CN104611838A - Method for producing silk mask base cloth through cocoons and silk mask - Google Patents
Method for producing silk mask base cloth through cocoons and silk mask Download PDFInfo
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- CN104611838A CN104611838A CN201510040948.4A CN201510040948A CN104611838A CN 104611838 A CN104611838 A CN 104611838A CN 201510040948 A CN201510040948 A CN 201510040948A CN 104611838 A CN104611838 A CN 104611838A
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4266—Natural fibres not provided for in group D04H1/425
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
The invention discloses a method for producing silk mask base cloth through cocoons. The method comprises the following steps that (1), cocoon washing is performed, namely, the cocoons are washed with clean water to remove dust and debris; (2), wetting is performed, namely, the washed cocoons are soaked in water to be sufficiently wet; (3), alkali soaking is performed, namely, the wet cocoons are evenly placed in a steaming barrel, and alkali water which can right wet the cocoons is sprayed on the cocoons so that the cocoons can be wet again; (4), steaming is performed, namely, the cocoons are steamed with steam so that sericin can be completely swollen; (5), washing is performed, namely, the steamed cocoons are washed with clean water; (6), cocoon peeling is performed, namely, pupas are peeled off; (7), the cocoons with the pupas peeled off are made into arc-shaped silk net films; (8), the silk net films are bleached, neutralized with a glacial acetic acid solution, dried and finally stamped to form the silk mask base cloth. By means of the method, the activity of the sericin can be maintained to the maximum degree. The technological process is simple, the nutrients of silk can be sufficiently utilized, and the silk mask base cloth is a pure natural skin-whitening, moisturizing, anti-wrinkling and UV-resisting product.
Description
Technical field
The present invention relates to cosmetic field, is method and silk mask that a kind of silk cocoon produces silk mask base cloth specifically.
Background technology
Along with living standard improves, facial mask has become the indispensable skin care products of modern from original luxury consumer goods.And silk relies on the 18 kinds of essential amino acids itself containing needed by human body, and become the very popular face mask substrate material of facial mask circle.
Silk mask commercially available at present mainly adopts the manufacturing process of nonwoven fabric, and the production technology of nonwoven fabric is comparatively complicated: mainly adopt silk spinning raw material (leftover bits and pieces namely in filature, waste silk, bourette etc.), through removal of impurities, cut off, come unstuck (or solid glue) refining, combing, add antistatic additive, regulation and control humiture after enter water thorn (or acupuncture) production line.These silk spinning raw material major parts are through physics repeatedly, chemical action (high temperature, high pressure, chemical assistant), although silk gum is still withed a hook at the end, but albumen is through sex change renaturation process repeatedly, and the activity of most of sericin is lost already, cannot reach desirable cosmetic result.In addition, the silk non-woven fabric that current water thorn (or acupuncture) line is produced is general more thick and heavy, and cause silk mask and the right difference of skin paste, result of use is undesirable, loses its skin-friendly.
In addition, people also adopt directly to be added in facial mask by fibroin and make silk mask, as Chinese patent CN102836104B discloses a kind of bamboo charcoal-cocoon fiber facial mask, fibroin is the natural polymer fibrin extracted from silk, content accounts for 70% ~ 80% of silk, containing 18 seed amino acids, wherein glycine (gly), alanine (ala) and serine (ser) account for more than 80% of total composition.Such leaching process complex process, and, the natural nutrition of silk cannot be retained completely.
Summary of the invention
For existing problem, the object of the present invention is to provide a kind of method of producing silk mask base cloth with silk cocoon of pure natural, the invention still further relates to a kind of silk mask.
To achieve these goals, technical scheme of the present invention is: a kind of silk cocoon produces the method for silk mask base cloth, it is characterized in that: complete in accordance with the following steps:
(1), cocoon is washed: silk cocoon clear water is washed away dust and foreign material;
(2), wetting: the silk cocoon after cleaning to be soaked in water and to make it fully wetting;
(3), caustic dip: the silk cocoon after wetting is evenly put into steaming kier, with the buck spray silk cocoon that be able to soak silk cocoon, makes silk cocoon again wetted;
(4), decatize: make silk gum complete swelling with steamed silk cocoon;
(5), cleaning: with the silk cocoon that clean water is steamed, remove remaining alkali lye;
(6), cocoon is shelled: by silkworm chrysalis peel-away removal;
(7), the silk cocoon of peel-away removal silkworm chrysalis is made arc silk nethike embrane;
(8), silk nethike embrane is obtained silk mask base cloth through bleaching, with glacial acetic acid solution neutralization, oven dry, last punch forming.
