CN104510675A - Hand sanitizer containing bamboo vinegar and preparation method thereof - Google Patents
Hand sanitizer containing bamboo vinegar and preparation method thereof Download PDFInfo
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- CN104510675A CN104510675A CN201510018554.9A CN201510018554A CN104510675A CN 104510675 A CN104510675 A CN 104510675A CN 201510018554 A CN201510018554 A CN 201510018554A CN 104510675 A CN104510675 A CN 104510675A
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Abstract
The invention belongs to the technical field of hand sanitizers, and particularly relates to a hand sanitizer containing bamboo vinegar. The hand sanitizer is prepared from the following raw materials in percentages by weight: 10-15% of bamboo vinegar, 10-20% of sodium fatty acid methyl ester sulfonate, 5-9% of alcohol ether carboxylate, 2-10% of jasmine flower extracting solution, 1-5% of NaCl and the balance of deionized water. The invention further provides a preparation method of the hand sanitizer. The preparation method comprises the following steps: adding deionized water in a stirring kettle, maintaining the temperature inside the kettle to be 60-70 DEG C, adding sodium fatty acid methyl ester sulfonate and alcohol ether carboxylate in sequence, stirring and homogenizing for 60-80 min, then adding the jasmine flower extracting solution, bamboo vinegar and NaCl, continuously stirring and homogenizing for 40-60 min, adjusting the pH value to be 7.35-7.45, and filling, so as to obtain the hand sanitizer containing bamboo vinegar. The hand sanitizer disclosed by the invention has a bactericidal effect, has good effects for cleaning and maintaining hand skin, and is non-toxic; waste liquid after hand washing does not pollute the environment, and is also beneficial for the treatment of waste water; the preparation method is simple in preparation technology and easy for operation.
Description
Technical field
The invention belongs to handwashing liquid technical field, be specifically related to a kind of handwashing liquid of bamboo vinegar liquid.
Background technology
People's hand-washing article in the past mainly soap, fancy soap etc., easy landing when they use, chance water logging, high temperature can be softened and naturally expend again, especially dirt on hand, antibacterial is easily infected with, become secondary pollution source, in addition, fancy soap, soap cleaning force are strong, but the zest had to a certain degree, life-time service can cause hand skin coarse.Along with the transformation of growth in the living standard and consumption idea, handwashing liquid becomes the succedaneum of traditional hand-washing article gradually, and oneself is widely used in the various places such as hospital, hotel, food and drink, family at present.The contact surface of handwashing liquid and hands is generally bottle pump head, easy to clean, avoids cross infection.By squash type taken amount, only need gently press nozzle, liquid just flows into the palm of the hand, and consumption is grasped by oneself, and it is all very convenient to deposit use.
Nowadays, along with the maturation of handwashing liquid production technology and the universal of market, the special handwashing liquid with various special efficacy has also constantly come out.As heavy duty detergent handwashing liquid, paint-removing handwashing liquid, anhydrous washing hand liquid, disinfection handwashing liquid etc.Wherein, disinfection handwashing liquid is the class that in the special handwashing liquid in market, occupancy volume is maximum.It is reported, the existing disinfection handwashing liquid commercially generally used, the effectiveness comparison in disinfection is desirable.But not good enough to considering in the nursing of hand skin, the component of disinfection is comparatively large to the zest of skin, life-time service easily cause hand skin dry, coarse, teach and split and peel.
Bamboo vinegar solution, is in the process of making charcoal with bamboo wood, collects the gas that bamboo wood produces in pyrolytic, and this gas is cooled at normal temperatures the liquid substance obtained.Bamboo vinegar solution contains nearly 300 kinds of natural polymer organic compound, the alkaline components etc. of organic acid, alcohols, ketone, aldehydes, esters and trace, use has no side effect, therefore can add in various cosmetics, its main component acetic acid can softening skin surface horny layer, and has the effect of convergence skin; Alcohols material contained by it can not only cleaning skin, and also has sterilization, disinfective action; Contained Ester penetrating power is strong, and can penetrate to the skin the nutritional labeling of cosmetics depths, improves skin effect; Antibacterial, non-stimulated, help speed-raising treatment small pox, subtract and take off skin inflammation and general red phenomenon thoroughly removes body soil and antibacterial, the unimpeded pore got clogged, controlled Sheng oils and fats; It also has extremely strong antioxidation.
