CN104523466A - Chinese herbal medicinal skin mucosa disinfection wet wipe - Google Patents
Chinese herbal medicinal skin mucosa disinfection wet wipe Download PDFInfo
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- CN104523466A CN104523466A CN201410700284.5A CN201410700284A CN104523466A CN 104523466 A CN104523466 A CN 104523466A CN 201410700284 A CN201410700284 A CN 201410700284A CN 104523466 A CN104523466 A CN 104523466A
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Abstract
The invention provides a Chinese herbal medicinal skin mucosa disinfection wet wipe. The Chinese herbal medicinal skin mucosa disinfection wet wipe comprises a disinfected nonwoven fabric and a disinfectant loaded on the disinfected nonwoven fabric. The disinfectant is prepared through the following steps: 1, taking 15 parts of Radix Scutellariae, 15 parts of honeysuckle flower, 15 parts of grapefruit, 8 parts of aloe and 4 parts of lavender, adding ethanol, extracting twice, mixing two extraction liquids, adding active carbon to decolor the obtained liquid mixture, filtering, and distilling the obtained filtrate until the volume of the obtained concentrate is 0.3 times the original volume; 2, taking 8 parts of garlic, adding ethanol, grinding, and filtering to obtain a filtrate for later use; 3, taking 4 parts of menthol, 2 parts of glycerin, 2 parts of chitosan quaternary ammonium salt, 0.3 parts of alkyl dimethyl benzyl ammonium chloride and 8 parts of sucrose palmitate, adding distilled water, and stirring for dissolving; and 4, mixing solutions obtained in step 1, step 2 and step 3, and uniformly stirring. The skin mucosa disinfection wet wipe has the advantages of no irritant smell, low toxicity, and weak irritation to skins, and is suitable for disinfecting skin mucosa; and the cooperation of Chinese herbal medicines and disinfection active components increases the sterilization and disinfection effects of the wet pipe.
Description
Technical field
The present invention relates to disinfection technology field, particularly a kind of Chinese herbal medicine skin mucosa pasteurization towelette.
Background technology
Protecting human body gets up by skin and mucosa, and making human body define an airtight system to external world, when harmful substance will invade human body, is first that extraneous paathogenic factor is blocked in external by skin and mucosa.So skin and mucosa are human body anti-infective the first line of defences.Therefore the sterilization outbalance of skin mucosa.
At present, skin mucosa disinfectant preparation mainly contains: 1, peracetic acid, peracetic acid mainly relies on its Strong oxdiative ability to the killing action of microorganism, it can destroy the permeability barrier of bacterial spore, and then destroy and dissolve core, the material damage of DNA, RNA, protein is spilt, causes spore dead.Peracetic acid is usually used in by virus contamination article or skin degerming, and during general sterilisation of objects, usable concentration is 0.5%, and during skin degerming, usable concentration is 0.2%-0.4%, and action time is 3 minutes.But Organic substance can reduce the bactericidal action of peracetic acid, needed for the thin rice seedling brood body killing 20% serum protection, peroxyacetic acid concentration need increase by 4 ~ 15 times, and need increase by 2 ~ 3 times to bacterial spore.Peracetic acid soln is unstable, need be placed in ventilating and cooling place during storage, first measures valid density altogether with front; With distilled water, deionized water or pure water prepared and diluted liquid, preserve no more than 48h under diluent room temperature.Peracetic acid has very strong corrosivity to metal, acutely decomposes, even blast when having bases or Organic substance to be mixed into.The medicinal liquid of high concentration has severe corrosive and zest, and its abnormal smells from the patient people is beyond affordability.2, alcohol disinfectant: 1. ethanol belongs to middle effect disinfectants, bactericidal action is very fast, and non-stimulated to human body, toxicity is less.Ethanol sterilization there are certain requirements concentration, and its effective volume fraction should be 65% ~ 75%.Water to ethanol play bactericidal action very necessary, need dilute ethanol time therefore for sterilizing, but concentration lower than 30% time bactericidal action very little, concentration is crossed strong or excessively weak, and bactericidal action all can reduce.The folk prescription ethanol disinfection preparation of 75% to human non-toxic, but due to the body constitution of people different, one or two people are irritated to ethanol, can cause erythra, erythema after contact.Ethanol disinfection preparation often uses, skin therefore can produce defat and drying, the phenomenon such as coarse.2. isopropyl alcohol: the bactericidal action of isopropyl alcohol is better than ethanol.But it belongs to slight noxious substance, when exceeding finite concentration, there is intense stimulus effect to respiratory mucosa and eye conjunctiva, and cell tissue can be caused downright bad.Aqueous isopropanol is by force fat dissolving, repeatedly contacts skin and can make xerosis cutis defat.In addition, Organic substance and low temperature all can make the bactericidal effect of isopropyl alcohol weaken.3, iodine-containing disinfectant: common ground povidone iodine and iodine tincture.Their halogenation microproteins of relying make it dead.Can kill vegetative forms of bacteria, fungus and fractionated viral.May be used for skin, mucosa sterilization, hospital is usually used in surgical hand sterilization.The working concentration of general iodine tincture is 2%, and povidone iodine working concentration is 0.3% to 0.5%.But iodide ion is extremely active, its oxidizing force is very strong, is a kind of material of instability, can reduce effective content and reduce disinfective action.And these disinfectant liquid for skin are mostly synthetics, as Iodic agent, alcohol disinfectant etc., the general poor stability of these materials, large to human body zest, life-time service has certain potential hazard to human body.