Adopt such scheme, the present invention directly makees silk mask base cloth with silk cocoon, there is the effect of frivolous recessiveness, the activity of sericin can be kept to greatest extent, technological process is short, preparation method is simple, and the silk mask base cloth obtained is the long filament of directly garnetting from silk cocoon, can not there is the phenomenon that short fiber drops.This mask substrate has the effect of porous, good permeability, 18 kinds of natural amino acids are rich in silk, can directly be absorbed and absorption by human hair, skin, have lasting moisture-retaining capacity, naturally crease-resistant, promotion collagen secretion, potently to brighten, uv-resistant, anti-inflammatory, anti-pock ability.
In such scheme, in step (3), the concentration of buck needs 0.8-1.2 gram of soda ash preparation by every 60 grams of silk cocoons, and the weight of water is about 5 times of silk cocoon amount.That is, every 60g silk cocoon needs the buck that is made into 0.8-1.2g soda ash and 300g water.
In such scheme, in step (4), steam injection is equipped with boiling in the steaming kier of silk cocoon, the time of boiling is 0.8-1.2h.To ensure silk gum complete swelling.
In such scheme, step (7), first silk cocoon is made less arc silk nethike embrane, less arc silk nethike embrane is made larger silk nethike embrane.
As preferably: silk is enclosed within semicircle mould and makes silk nethike embrane.
In such scheme: in step (8), according to mass percent, in bleaching liquid containing 0.7% waterglass, 0.7% textile soap and 2.5% hydrogen peroxide, bath raio is 1:18-22, bleaching time 2-24h.
In such scheme: in step (8), the mass concentration of glacial acetic acid solution is 0.3%, bath raio 1:12-18, and soak time is 0.5-1h.
Another object of the present invention is achieved in that a kind of silk mask, it is characterized in that: on the silk mask base cloth obtained by step (1)-(7), spray can make the Protease Treatment liquid of the abundant swelling renaturation of silk gum, then enclose pearl film, obtain silk mask.
Adopt such scheme, Protease Treatment liquid just can directly use after making the swelling renaturation of silk gum of silk mask base cloth.Make full use of the nutriment such as hydrolysis fibroin and amino acid of the silk of pure natural, can play moisturizing and prevent xerodermatic effect, just look like the bionic dermis of people, good permeability, light weight.
As preferably: containing 0.3% protease, the glycerine of 5-10% and the glacial acetic acid of 0.3% in described Protease Treatment liquid.Also can adopt other Protease Treatment liquid, other nutriment can also be added in treatment fluid, make different facial masks.
The invention has the beneficial effects as follows: compared with traditional silk mask, the present invention has the effect of frivolous recessiveness, and farthest can keep the activity of sericin.In addition, directly adopt silk cocoon to produce the mode of facial mask, not only shorten technological process, and the silk mask obtained is the long filament of directly garnetting from silk cocoon, the short fiber that can not exist in silk non-woven fabric drops phenomenon.The present invention makes full use of the nutriment of silk, is the whitening of pure natural, moisturizing, crease-resistant, uv-resistant product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described:
The preparation of embodiment 1 silk mask base cloth, completes in accordance with the following steps:
1, cocoon is washed: silk cocoon clear water is washed away dust and foreign material.
2, wetting: be soaked in water the silk cocoon after cleaning certain hour, makes it fully wetting.
3, caustic dip: the silk cocoon after cleaning is wetting evenly puts into steaming kier, drenches silk cocoon with the buck that again be able to soak silk cocoon.The concentration of this buck needs 0.8 gram of soda ash preparation by every 60 grams of silk cocoons.The weight of water is about 5 times of silk cocoon amount.That is, every 60g silk cocoon needs the buck that is made into 0.8g soda ash and 300g water.
