleaching rear monofilament after insulation 1h;
S7, post processing: rinse after bleaching after monofilament 3min with 60 DEG C of water, then with 20 DEG C of water flushing 8min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 65 DEG C, and drying time is 30min.
Embodiment 3
The preparation method of a kind of prefabricated monofilament material for cotton/monofilament blending that the present invention proposes, comprises following steps:
S1, once boil de-: be the sodium hydroxide solution of 45wt% by weight by 112 parts of water, 32 parts of monofilaments, 17 parts of mass fractions, 5 parts of kerosene, 1.6 parts of tea oil, 4 parts of refining agent MRN, 0.8 part of JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 58min, and once boiling de-temperature is 96 DEG C; Wherein, stir once every 13min, each mixing time 2.5min;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, one time steam temperature is 113 DEG C, and a steaming time is 31min;
S3, secondary boil de-: be the sodium hydroxide solution of 46wt% by 115 parts of water, 11 parts of mass fractions by weight, 2.2 parts of refining agent MOL-201,2.1 parts of shin-gosen refining agent AV-SCOUR-81,3.3 parts of chelating agent EDTA, 1.9 parts of kerosene, 0.6 part of tea oil drop into the 3rd process vessels, after raising the 3rd process vessel and contents temperature to 88 thereof DEG C, drop into monofilament after a decatize, continue rising the 3rd process vessel and contents temperature to 98 DEG C thereof, obtain secondary after insulation 1.8h and boil de-rear monofilament; Wherein, stir once every 12min, each mixing time 3min;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 116 DEG C, and secondary steaming time is 38min;
S5, placement: monofilament after secondary decatize is placed under 26 DEG C of environment 11h obtain placing after monofilament; Wherein, solar irradiation should be avoided to be mapped to monofilament after secondary decatize;
S6, bleaching: by weight 5 parts of sodium chlorate, 0.4 part of hydrogen peroxide, 1.5 parts of stabilizing agent LTP-S128 and 108 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature to 97 DEG C thereof, obtain bleaching rear monofilament after insulation 1.4h;
S7, post processing: rinse after bleaching after monofilament 4min with 56 DEG C of water, then with 18 DEG C of water flushing 9min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 61 DEG C, and drying time is 33min.
Embodiment 4
The preparation method of a kind of prefabricated monofilament material for cotton/monofilament blending that the present invention proposes, comprises following steps:
S1, once boil de-: be the sodium hydroxide solution of 46wt% by weight by 108 parts of water, 33 parts of monofilaments, 16 parts of mass fractions, 4.5 parts of kerosene, 1.7 parts of tea oil, 3.5 parts of refining agent MRN, 0.9 part of JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 56min, and once boiling de-temperature is 97 DEG C; Wherein, stir once every 12min, each mixing time 3min;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, one time steam temperature is 112 DEG C, and a steaming time is 32min;
S3, secondary boil de-: be the sodium hydroxide solution of 45wt% by 108 parts of water, 12 parts of mass fractions by weight, 2.3 parts of refining agent MOL-201,1.9 parts of shin-gosen refining agent AV-SCOUR-81,3.4 parts of chelating agent EDTA, 1.8 parts of kerosene, 0.7 part of tea oil drop into the 3rd process vessels, after raising the 3rd process vessel and contents temperature to 86 thereof DEG C, drop into monofilament after a decatize, continue rising the 3rd process vessel and contents temperature to 99 DEG C thereof, obtain secondary after insulation 1.6h and boil de-rear monofilament; Wherein, stir once every 13min, each mixing time 2.5min;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 118 DEG C, and secondary steaming time is 36min;
S5, placement: monofilament after secondary decatize is placed under 27 DEG C of environment 10.5h obtain placing after monofilament; Wherein, solar irradiation should be avoided to be mapped to monofilament after secondary decatize;
S6, bleaching: by weight 6 parts of sodium chlorate, 0.3 part of hydrogen peroxide, 2 parts of stabilizing agent LTP-S128 and 104 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature to 98 DEG C thereof, obtain bleaching rear monofilament after insulation 1.2h;
S7, post processing: rinse after bleaching after monofilament 3.5min with 57 DEG C of water, then with 19 DEG C of water flushing 8.5min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 62 DEG C, and drying time is 32min.