Existing pasteurization towelette has two kinds, a kind of for abrading, hurting, clean, the sterilization of the minor cut or wound such as scuffing and surrounding skin, institute's immersion fluid main component is Benzalkonii Chloridum etc., and clean, sterilization once completes; Another kind has broad-spectrum bactericidal action, for clean, the skin moistening of skin, sterilization, sterilization, also can be used for articles for daily use, sanitary ware, can effectively kill staphylococcus aureus, escherichia coli, gonorrhea diplococcus, bacillus pyocyaneus etc. rapidly, institute's immersion fluid is pure water, sterilization component, Aloe, lanoline, kappa pyrimidine antibacterial etc.What wherein chemical sterilization composition was conventional has hibitane, iodine, ethanol, glutaraldehyde etc., and they have respective pluses and minuses respectively, can not disinfection comprehensively and effectively.And these disinfectant liquid for skin are mostly synthetics, as Iodic agent, alcohol disinfectant etc., the general poor stability of these materials, large to human body zest, life-time service has certain potential hazard to human body.
One section of notification number is disclose a kind of pasteurization towelette and preparation method thereof in the patent document of CN1415203, after the pasteurization towelette of this invention is mixed with aqueous solution of chlorine dioxide by Folium Ilicis Purpureae water extract, then forms with sterilizing non-woven fabrics dipping; Pasteurization towelette all has good bactericidal effect to escherichia coli, staphylococcus aureus, its sterilizing rate is high, and shelf characteric is stablized, long shelf-life, non-stimulated to skin, to the reaction of skin ametaboly, its matter is soft thick, soft, use safety, be easy to carry, be applicable to multiple place, be people's daily life and tourism time the good hygienic article of one.One section of notification number is disclose a kind of pasteurization towelette and preparation method thereof in the patent document of CN1415203, after the pasteurization towelette of this invention is mixed with aqueous solution of chlorine dioxide by Folium Ilicis Purpureae water extract, then forms with sterilizing non-woven fabrics dipping; Pasteurization towelette all has good bactericidal effect to escherichia coli, staphylococcus aureus, its sterilizing rate is high, and shelf characteric is stablized, long shelf-life, non-stimulated to skin, to the reaction of skin ametaboly, its matter is soft thick, soft, use safety, be easy to carry, be applicable to multiple place, be people's daily life and tourism time the good hygienic article of one.But this wet tissue contains chlorine dioxide, chlorine-containing disinfectant has obvious stimulation to the respiratory mucosa of people and skin, can draw tears from sb, cough, and chafe and mucosa, severe patient can make people produce chlorine poisoning, is not suitable for the sterilization of skin.
Summary of the invention
The object of the present invention is to provide a kind of Chinese herbal medicine skin mucosa pasteurization towelette, use this skin mucosa pasteurization towelette to skin degerming, can effectively sterilize comprehensively, little to skin irritation, toxicity is little, uses rear skin moist, is applicable to the sterilization of skin mucosa.
For solving the problems of the technologies described above, the present invention is achieved through the following technical solutions.
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, add the ethanol of 6-8 times amount, 30-35min is extracted at 70-80 DEG C, filter, medicinal residues add the ethanol extraction 20-25min of 4-5 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 60%-70% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
Described Chinese herbal medicine skin mucosa pasteurization towelette sterilizing non-woven fabrics is placed in above-mentioned disinfectant to soak after 0.5-1 hour obtained.