4, decatize: by steam injection steaming kier boiling silk cocoon 0.8h, allows silk gum complete swelling.
5, clean: to install with permeable utensil put into clean water by boiling steamed silk cocoon, remaining alkali is cleaned up.
6, cocoon is shelled: manual by silkworm chrysalis peel-away removal;
7, make silk nethike embrane: be enclosed within by the silk cocoon of peel-away removal silkworm chrysalis on the circular arc mould more bashful than people, make silk cocoon under the effect of circular arc mould, be separated into less silk nethike embrane, probably every 3 silk cocoons form a nethike embrane,
Again by less silk net Membrane cover on the circular arc mould of being bold than people, make the area of its silk nethike embrane be enough to shaping all kinds of facial mask.
8, bleach: at bath raio 1:18, bleach 2h with bleaching liquid, in bleaching liquid according to mass percent contain 0.7% waterglass, 0.7% textile soap and 2.5% hydrogen peroxide.
9 neutralizations: silk nethike embrane is that in the glacial acetic acid solution of 0.3%, soak time is 0.5-1h in mass concentration by bath raio 1:12.
10 dry;
11. punch formings: use blade type mould, strike out facial mask finished product by silk nethike embrane, specifically such as stamp out the hole etc. of two eyes, make it be shaped to a mask substrate.
Embodiment 2
The preparation of silk mask base cloth, completes in accordance with the following steps:
1, cocoon is washed: silk cocoon clear water is washed away dust and foreign material.
2, wetting: be soaked in water the silk cocoon after cleaning certain hour, makes it fully wetting.
3, caustic dip: the silk cocoon after cleaning is wetting evenly puts into steaming kier, drenches silk cocoon with the buck that again be able to soak silk cocoon.The concentration of this buck needs 1.2 grams of soda ash preparations by every 60 grams of silk cocoons.The weight of water is about 5 times of silk cocoon amount.That is, every 60g silk cocoon needs the buck that is made into 1.2g soda ash and 300g water.
4, decatize: by steam injection steaming kier boiling silk cocoon 1.2h, allows silk gum complete swelling.
5, clean: to install with permeable utensil put into clean water by boiling steamed silk cocoon, remaining alkali is cleaned up.
6, cocoon is shelled: manual by silkworm chrysalis peel-away removal;
7, make silk nethike embrane: be enclosed within by the silk cocoon of peel-away removal silkworm chrysalis on the circular arc mould more bashful than people, make silk cocoon under the effect of circular arc mould, be separated into less silk nethike embrane, probably every 3 silk cocoons form a nethike embrane,
Again by less silk net Membrane cover on the circular arc mould of being bold than people, make the area of its silk nethike embrane be enough to shaping all kinds of facial mask.
8, bleach: at bath raio 1:22, bleach 24h with bleaching liquid, in bleaching liquid according to mass percent contain 0.7% waterglass, 0.7% textile soap and 2.5% hydrogen peroxide.
9 neutralizations: silk nethike embrane is that in the glacial acetic acid solution of 0.3%, soak time is 0.5-1h in mass concentration by bath raio 1:18.
10 dry;
11. punch formings: use blade type mould, strike out facial mask finished product by silk nethike embrane, specifically such as stamp out the hole etc. of two eyes, make it be shaped to a mask substrate.
Embodiment 3
The preparation of silk mask base cloth, completes in accordance with the following steps:
1, cocoon is washed: silk cocoon clear water is washed away dust and foreign material.
2, wetting: be soaked in water the silk cocoon after cleaning certain hour, makes it fully wetting.
3, caustic dip: the silk cocoon after cleaning is wetting evenly puts into steaming kier, drenches silk cocoon with the buck that again be able to soak silk cocoon.The concentration of this buck needs 1 gram of soda ash preparation by every 60 grams of silk cocoons.The weight of water is about 5 times of silk cocoon amount.That is, every 60g silk cocoon needs the buck that is made into 1g soda ash and 300g water.
4, decatize: by steam injection steaming kier boiling silk cocoon 1h, allows silk gum complete swelling.
5, clean: to install with permeable utensil put into clean water by boiling steamed silk cocoon, remaining alkali is cleaned up.