The present invention propose the above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (5)
1., for a preparation method for the prefabricated monofilament material of cotton/monofilament blending, it is characterized in that, comprise following steps:
S1, once boil de-: be the sodium hydroxide solution of 44-47wt% by weight by 100-120 part water, 30-35 part monofilament, 15-18 part mass fraction, 4-6 part kerosene, 1.5-1.8 part tea oil, 3-5 part refining agent MRN, 0.7-1 part JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 55-60min, and once boiling de-temperature is 95-98 DEG C;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, a steam temperature is 110-115 DEG C, and a steaming time is 30-33min;
S3, secondary boil de-: be the sodium hydroxide solution of 44-47wt% by weight by 100-120 part water, 10-13 part mass fraction, 2-2.5 part refining agent MOL-201,1.8-2.2 part shin-gosen refining agent AV-SCOUR-81,3.2-3.5 part chelating agent EDTA, 1.6-2 part kerosene, 0.5-0.8 part tea oil drops into the 3rd process vessel, raise the 3rd process vessel and contents temperature thereof to after 85-90 DEG C, drop into monofilament after a decatize, continuation rising the 3rd process vessel and contents temperature thereof, to 97-100 DEG C, obtain secondary and boil de-rear monofilament after insulation 1.5-2h;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 115-120 DEG C, and secondary steaming time is 35-40min;
S5, placement: monofilament after secondary decatize is placed under 25-28 DEG C of environment 10-12h obtain placing after monofilament;
S6, bleaching: by weight 4-7 part sodium chlorate, 0.2-0.5 part hydrogen peroxide, 1-3 part stabilizing agent LTP-S128 and 100-110 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature thereof to 96-100 DEG C, obtain bleaching rear monofilament after insulation 1-1.5h;
S7, post processing: rinse after bleaching after monofilament 3-5min with 55-60 DEG C of water, then with 17-20 DEG C of water flushing 8-10min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 60-65 DEG C, and drying time is 30-35min.
2. according to claim 1 for the preparation method of the prefabricated monofilament material of cotton/monofilament blending, it is characterized in that, in S1, the weight ratio of kerosene, tea oil, refining agent MRN, JFC is 4.5-5:1.6-1.7:3.5-4:0.8-0.9.
3. according to claim 1 or 2 for the preparation method of the prefabricated monofilament material of cotton/monofilament blending, it is characterized in that, in S2, the weight ratio of refining agent MOL-201, shin-gosen refining agent AV-SCOUR-81, chelating agent EDTA, kerosene, tea oil is 2.2-2.3:1.9-2.1:3.3-3.4:1.8-1.9:0.6-0.7.
4. according to any one of claim 1-3 for the preparation method of the prefabricated monofilament material of cotton/monofilament blending, it is characterized in that, in S1, S3, every 10-15min stir once, each mixing time 2-3min.