Preferably, in the process of lapping of Bulbus Allii, add the white vinegar of 0.5-1 part.
Preferably, Bulbus Allii grinding is the ethanol grinding adding 0.5-1 times amount
In described step (3), the addition of distilled water is 150-180 part.
Described Bulbus Allii is only head purple garlic.
Described Bulbus Allii is the Bulbus Allii slurry that fresh garlic is worn into.
Described grapefruit is the sarcocarp after squeezing the juice in the Renhe of grapefruit.
Beneficial effect:
1, the present invention adopts Chinese herbal medicine and chitosan quaternary ammonium salt, zephiran, the composite sterilization component as this skin mucosa pasteurization towelette, decrease the use amount of chemical bactericide, each pathogenic bacteria can be effectively killed while greatly reducing the toxicity of wet tissue, wherein each composition composite obtain skin irritation little, be particularly suitable for the sterilizing of skin mucosa, in addition, the disinfectant of wet tissue selects chitosan quaternary ammonium salt and zephiran to share, there is synergism, the bactericidal action of chitosan quaternary ammonium salt can be improved; Containing grapefruit in the present invention, grapefruit extract can effectively kill all kinds of pathogenic bacteria, has effect of moisturizing and anti-inflammation simultaneously, contribute to the healing of skin wound in the present invention containing Aloe, lavandula angustifolia extracting solution has cleaning skin, anti-inflammatory efficacy, can prevention infection and inflammation effect; , light anaesthesia can also be played and do in order to detumescence pain; Palmic acid sucrose ester in the present invention can promote medicinal herb components dissolubility and improve the effect of bactericidal effect, is be made up of sucrose and oils and fats, tasteless, nontoxic, and energy biodegradation, not chafe, do not pollute the environment
Pasteurization towelette of the present invention has no irritating odor, toxicity is low, weak to the zest of skin mucosa and eyes, environmentally safe.Simultaneously due to the mating reaction of antimicrobial activity composition, improve disinfection effect, increase germicidal efficiency.
2, the present invention adopts only head purple garlic, and containing more sterilization component, bactericidal effect is good, and the bactericidal action adding white vinegar and Bulbus Allii has collaborative effect, strengthens bactericidal effect.Grapefruit raw material in the present invention is the sarcocarp selecting the Renhe of grapefruit to squeeze juice, and raw material is cheap and easy to get, cost-saving.
Detailed description of the invention
The present invention is further illustrated below by detailed description of the invention.
Embodiment 1
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 6 times amount, 35min is extracted at 70 DEG C, filter, medicinal residues add the ethanol extraction 20min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 60% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
Embodiment 2
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 7 times amount, 30min is extracted at 75 DEG C, filter, medicinal residues add the ethanol extraction 20min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 65% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
Embodiment 3
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 8 times amount, 32min is extracted at 80 DEG C, filter, medicinal residues add the ethanol extraction 23min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 70% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
Embodiment 4
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 7 times amount, 30min is extracted at 75 DEG C, filter, medicinal residues add the ethanol extraction 25min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 60% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
Preferably, in the process of lapping of Bulbus Allii, add the white vinegar of 0.5-1 part.Preferably, the ethanol grinding of 0.5-1 times amount is added during Bulbus Allii grinding.
Embodiment 5
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 6 times amount, 35min is extracted at 70 DEG C, filter, medicinal residues add the ethanol extraction 20min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 60% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
In the present embodiment, Bulbus Allii adopts only head purple garlic.The Bulbus Allii slurry preferably adopting fresh Bulbus Allii to wear into.Grapefruit can squeeze the juice with the Renhe of grapefruit after sarcocarp.
Embodiment 6
A kind of Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, adds the ethanol of 7 times amount, 30min is extracted at 75 DEG C, filter, medicinal residues add the ethanol extraction 20min of 4 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 65% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
In step (3), addition 150-180 part of distilled water as well.