Bamboo vinegar solution is applied to handwashing liquid field, there is very large sight.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of handwashing liquid of bamboo vinegar liquid, and this handwashing liquid has bactericidal action, and have good effects to the maintenance of hand skin clean, nontoxic, the waste liquid washing hands is not only free from environmental pollution, but also is conducive to the process of waste water.
For achieving the above object, the present invention adopts following technical scheme:
A handwashing liquid for bamboo vinegar liquid, be made up of the raw material of following percentage by weight:
Preferably, the handwashing liquid of bamboo vinegar liquid of the present invention, be made up of the raw material of following percentage by weight:
Bamboo vinegar solution of the present invention can be raw liquid of bamboo vinegar or smart Bamboo vinegar solution, preferably, the present invention select relative density be 1.02 ~ 1.06 Bamboo vinegar solution.Bamboo vinegar solution extracts to concentrate from natural plants, the acidic liquid product obtained when being bamboo wood carbonized.In Bamboo vinegar solution, contained esters penetration is strong, nutritional labeling can be added to skin depths, and contained acetic acid can softening skin horny layer, has good effects, and has no side effect, but kill pathogenic bacterium significantly active to skin clean maintenance.When the handwashing liquid of bamboo vinegar liquid composition is finished discharge, can also use as waste water treating agent, protection of the environment.The result of study of Inst. of Environment Engineering, Zhongnan Forest College shows, during with Bamboo vinegar solution process sanitary wastewater, only need the Bamboo vinegar solution of 1% that the removal effect of CODcr (COD) can be made to improve 10%, it is significant to the contribution of environmental protection.
The relative density of the Flos Jasmini Sambac extracting solution selected of the present invention is 1.10 ~ 1.20.Derived essential oil delicate fragrance in Flos Jasmini Sambac extracting solution is natural, traditional compound essence can be replaced, natural health, have staff and well nurse moisture-keeping function, Flos Jasmini Sambac extracting solution also has antioxidation, can be used as natural antiseptic agent, the Flavonoid substances simultaneously in Flos Jasmini Sambac extracting solution also has good bactericidal action.
In the present invention, methyl sodiosul foaliphatate is from natural plant grease synthesis, and moderate notoxic is a kind of novel environment friendly surfactant of scourability excellence.It has excellent surface activity and outstanding anti-hard water washability, and safety is good, meets the instructions for use of body care product.
In the present invention, alcohol ether carboxylate is the achievement in research of country " 95 " tackling of key scientific and technical problems that Chinese daily use chemicals institute bears, and is the novel multi-functional anion surfactant of a class.Its main environment shows as easily biological-degradable, and the degradation rate of OECD demonstration test is 98%, can degradablely be CO in natural environment
2and water, nontoxic, non-stimulated, use safety.
The present invention also provides the preparation method of the handwashing liquid of bamboo vinegar liquid, preparation process is: deionized water is added stirred tank, temperature in the kettle is kept to be 60 ~ 70 DEG C, add methyl sodiosul foaliphatate, alcohol ether carboxylate successively, stir homogenizing 60 ~ 80min, then add Flos Jasmini Sambac extracting solution, Bamboo vinegar solution and NaCl, continue to stir homogenizing 40 ~ 60min, adjust ph is 7.35 ~ 7.45, fill, i.e. the handwashing liquid of obtained bamboo vinegar liquid.
The present invention's concentration be 1mol/L sodium carbonate or sodium bicarbonate to regulate the pH value of handwashing liquid, sodium carbonate used or sodium bicarbonate are food stage, do not injure skin.
Beneficial effect of the present invention is:
1, handwashing liquid of the present invention plays the effect of fungi-proofing sterilization, there is the effect such as cleaning skin and sterilization, sterilization, antiinflammatory, also have hand skin and tighten skin, blood circulation promoting, pachylosis, allergic dermatitis are also had to the effect of auxiliary treatment, there is the effect that fine decontamination is clean.
2, raw materials used gentle environmental protection of the present invention, environmentally safe, Bamboo vinegar solution can also process waste water, improves the effect of water quality.
