Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of preparation method that with the addition of the square brick of the admixture that can improve concrete square brick epistasis morning energy is provided.
For achieving the above object, the technical solution used in the present invention is as follows:
A preparation method for square brick, its square brick is high-strength square brick, it is characterized in that:
Take raw material: cement 414g, concrete square brick admixture 36g, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, first by cement, concrete square brick admixture and 100 ml water are put into concrete mixer and are stirred 2 minutes, add sand again, stone, polypropylene fibre, naphthalene water reducer and 125ml water continue stirring 2 minutes, pour into a mould after stirring in progressive die tool and carry out standing precuring, the time leaving standstill precuring is 8 hours, the temperature leaving standstill precuring should control at 45 DEG C, put into autoclave after standing precuring completes and carry out steam press maintenance 18 hours, when carrying out steam press maintenance, vapor pressure in autoclave should remain on 0.8MPa, after steam press maintenance completes, go out still namely obtain high-strength square brick,
Described concrete square brick admixture preparation method step is:
Step (1): according to 27 parts, diatomite, dickite 27 parts, montmorillonite 17 parts, malthacite 12 parts, vermiculite 17 parts, 17 parts, saltcake, polyvinyl alcohol 3.6 parts, 3.4 parts, iron(ic) chloride, borax 1.3 parts, 2.8 parts, gypsum, water glass 2.7 parts, 1.1 parts, ferrous sulfate, methylcellulose gum 2.3 parts, 1.6 parts, sodium carbonate, proportioning prepares raw material
Step (2): by 27 parts, diatomite, dickite 27 parts, montmorillonite 17 parts carry out grinding in pulverizer, rotating speed is 120r/min, grinding 9 hours, grinding composition granule degree size is 1.2-1.4mm, afterwards grinding thing is put into High Temperature Furnaces Heating Apparatus, according to heating up at a slow speed, middling speed heats up, be rapidly heated and constant temperature Four processes carries out temperature control and fires: be warming up at a slow speed 300 DEG C with the speed of 2 DEG C/min, 500 DEG C are warming up to afterwards with the speed middling speed of 5 DEG C/min, be rapidly heated to 800 DEG C with the speed of 8 DEG C/min afterwards, then constant temperature is incubated 3 hours; To come out of the stove naturally cooling, after cooling in pulverizer grinding 3 hours again, obtaining mixture A granularity size is 0.8-1mm,
Step (3): by malthacite 12 parts, vermiculite 17 parts, 17 parts, saltcake carry out grinding in pulverizer, rotating speed is 100r/min, grinding 3 hours, and obtaining compound particles granularity size is 0.6-0.8mm, afterwards grinding thing is heated, Heating temperature 700 DEG C, is incubated 2 hours, after cooling in pulverizer grinding 3 hours again, obtaining mixture B granularity size is 0.3-0.5mm
Step (4): step (2) is obtained mixture A and step (3) is obtained mixture B loading in mechanical mixer, mechanically mixing 0.5 hour, pour polyvinyl alcohol 3.6 parts, 3.4 parts, iron(ic) chloride, borax 1.3 parts afterwards into, 2.8 parts, gypsum, water glass 2.7 parts, 1.1 parts, ferrous sulfate, methylcellulose gum 2.3 parts, 1.6 parts, sodium carbonate, mechanically mixing 1 hour again, obtains concrete square brick admixture.