Claims (8)
1. a Chinese herbal medicine skin mucosa pasteurization towelette, comprise sterilizing non-woven fabrics, the disinfectant be carried on sterilizing non-woven fabrics, it is characterized in that: described disinfectant is prepared by following step: (1) takes Radix Scutellariae 15 parts, Flos Lonicerae 15 parts, grapefruit 15 parts, Aloe 8 parts, lavandula angustifolia 4 parts, add the ethanol of 6-8 times amount, 30-35min is extracted at 70-80 DEG C, filter, medicinal residues add the ethanol extraction 20-25min of 4-5 times amount again, filter, merging filtrate, add activated carbon decolorizing, filter, filtrate distillation and concentration is for subsequent use to 0.3 times of original volume;
(2) take 8 parts, Bulbus Allii, the ethanol adding appropriate 60%-70% fully grinds, and filter, filtrate is for subsequent use;
(3) Mentholum 4 parts, glycerol 2 parts, chitosan quaternary ammonium salt 2 parts is taken, zephiran 0.3 part, Palmic acid sucrose ester 8 parts, adding distil water stirring and dissolving;
(4) liquid obtained for step (2) agent step (3) is joined in the concentrated solution in step (1), stirring and dissolving and get final product.
2. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: described Chinese herbal medicine skin mucosa pasteurization towelette sterilizing non-woven fabrics is placed in above-mentioned disinfectant to soak after 0.5-1 hour obtained.
3. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: the white vinegar adding 0.5-1 part in the process of lapping of Bulbus Allii.
4. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: Bulbus Allii grinding is the ethanol grinding adding 0.5-1 times amount.
5. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: in described step (3), the addition of distilled water is 150-180 part.
6. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: described Bulbus Allii is only head purple garlic.
7. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: described Bulbus Allii is the Bulbus Allii slurry that fresh garlic is worn into.
8. a kind of Chinese herbal medicine skin mucosa pasteurization towelette according to claim 1, is characterized in that: described grapefruit is the sarcocarp after squeezing the juice in the Renhe of grapefruit.
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CN201410700284.5A CN104523466A (en) | 2014-11-28 | 2014-11-28 | Chinese herbal medicinal skin mucosa disinfection wet wipe |
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Cited By (4)
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CN107049848A (en) * | 2016-12-29 | 2017-08-18 | 安徽比伦生活用纸有限公司 | A kind of natural no stimulation wet tissue soak |
CN111773157A (en) * | 2020-07-28 | 2020-10-16 | 江苏省健尔康医用敷料有限公司 | Wet tissue and preparation method thereof |
CN112205425A (en) * | 2020-10-13 | 2021-01-12 | 湖南弘烨医疗器械有限公司 | Novel medical disinfection wet tissue and manufacturing method thereof |
CN112400905A (en) * | 2020-12-11 | 2021-02-26 | 陕西汤普医疗器械有限公司 | Acidic oxidation potential water antibacterial liquid and preparation method thereof |
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CN102552060A (en) * | 2011-12-30 | 2012-07-11 | 华侨大学 | Quaternized chitosan containing wet wipe compound liquid with functions of anti-bacteria, moisture retention and skin protection and preparation method thereof |
CN103169641A (en) * | 2013-03-14 | 2013-06-26 | 金红叶纸业集团有限公司 | Acne-removing and skin-clearing composition and tissue applying same |
CN103816089A (en) * | 2014-03-11 | 2014-05-28 | 广州市洋林生物科技开发有限公司 | Skin mucous menbrane antimicrobial fluid and skin mucous menbrane antimicrobial wet tissue |
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Patent Citations (4)
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CN102488705A (en) * | 2011-12-08 | 2012-06-13 | 施耐克江苏生物制药有限公司 | Skin mucous membrane disinfectant for killing virus |
CN102552060A (en) * | 2011-12-30 | 2012-07-11 | 华侨大学 | Quaternized chitosan containing wet wipe compound liquid with functions of anti-bacteria, moisture retention and skin protection and preparation method thereof |
CN103169641A (en) * | 2013-03-14 | 2013-06-26 | 金红叶纸业集团有限公司 | Acne-removing and skin-clearing composition and tissue applying same |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107049848A (en) * | 2016-12-29 | 2017-08-18 | 安徽比伦生活用纸有限公司 | A kind of natural no stimulation wet tissue soak |
CN111773157A (en) * | 2020-07-28 | 2020-10-16 | 江苏省健尔康医用敷料有限公司 | Wet tissue and preparation method thereof |
CN111773157B (en) * | 2020-07-28 | 2022-04-12 | 健尔康医疗科技股份有限公司 | Wet tissue and preparation method thereof |
CN112205425A (en) * | 2020-10-13 | 2021-01-12 | 湖南弘烨医疗器械有限公司 | Novel medical disinfection wet tissue and manufacturing method thereof |
CN112400905A (en) * | 2020-12-11 | 2021-02-26 | 陕西汤普医疗器械有限公司 | Acidic oxidation potential water antibacterial liquid and preparation method thereof |
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