3, the inventive method preparation technology is simple, is easy to operation.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described, but the present invention is not limited to these embodiments.
Embodiment 1
55kg deionized water is added stirred tank, temperature in the kettle is kept to be 60 DEG C, add 20kg methyl sodiosul foaliphatate, 5kg alcohol ether carboxylate successively, stir homogenizing 80min, add again 9kg relative density be 1.10 Flos Jasmini Sambac extracting solution, 10kg relative density be 1.06 Bamboo vinegar solution and 1kg NaCl, continue to stir homogenizing 40min, adjust ph is 7.35, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
Embodiment 2
59kg deionized water is added stirred tank, temperature in the kettle is kept to be 65 DEG C, add 18kg methyl sodiosul foaliphatate, 6kg alcohol ether carboxylate successively, stir homogenizing 65min, add again 2kg relative density be 1.12 Flos Jasmini Sambac extracting solution, 11kg relative density be 1.05 Bamboo vinegar solution and 4kg NaCl, continue to stir homogenizing 45min, adjust ph is 7.37, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
Embodiment 3
57kg deionized water is added stirred tank, temperature in the kettle is kept to be 65 DEG C, add 15kg methyl sodiosul foaliphatate, 7kg alcohol ether carboxylate successively, stir homogenizing 70min, add again 6kg relative density be 1.15 Flos Jasmini Sambac extracting solution, 12kg relative density be 1.04 Bamboo vinegar solution and 3kg NaCl, continue to stir homogenizing 50min, adjust ph is 7.40, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
Embodiment 4
51kg deionized water is added stirred tank, temperature in the kettle is kept to be 70 DEG C, add 13kg methyl sodiosul foaliphatate, 8kg alcohol ether carboxylate successively, stir homogenizing 75min, add again 10kg relative density be 1.17 Flos Jasmini Sambac extracting solution, 14kg relative density be 1.03 Bamboo vinegar solution and 4kg NaCl, continue to stir homogenizing 55min, adjust ph is 7.42, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
Embodiment 5
56kg deionized water is added stirred tank, temperature in the kettle is kept to be 65 DEG C, add 10kg methyl sodiosul foaliphatate, 9kg alcohol ether carboxylate successively, stir homogenizing 80min, add again 5kg relative density be 1.20 Flos Jasmini Sambac extracting solution, 15kg relative density be 1.02 Bamboo vinegar solution and 5kg NaCl, continue to stir homogenizing 60min, adjust ph is 7.45, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
Test example
1, irritation test: select the healthy rabbit that 3 about 2kg skin is intact, remove with the hair of depilatory by family's rabbit back spinal column both sides, must not injured skin.Unhairing scope, left and right each about 3cm*3cm.Picking handwashing liquid stock solution with cotton swab smears on the unhairing intact skin of rabbit side, washes away residual handwashing liquid after 4h with warm water.Rabbit opposite side skin of unhairing, as blank, is smeared once, is smeared 14d continuously every day.24h observed result after at every turn smearing.Test display, 3 rabbit skin of back none produce redness, inflammation, phenomenon, experimental group and the matched group indifference such as to fester.Prove that this handwashing liquid is to no skin irritation.
2, bactericidal assay:
In Suspension quantitative bactericidal test, first get the Bacillus proteus after activation, escherichia coli, staphylococcus, Diplococcus pneumoniae and tubercule bacillus and be seeded in triangle shaking flask, 37 DEG C, 160r/min shaken cultivation 36h.Then inoculate the above-mentioned bacteria suspension of 1ml respectively to mix with 2% diluent of the handwashing liquid of 9ml embodiment 1 ~ 5 respectively, 37 DEG C, 160r/min vibrates 30min, measure the kill oncomelania of detergent to Bacillus proteus, escherichia coli, staphylococcus, Diplococcus pneumoniae and tubercule bacillus by the dilution method of falling ware, calculating bactericidal effect is as table 1:
Table 1 embodiment 1 ~ 5 bactericidal effect tables of data
| Strain | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Bacillus proteus | 97％ | 98％ | 98％ | 94％ | 95％ |
| Escherichia coli | 90％ | 93％ | 95％ | 95％ | 94％ |
| Staphylococcus | 97％ | 98％ | 99％ | 96％ | 95％ |
| Diplococcus pneumoniae | 94％ | 92％ | 94％ | 94％ | 93％ |
| Tubercule bacillus | 95％ | 96％ | 98％ | 94％ | 92％ |
Claims (5)
1. a handwashing liquid for bamboo vinegar liquid, is characterized in that, is made up of the raw material of following percentage by weight:
2. the handwashing liquid of bamboo vinegar liquid according to claim 1, is characterized in that, is made up of the raw material of following percentage by weight:
3. the handwashing liquid of bamboo vinegar liquid according to claim 1 and 2, is characterized in that: described Bamboo vinegar solution relative density is 1.02 ~ 1.06.