A preparation method for square brick, its square brick is high-strength square brick, it is characterized in that:
Take raw material: cement 414g, concrete square brick admixture 36g, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, first by cement, concrete square brick admixture and 100 ml water are put into concrete mixer and are stirred 2 minutes, add sand again, stone, polypropylene fibre, naphthalene water reducer and 125ml water continue stirring 2 minutes, pour into a mould after stirring in progressive die tool and carry out standing precuring, the time leaving standstill precuring is 8 hours, the temperature leaving standstill precuring should control at 45 DEG C, put into autoclave after standing precuring completes and carry out steam press maintenance 18 hours, when carrying out steam press maintenance, vapor pressure in autoclave should remain on 0.8MPa, after steam press maintenance completes, go out still namely obtain high-strength square brick,
Described concrete square brick admixture preparation method step is:
Step (1): according to 26 parts, diatomite, dickite 26 parts, montmorillonite 16 parts, malthacite 13 parts, vermiculite 16 parts, 16 parts, saltcake, polyvinyl alcohol 3.4 parts, 3.2 parts, iron(ic) chloride, borax 1.3 parts, 2.4 parts, gypsum, water glass 2.6 parts, 1.7 parts, ferrous sulfate, methylcellulose gum 2.8 parts, 1.9 parts, sodium carbonate, proportioning prepares raw material
Step (2): by 26 parts, diatomite, dickite 26 parts, montmorillonite 16 parts carry out grinding in pulverizer, rotating speed is 120r/min, grinding 9 hours, grinding composition granule degree size is 1.2-1.4mm, afterwards grinding thing is put into High Temperature Furnaces Heating Apparatus, according to heating up at a slow speed, middling speed heats up, be rapidly heated and constant temperature Four processes carries out temperature control and fires: be warming up at a slow speed 300 DEG C with the speed of 2 DEG C/min, 500 DEG C are warming up to afterwards with the speed middling speed of 5 DEG C/min, be rapidly heated to 800 DEG C with the speed of 8 DEG C/min afterwards, then constant temperature is incubated 3 hours; To come out of the stove naturally cooling, after cooling in pulverizer grinding 3 hours again, obtaining mixture A granularity size is 0.8-1mm,
Step (3): by malthacite 13 parts, vermiculite 16 parts, 16 parts, saltcake carry out grinding in pulverizer, rotating speed is 100r/min, grinding 3 hours, and obtaining compound particles granularity size is 0.6-0.8mm, afterwards grinding thing is heated, Heating temperature 700 DEG C, is incubated 2 hours, after cooling in pulverizer grinding 3 hours again, obtaining mixture B granularity size is 0.3-0.5mm
Step (4): step (2) is obtained mixture A and step (3) is obtained mixture B loading in mechanical mixer, mechanically mixing 0.5 hour, pour polyvinyl alcohol 3.4 parts, 3.2 parts, iron(ic) chloride, borax 1.3 parts afterwards into, 2.4 parts, gypsum, water glass 2.6 parts, 1.7 parts, ferrous sulfate, methylcellulose gum 2.8 parts, 1.9 parts, sodium carbonate, mechanically mixing 1 hour again, obtains concrete square brick admixture.
Compared with prior art, the present invention has following beneficial effect:
1, the preparation of base sample: adopt cement 450g, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, and shaping 40 × 40 × 160mm test specimen, carry out maintenance.
2, the preparation of test sample: adopt cement 414g, the concrete square brick admixture 36g prepared, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, and shaping 40 × 40 × 160mm test specimen, carry out maintenance.
When obtained concrete square brick admixture is substituted the cement of 8 ﹪, concrete square brick test sample ultimate compression strength is after testing: 3 days ultimate compression strength is 17.8MPa, 28 days ultimate compression strength is 41.7MPa, compared with not adding the base sample ultimate compression strength of concrete square brick admixture under similarity condition, within 3 days, ultimate compression strength improves 4.3MPa, and within 28 days, ultimate compression strength improves 3.5MPa.Concrete square brick admixture starting material of the present invention are easily purchased, and production technique is uncomplicated, are simply easy to produce product, conveniently also can evenly use in use procedure, meet the stability of producing, and improve production efficiency, provide cost savings.
Embodiment
Embodiment 1
A preparation method for square brick, its square brick is high-strength square brick, it is characterized in that:
Take raw material: cement 414g, concrete square brick admixture 36g, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, first by cement, concrete square brick admixture and 100 ml water are put into concrete mixer and are stirred 2 minutes, add sand again, stone, polypropylene fibre, naphthalene water reducer and 125ml water continue stirring 2 minutes, pour into a mould after stirring in progressive die tool and carry out standing precuring, the time leaving standstill precuring is 8 hours, the temperature leaving standstill precuring should control at 45 DEG C, put into autoclave after standing precuring completes and carry out steam press maintenance 18 hours, when carrying out steam press maintenance, vapor pressure in autoclave should remain on 0.8MPa, after steam press maintenance completes, go out still namely obtain high-strength square brick,
Described concrete square brick admixture preparation method step is:
Step (1): according to 27 parts, diatomite, dickite 27 parts, montmorillonite 17 parts, malthacite 12 parts, vermiculite 17 parts, 17 parts, saltcake, polyvinyl alcohol 3.6 parts, 3.4 parts, iron(ic) chloride, borax 1.3 parts, 2.8 parts, gypsum, water glass 2.7 parts, 1.1 parts, ferrous sulfate, methylcellulose gum 2.3 parts, 1.6 parts, sodium carbonate, proportioning prepares raw material
Step (2): by 27 parts, diatomite, dickite 27 parts, montmorillonite 17 parts carry out grinding in pulverizer, rotating speed is 120r/min, grinding 9 hours, grinding composition granule degree size is 1.2-1.4mm, afterwards grinding thing is put into High Temperature Furnaces Heating Apparatus, according to heating up at a slow speed, middling speed heats up, be rapidly heated and constant temperature Four processes carries out temperature control and fires: be warming up at a slow speed 300 DEG C with the speed of 2 DEG C/min, 500 DEG C are warming up to afterwards with the speed middling speed of 5 DEG C/min, be rapidly heated to 800 DEG C with the speed of 8 DEG C/min afterwards, then constant temperature is incubated 3 hours; To come out of the stove naturally cooling, after cooling in pulverizer grinding 3 hours again, obtaining mixture A granularity size is 0.8-1mm,
Step (3): by malthacite 12 parts, vermiculite 17 parts, 17 parts, saltcake carry out grinding in pulverizer, rotating speed is 100r/min, grinding 3 hours, and obtaining compound particles granularity size is 0.6-0.8mm, afterwards grinding thing is heated, Heating temperature 700 DEG C, is incubated 2 hours, after cooling in pulverizer grinding 3 hours again, obtaining mixture B granularity size is 0.3-0.5mm
Step (4): step (2) is obtained mixture A and step (3) is obtained mixture B loading in mechanical mixer, mechanically mixing 0.5 hour, pour polyvinyl alcohol 3.6 parts, 3.4 parts, iron(ic) chloride, borax 1.3 parts afterwards into, 2.8 parts, gypsum, water glass 2.7 parts, 1.1 parts, ferrous sulfate, methylcellulose gum 2.3 parts, 1.6 parts, sodium carbonate, mechanically mixing 1 hour again, obtains concrete square brick admixture.