6, cocoon is shelled: manual by silkworm chrysalis peel-away removal;
7, make silk nethike embrane: be enclosed within by the silk cocoon of peel-away removal silkworm chrysalis on the circular arc mould more bashful than people, make silk cocoon under the effect of circular arc mould, be separated into less silk nethike embrane, probably every 3 silk cocoons form a nethike embrane,
Again by less silk net Membrane cover on the circular arc mould of being bold than people, make the area of its silk nethike embrane be enough to shaping all kinds of facial mask.
8, bleach: at bath raio 1:20, bleach 10h with bleaching liquid, in bleaching liquid according to mass percent contain 0.7% waterglass, 0.7% textile soap and 2.5% hydrogen peroxide.
9 neutralizations: silk nethike embrane is that in the glacial acetic acid solution of 0.3%, soak time is 0.5-1h in mass concentration by bath raio 1:15.
10 dry;
11. punch formings: use blade type mould, strike out facial mask finished product by silk nethike embrane, specifically such as stamp out the hole etc. of two eyes, make it be shaped to a mask substrate.
Embodiment 4: the preparation of silk mask
By silk mask base cloth spray Protease Treatment liquid obtained for embodiment 1-3.Make the abundant swelling Protease Treatment liquid of silk gum according to mass percent: the glycerine containing 0.3% protease, 5-10% and the glacial acetic acid of 0.3%.Then enclose pearl film, silk mask finished product.Certainly, Protease Treatment liquid is not limited to said ratio, can also add other nutriment, make different facial masks, also can adopt other Protease Treatment liquid in Protease Treatment liquid.
The present invention is not limited to above-mentioned specific embodiment, should be appreciated that those of ordinary skill in the art just design according to the present invention can make many modifications and variations without the need to creative work.In a word, all technical staff in the art, all should by the determined protection domain of claims under this invention's idea on the basis of existing technology by the available technical scheme of logical analysis, reasoning, or a limited experiment.
Claims (9)
1. produce a method for silk mask base cloth with silk cocoon, it is characterized in that: complete in accordance with the following steps:
(1), cocoon is washed: silk cocoon clear water is washed away dust and foreign material;
(2), wetting: the silk cocoon after cleaning to be soaked in water and to make it fully wetting;
(3), caustic dip: the silk cocoon after wetting is evenly put into steaming kier, with the buck spray silk cocoon that be able to soak silk cocoon, makes silk cocoon again wetted;
(4), decatize: make silk gum complete swelling with steamed silk cocoon;
(5), cleaning: with the silk cocoon that clean water is steamed, remove remaining alkali lye;
(6), cocoon is shelled: by silkworm chrysalis peel-away removal;
(7), the silk cocoon of peel-away removal silkworm chrysalis is made arc silk nethike embrane;
(8), silk nethike embrane is obtained silk mask base cloth through bleaching, with glacial acetic acid solution neutralization, oven dry, last punch forming.
2. produce the method for silk mask base cloth according to claim 1 with silk cocoon, it is characterized in that: in step (3), the concentration of buck needs 0.8-1.2 gram of soda ash preparation by every 60 grams of silk cocoons.
3. produce the method for silk mask base cloth according to claim 2 with silk cocoon, it is characterized in that: in step (4), steam injection is equipped with boiling in the steaming kier of silk cocoon, the time of boiling is 0.8-1.2h.
4. produce the method for silk mask base cloth according to claim 3 with silk cocoon, it is characterized in that: step (7), first silk cocoon is made less arc silk nethike embrane, less arc silk nethike embrane is made larger silk nethike embrane.
5. produce the method for silk mask base cloth according to claim 4 with silk cocoon, it is characterized in that: silk is enclosed within semicircle mould and makes silk nethike embrane.
6. the method for silk mask base cloth is produced according to claim 5 with silk cocoon, it is characterized in that: in step (8), according to mass percent, in bleaching liquid containing 0.7% waterglass, 0.7% textile soap and 2.5% hydrogen peroxide; bath raio is 1:18-22, bleaching time 2-24h.
7. produce the method for silk mask base cloth according to claim 6 with silk cocoon, it is characterized in that: in step (8), the mass concentration of glacial acetic acid solution is 0.3%, bath raio 1:12-18, and soak time is 0.5-1h.