4. the handwashing liquid of bamboo vinegar liquid according to claim 1 and 2, is characterized in that: the relative density of described Flos Jasmini Sambac extracting solution is 1.10 ~ 1.20.
5. the preparation method of the handwashing liquid of a bamboo vinegar liquid, it is characterized in that, preparation process is: deionized water is added stirred tank, keeps temperature in the kettle to be 60 ~ 70 DEG C, adds methyl sodiosul foaliphatate, alcohol ether carboxylate successively, stir homogenizing 60 ~ 80min, add Flos Jasmini Sambac extracting solution, Bamboo vinegar solution and NaCl again, continue to stir homogenizing 40 ~ 60min, adjust ph is 7.35 ~ 7.45, fill, the i.e. handwashing liquid of obtained bamboo vinegar liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510018554.9A CN104510675A (en) | 2015-01-14 | 2015-01-14 | Hand sanitizer containing bamboo vinegar and preparation method thereof |
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| CN201510018554.9A CN104510675A (en) | 2015-01-14 | 2015-01-14 | Hand sanitizer containing bamboo vinegar and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265350A (en) * | 2016-09-22 | 2017-01-04 | 长兴净安环保科技有限公司 | A kind of bacteriostatic hand sanitizer and preparation method thereof |
| CN106265382A (en) * | 2016-10-14 | 2017-01-04 | 柳州立洁科技有限公司 | A kind of disinfection hand cleanser and preparation method thereof |
| CN106309330A (en) * | 2016-10-14 | 2017-01-11 | 柳州立洁科技有限公司 | High-efficient moisturizing cleaning hand-washing solution and preparation method thereof |
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| CN101708289A (en) * | 2009-11-30 | 2010-05-19 | 浙江工业大学 | Preparation method for bamboo vinegar antibacterial liquid |
| CN102397180A (en) * | 2010-09-16 | 2012-04-04 | 崔士强 | Hand-washing solution with nourishing effect |
| CN103222942A (en) * | 2013-05-17 | 2013-07-31 | 江阴中利生物技术有限公司 | Chinese herbal medicine foot bath solution added with bamboo vinegar and preparation method thereof |
| CN104152287A (en) * | 2014-08-29 | 2014-11-19 | 周可幸 | Bactericidal and anti-bacterial type tableware detergent |
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2015
- 2015-01-14 CN CN201510018554.9A patent/CN104510675A/en active Pending
Patent Citations (4)
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| CN101708289A (en) * | 2009-11-30 | 2010-05-19 | 浙江工业大学 | Preparation method for bamboo vinegar antibacterial liquid |
| CN102397180A (en) * | 2010-09-16 | 2012-04-04 | 崔士强 | Hand-washing solution with nourishing effect |
| CN103222942A (en) * | 2013-05-17 | 2013-07-31 | 江阴中利生物技术有限公司 | Chinese herbal medicine foot bath solution added with bamboo vinegar and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265350A (en) * | 2016-09-22 | 2017-01-04 | 长兴净安环保科技有限公司 | A kind of bacteriostatic hand sanitizer and preparation method thereof |
| CN106265382A (en) * | 2016-10-14 | 2017-01-04 | 柳州立洁科技有限公司 | A kind of disinfection hand cleanser and preparation method thereof |
| CN106309330A (en) * | 2016-10-14 | 2017-01-11 | 柳州立洁科技有限公司 | High-efficient moisturizing cleaning hand-washing solution and preparation method thereof |
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Application publication date: 20150415 |