5. according to any one of claim 1-5 for the preparation method of the prefabricated monofilament material of cotton/monofilament blending, it is characterized in that, comprise following steps:
S1, once boil de-: be the sodium hydroxide solution of 45-46wt% by weight by 108-112 part water, 32-33 part monofilament, 16-17 part mass fraction, 4.5-5 part kerosene, 1.6-1.7 part tea oil, 3.5-4 part refining agent MRN, 0.8-0.9 part JFC add in the first process vessel once boil de-once boiled de-after monofilament, once boiling the de-time is 56-58min, and once boiling de-temperature is 96-97 DEG C;
S2, a decatize: will once boil de-after monofilament drop in the second process vessel and carry out a decatize and obtain monofilament after a decatize, a steam temperature is 112-113 DEG C, and a steaming time is 31-32min;
S3, secondary boil de-: be the sodium hydroxide solution of 45-46wt% by weight by 108-115 part water, 11-12 part mass fraction, 2.2-2.3 part refining agent MOL-201,1.9-2.1 part shin-gosen refining agent AV-SCOUR-81,3.3-3.4 part chelating agent EDTA, 1.8-1.9 part kerosene, 0.6-0.7 part tea oil drops into the 3rd process vessel, raise the 3rd process vessel and contents temperature thereof to after 86-88 DEG C, drop into monofilament after a decatize, continuation rising the 3rd process vessel and contents temperature thereof, to 98-99 DEG C, obtain secondary and boil de-rear monofilament after insulation 1.6-1.8h;
S4, secondary decatize: secondary is boiled de-after monofilament drop in the second process vessel and carry out secondary decatize and obtain monofilament after secondary decatize, secondary steam temperature is 116-118 DEG C, and secondary steaming time is 36-38min;
S5, placement: monofilament after secondary decatize is placed under 26-27 DEG C of environment 10.5-11h obtain placing after monofilament;
S6, bleaching: by weight 5-6 part sodium chlorate, 0.3-0.4 part hydrogen peroxide, 1.5-2 part stabilizing agent LTP-S128 and 104-108 part water are added the 4th process vessel, monofilament after placing is dropped into after stirring, raise the 4th process vessel and contents temperature thereof to 97-98 DEG C, obtain bleaching rear monofilament after insulation 1.2-1.4h;
S7, post processing: rinse after bleaching after monofilament 3.5-4min with 56-57 DEG C of water, then with 18-19 DEG C of water flushing 8.5-9min, drain the prefabricated monofilament material that rear drying obtains for cotton/monofilament blending, baking temperature is 61-62 DEG C, and drying time is 32-33min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510087160.9A CN104651955B (en) | 2015-02-25 | 2015-02-25 | A kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510087160.9A CN104651955B (en) | 2015-02-25 | 2015-02-25 | A kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104651955A true CN104651955A (en) | 2015-05-27 |
| CN104651955B CN104651955B (en) | 2016-07-06 |
Family
ID=53243576
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510087160.9A Active CN104651955B (en) | 2015-02-25 | 2015-02-25 | A kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104651955B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105483837A (en) * | 2016-01-20 | 2016-04-13 | 沈习军 | Method for deep processing of oil palm fiber |
| CN107083573A (en) * | 2017-06-07 | 2017-08-22 | 思南县唯山棕制品厂 | A kind of monofilament method of modifying |
| CN107164807A (en) * | 2017-06-12 | 2017-09-15 | 思南县唯山棕制品厂 | It is a kind of to improve the method for monofilament toughness |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004018747A1 (en) * | 2002-08-23 | 2004-03-04 | Interactive Star Sdn Bhd | Fibre mat |
| CN101469454A (en) * | 2007-12-27 | 2009-07-01 | 南方汇通股份有限公司 | Method for extracting fiber from oil palm fruit clusters and obtained fiber |
| CN101476164A (en) * | 2008-12-19 | 2009-07-08 | 南方汇通股份有限公司 | Oil palm fiber treatment method |
| CN101638858A (en) * | 2008-12-26 | 2010-02-03 | 青岛智森科技发展有限公司 | New pulping process of chemical mechanical pulp (CEMP) employing oil palm EFB high concentration extrusion displacement method |
| CN102409410A (en) * | 2011-08-24 | 2012-04-11 | 李超 | Novel bamboo palm fiber extraction process |
| CN103556249A (en) * | 2013-10-24 | 2014-02-05 | 恒天海龙股份有限公司 | Palm viscose and preparation method thereof |