8. a silk mask, is characterized in that: on the silk mask base cloth obtained by step (1)-(7), spray can make the Protease Treatment liquid of the abundant swelling renaturation of silk gum, then encloses pearl film, obtains silk mask.
9. silk mask according to claim 8, is characterized in that: containing 0.3% protease, the glycerine of 5-10% and the glacial acetic acid of 0.3% in described Protease Treatment liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510040948.4A CN104611838B (en) | 2015-01-27 | 2015-01-27 | A kind of silk cocoon produces method and the silk mask of silk mask base cloth |
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| CN201510040948.4A CN104611838B (en) | 2015-01-27 | 2015-01-27 | A kind of silk cocoon produces method and the silk mask of silk mask base cloth |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107142615A (en) * | 2016-05-17 | 2017-09-08 | 广州宇然膜丽无纺制品有限公司 | A kind of silk film cloth and preparation method thereof |
| CN107320359A (en) * | 2017-06-23 | 2017-11-07 | 芜湖凌梦电子商务有限公司 | A kind of preparation method of the fibroin facial mask containing peony essential oil |
| CN107503042A (en) * | 2017-08-28 | 2017-12-22 | 杭州路先非织造股份有限公司 | A kind of spunlaced face mask base material and preparation method thereof |
| CN108392435A (en) * | 2018-05-15 | 2018-08-14 | 西南大学 | A kind of silk mask |
| CN112587419A (en) * | 2020-12-31 | 2021-04-02 | 广西八园农业科技有限公司 | Preparation method of silk mask |
| CN113265768A (en) * | 2021-06-10 | 2021-08-17 | 盐城工业职业技术学院 | Method for producing flat silk surface membrane material from whole silk glue silkworm and common castor silkworm |
| JP2022073360A (en) * | 2020-10-30 | 2022-05-17 | 山岸 幸一 | Floss-made multi-layer filter, manufacturing method therefor, silk filter mask using the same, and manufacturing method therefor |
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| CN1800472A (en) * | 2006-01-13 | 2006-07-12 | 席星航 | Silk denaturated nonwoven fabric containing sericin, and its uses |
| CN104146884A (en) * | 2014-07-16 | 2014-11-19 | 东华大学 | Preparation method of rapid and absorbable pure natural silk mask |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107142615A (en) * | 2016-05-17 | 2017-09-08 | 广州宇然膜丽无纺制品有限公司 | A kind of silk film cloth and preparation method thereof |
| CN107320359A (en) * | 2017-06-23 | 2017-11-07 | 芜湖凌梦电子商务有限公司 | A kind of preparation method of the fibroin facial mask containing peony essential oil |
| CN107503042A (en) * | 2017-08-28 | 2017-12-22 | 杭州路先非织造股份有限公司 | A kind of spunlaced face mask base material and preparation method thereof |
| CN107503042B (en) * | 2017-08-28 | 2023-06-02 | 杭州路先非织造股份有限公司 | Water-jet mask base material and preparation method thereof |
| CN108392435A (en) * | 2018-05-15 | 2018-08-14 | 西南大学 | A kind of silk mask |
| JP2022073360A (en) * | 2020-10-30 | 2022-05-17 | 山岸 幸一 | Floss-made multi-layer filter, manufacturing method therefor, silk filter mask using the same, and manufacturing method therefor |
| JP7332564B2 (en) | 2020-10-30 | 2023-08-23 | 山岸 幸一 | Multi-layer floss filter, manufacturing method thereof, silk filter mask using same, and manufacturing method thereof |
| CN112587419A (en) * | 2020-12-31 | 2021-04-02 | 广西八园农业科技有限公司 | Preparation method of silk mask |
| CN113265768A (en) * | 2021-06-10 | 2021-08-17 | 盐城工业职业技术学院 | Method for producing flat silk surface membrane material from whole silk glue silkworm and common castor silkworm |
| CN113265768B (en) * | 2021-06-10 | 2022-03-22 | 盐城工业职业技术学院 | Method for producing flat silk surface membrane material from whole silk glue silkworm and common castor silkworm |
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| CN104611838B (en) | 2015-09-23 |
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