Embodiment 2
A preparation method for square brick, its square brick is high-strength square brick, it is characterized in that:
Take raw material: cement 414g, concrete square brick admixture 36g, sand 650g, stone 1100 g, water consumption 225ml, polypropylene fibre 4g, naphthalene water reducer 3g, first by cement, concrete square brick admixture and 100 ml water are put into concrete mixer and are stirred 2 minutes, add sand again, stone, polypropylene fibre, naphthalene water reducer and 125ml water continue stirring 2 minutes, pour into a mould after stirring in progressive die tool and carry out standing precuring, the time leaving standstill precuring is 8 hours, the temperature leaving standstill precuring should control at 45 DEG C, put into autoclave after standing precuring completes and carry out steam press maintenance 18 hours, when carrying out steam press maintenance, vapor pressure in autoclave should remain on 0.8MPa, after steam press maintenance completes, go out still namely obtain high-strength square brick,
Described concrete square brick admixture preparation method step is:
Step (1): according to 26 parts, diatomite, dickite 26 parts, montmorillonite 16 parts, malthacite 13 parts, vermiculite 16 parts, 16 parts, saltcake, polyvinyl alcohol 3.4 parts, 3.2 parts, iron(ic) chloride, borax 1.3 parts, 2.4 parts, gypsum, water glass 2.6 parts, 1.7 parts, ferrous sulfate, methylcellulose gum 2.8 parts, 1.9 parts, sodium carbonate, proportioning prepares raw material
Step (2): by 26 parts, diatomite, dickite 26 parts, montmorillonite 16 parts carry out grinding in pulverizer, rotating speed is 120r/min, grinding 9 hours, grinding composition granule degree size is 1.2-1.4mm, afterwards grinding thing is put into High Temperature Furnaces Heating Apparatus, according to heating up at a slow speed, middling speed heats up, be rapidly heated and constant temperature Four processes carries out temperature control and fires: be warming up at a slow speed 300 DEG C with the speed of 2 DEG C/min, 500 DEG C are warming up to afterwards with the speed middling speed of 5 DEG C/min, be rapidly heated to 800 DEG C with the speed of 8 DEG C/min afterwards, then constant temperature is incubated 3 hours; To come out of the stove naturally cooling, after cooling in pulverizer grinding 3 hours again, obtaining mixture A granularity size is 0.8-1mm,
Step (3): by malthacite 13 parts, vermiculite 16 parts, 16 parts, saltcake carry out grinding in pulverizer, rotating speed is 100r/min, grinding 3 hours, and obtaining compound particles granularity size is 0.6-0.8mm, afterwards grinding thing is heated, Heating temperature 700 DEG C, is incubated 2 hours, after cooling in pulverizer grinding 3 hours again, obtaining mixture B granularity size is 0.3-0.5mm
Step (4): step (2) is obtained mixture A and step (3) is obtained mixture B loading in mechanical mixer, mechanically mixing 0.5 hour, pour polyvinyl alcohol 3.4 parts, 3.2 parts, iron(ic) chloride, borax 1.3 parts afterwards into, 2.4 parts, gypsum, water glass 2.6 parts, 1.7 parts, ferrous sulfate, methylcellulose gum 2.8 parts, 1.9 parts, sodium carbonate, mechanically mixing 1 hour again, obtains concrete square brick admixture.