| CN104195650A (en) * | 2014-08-21 | 2014-12-10 | 浙江省义乌市亨德利毛纺有限公司 | Production technology of spinnability soft coconut shell fine fibers and application of fiber product |
-
2015
- 2015-02-25 CN CN201510087160.9A patent/CN104651955B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004018747A1 (en) * | 2002-08-23 | 2004-03-04 | Interactive Star Sdn Bhd | Fibre mat |
| CN101469454A (en) * | 2007-12-27 | 2009-07-01 | 南方汇通股份有限公司 | Method for extracting fiber from oil palm fruit clusters and obtained fiber |
| CN101476164A (en) * | 2008-12-19 | 2009-07-08 | 南方汇通股份有限公司 | Oil palm fiber treatment method |
| CN101638858A (en) * | 2008-12-26 | 2010-02-03 | 青岛智森科技发展有限公司 | New pulping process of chemical mechanical pulp (CEMP) employing oil palm EFB high concentration extrusion displacement method |
| CN102409410A (en) * | 2011-08-24 | 2012-04-11 | 李超 | Novel bamboo palm fiber extraction process |
| CN103556249A (en) * | 2013-10-24 | 2014-02-05 | 恒天海龙股份有限公司 | Palm viscose and preparation method thereof |
| CN104195650A (en) * | 2014-08-21 | 2014-12-10 | 浙江省义乌市亨德利毛纺有限公司 | Production technology of spinnability soft coconut shell fine fibers and application of fiber product |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105483837A (en) * | 2016-01-20 | 2016-04-13 | 沈习军 | Method for deep processing of oil palm fiber |
| CN107083573A (en) * | 2017-06-07 | 2017-08-22 | 思南县唯山棕制品厂 | A kind of monofilament method of modifying |
| CN107083573B (en) * | 2017-06-07 | 2019-10-15 | 思南县唯一山棕制品厂 | A kind of monofilament method of modifying |
| CN107164807A (en) * | 2017-06-12 | 2017-09-15 | 思南县唯山棕制品厂 | It is a kind of to improve the method for monofilament toughness |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104651955B (en) | 2016-07-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101509168B (en) | Elastic towel of untwisted yarn and processing method | |
| CN104651955B (en) | A kind of preparation method of the prefabricated monofilament material for cotton/monofilament blending | |
| CN104651998B (en) | Preparation method for high-toughness monofilament blended cotton yarn | |
| CN104264478B (en) | A kind of bamboo fiber towel goods prepared by modified adhesive | |
| Wang et al. | One-step processing and bleaching of mechanically separated kenaf fibers: Effects on physical and chemical properties | |
| CN101250757B (en) | Technique for ramie degumming | |
| CN106142272A (en) | A kind of wicker anticorrosion sofening treatment method | |
| CN107858863A (en) | A kind of preparation method of unbleached paper | |
| CN101513817B (en) | Method for manufacturing corn leaf plane calligraphy and painting | |
| CN103882733A (en) | Natural environment-friendly tea staining technology for bedding articles and underwear | |
| CN105821487B (en) | Production method of banana stem fiber refined-dry ramie | |
| CN104342925B (en) | A kind of preparation method of the bamboo cotton towel cloth containing environmental protection binding agent | |
| CN107955225A (en) | A kind of latex product for natural emulsion brassiere and preparation method thereof | |
| CN107558236A (en) | A kind of alkaline-resisting high temperature resistant film of cold water solubles and preparation method thereof | |
| CN105147762A (en) | Soybean oil emulsion | |
| CN108714952A (en) | A kind of method of discarded bamboo stick bamboo chip recycling processing | |
| CN104924397A (en) | Rattan softening method | |
| CN106592229A (en) | Cashmere fabric anti-pilling finishing liquor containing modified sericin and preparation method of finishing liquor | |
| CN104264461A (en) | Preparation method of flame-retardant photochromic silk fabric | |
| CN103938280A (en) | Machine-processed silk floss degumming method | |
| CN107584605A (en) | A kind of method of discarded bamboo stick bamboo chip recovery processing | |
| CN104630905A (en) | Fibrilia oil supply emulsion and preparation method thereof | |
| CN104403853A (en) | Brightening laundry detergent | |
| CN103410002B (en) | Woolen sweater treating fluid containing polyoxyethylene glycol bisstearate | |
| CN108865502A (en) | A kind of detergent and preparation method thereof for leather and fur products |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |