CN104480696B - A kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique - Google Patents
A kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique Download PDFInfo
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Abstract
The present invention relates to a kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique, belong to fabrics printing and dyeing processing technique field.Resistant slide finishing agent is made up of following component in percentage by weight: silicon dioxide gel 20～40%, silicate solutions 30～60%, hydroxy Al 5～10%, polythene wax emulsion 5～8%, remaining is water.Compared with prior art, its remarkable advantage is the present invention: first, and consumption is low, just can reach excellent effect under the consumption of this finishing agent consumption 3～8g/L, good with the compatibility of softening agent, does not affect fabric feeling while improving the resistant slide performance of fabric.Second, compounding a certain amount of Tissuemat E improves fabric anti-fluffing anti-pilling performance.
Description
Technical field
The present invention relates to a kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique, belong to and spin
Fabric dyeing and printing process technical field.
Background technology
Sliding phenomenon is the most common in the fabric being made up of the raw material that the coefficient of friction such as tencel, Modal is less, owing to this type of regenerates
There is not natural distortion, surface relative smooth in cellulose fibre, have employed again some short textures, the specifications design of long floating-point,
Inevitably produce sliding；On the other hand will necessarily arrange through softening agent in postfinishing process, the addition fall of softening agent
The low surface tension of fiber, decreases the friction between yarn, and in order to reach the effect of Silk, the many selections of softening agent type
Smooth type, is so easier to cause fabric slippage.Moreover, owing to the addition of softening agent decreases the friction between yarn, fall
Low interfibrous cohesive force, also can reduce the anti-fluffing and anti-pilling performance of fabric simultaneously.Current resistant slide finishing agent mainly with
Fiber surface film forming and between the fibers performance network cross-linked structure two ways play resistant slide and certain anti-fluffing and anti-pilling effect
Really, but though film forming analog assistant does not affect feel, but resistant slide effect is bad；Though becoming network cross-linked analog assistant can reach preferable
Resistant slide effect, but affect fabric feeling, the most puckery.Patent CN103031718A discloses a kind of resistant slide dressing liquid formula,
The resistant slide finishing agent of its 50～60g/L consumption, the resin finishing agent of 25g/L consumption, although preferable resistant slide can be obtained and resist
Pilling effect, but it is clear that consumption is too big, affects the feel of fabric very much.Patent CN101864634A discloses one
Textile for air sacs, by individually padding organosilicon sliding dressing liquid in postfinishing process, prepared fabric has in suture site
Preferably slipping property.Because as automotive airbag fabric, less demanding to the feel of fabric, the most in fact this fabric feeling is also
Bad.
Summary of the invention
The technical problem to be solved is: the use of conventional fabric resistant slide finishing agent influences whether the feel of fabric,
A kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique are proposed.
Technical scheme:
According to an aspect of the present invention, a kind of regenerated celulose fibre fabric resistant slide finishing agent, by percentage by weight
Following component formed: silicon dioxide gel 20～40%, silicate solutions 30～60%, hydroxy Al 5～10%, polyethylene
Wax emulsion 5～8%, remaining is water.
Described silicate solutions refers to the arbitrary proportion mixing of the one or two kinds of in sodium silicate solution or potassium silicate solution
Thing.
Described silicate solutions processed through acid cation-exchanger, or acidified.
Described acidifying refers to add mineral acid in silicate solutions；Described mineral acid selected from sulphuric acid, hydrochloric acid, phosphoric acid,
One or several mixture in nitric acid.
The content of the described sodium silicate in sodium silicate solution is 10～30wt%, containing of the described potassium silicate in potassium silicate solution
Amount is 10～30wt%.
Described silicate solutions is according to weight ratio (0.5～2) by sodium silicate solution and potassium silicate solution: form mixed by 1.
The range of solid content of described silicon dioxide gel is 5～45wt%, preferably 10～30wt%, further preferably 15～25wt%,
Most preferably 20wt%.
Silicon dioxide particle diameter in described silicon dioxide gel is 1～15nm.
The solid content 15～50wt% of described polythene wax emulsion, preferably 20～40wt%, most preferably 30wt%.
Tissuemat E molecular weight ranges 500～1000 in described polythene wax emulsion, emulsifying agent is sodium lauryl sulphate.
According to another aspect of the present invention, the textile pad working solution of above-mentioned resistant slide finishing agent is included.
The content of the resistant slide finishing agent in described working solution is 3～8g/L.
Described working solution also includes softening agent 20～40g/L.
Described softening agent is cation or nonionic softening agent.
According to another aspect of the present invention, a kind of regenerated celulose fibre fabric resistant slide finishing technique, comprise the steps:
Regenerated celulose fibre fabric is padded process in working solution, then through shaping process.
Pad and be processed as 1 leaching 1 and roll, pick-up 70～80%.
The temperature range 160 of described shaping process～170 DEG C.
Beneficial effect
First, consumption is low, just can reach excellent effect, with the compatibility of softening agent under the consumption of this finishing agent consumption 3～8g/L
Property good, improve fabric resistant slide performance while do not affect fabric feeling.Second, compounding a certain amount of Tissuemat E improves to be knitted
Thing anti-fluffing and anti-pilling performance.
Detailed description of the invention
Below by detailed description of the invention, the present invention is described in further detail.It will be apparent, however, to one skilled in the art, that it is following
Embodiment is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.Unreceipted concrete technology or condition in embodiment
Person, according to the technology described by the document in this area or condition (" dyeing and finishing technology and the principle " such as write with reference to Zhao Tao, in
Weaving publishing house of state, 2009) or carry out according to product description.Agents useful for same or instrument unreceipted production firm person, being can
With by city available from conventional products.
The number as range limit not only including clearly listing should be interpreted as in a flexible way using the value of range format expression
Value, but also include containing all single numerical value within the range or subinterval, just as each numerical value and subinterval are clearly arranged
Enumerate.Such as, the concentration range of " about 0.1% to about 5% " should be understood to not only to include clearly to list about 0.1% to
The concentration of about 5%, also includes the single concentration (e.g., 1%, 2%, 3% and 4%) in the range of indication and subinterval is (such as,
0.1% to 0.5%, 1% to 2.2%, 3.3% to 4.4%).
Percentage ratio % in following example is mass percent in the case of without specified otherwise.
The silicon dioxide gel used in the present invention is the colloidal sol thing containing nano SiO 2 particle, and this inorganic polysilicate exists
Dehydrated crosslinking in heating process, forms network structure with fibrous tissue IPN, has fettered the relative movement between fiber further,
Thus improve the sliding friction resistance between yarn and yarn, play good resistant slide effect.The silicon dioxide that the present invention uses
Sol particles particle diameter is preferably 1～15nm, and particle diameter is minimum, specific surface area is big, and the impact on fabric feeling is the least, these microgranules
It is linked into segment or netted and form three dimensional structure.The range of solid content of silicon dioxide gel is 5～45wt%, preferably 10～
30wt%, further preferably 15～25wt%, most preferably 20wt%.
In order to improve the stability of silicon dioxide gel further, finishing agent also includes silicate solutions, and silicate
Solution self also has certain adhesive power, and the slip resistance of fiber is also had certain help.The content range of silicate solutions
Preferably 10～30wt%.One or two kinds of in the preferred sodium silicate solution of silicate solutions or potassium silicate solution arbitrarily than
Example mixture, preferably under, the content of the sodium silicate in sodium silicate solution is preferably 10～30wt%, potassium silicate solution
In the content of potassium silicate be preferably 10～30wt%.In a preferred embodiment, silicate solutions is by sodium silicate solution
With potassium silicate solution according to weight ratio (0.5～2): form mixed by 1, more preferably 1:1, it is possible to obtain more excellent antiskid
Performance.In an other embodiment, silicate solutions is to process through acid cation-exchanger, or passes through
Acidifying, acidifying refers to add mineral acid in silicate solutions；Described mineral acid is selected from sulphuric acid, hydrochloric acid, phosphoric acid, nitric acid
In one or several mixture, the effect of acidifying is that regulation arranges pH value also by introducing hydrion, make solution in
Faintly acid, promotes silicate solutions and the compatibility of softening agent in working solution.
In finishing agent, also include hydroxy Al 5～10%.After dressing liquid is acidified, if hydrogen ion concentration is high, silicate is molten
Liquid can produce coacervation, and hydroxy Al itself is a kind of solution stabilizer, adds hydroxy Al and can ensure that the stability of solution and divide
Dissipate property.
Addition 5～8% polythene wax emulsion, it is therefore an objective to slip property promotes meanwhile, it is capable to improve the pilling resistance of fabric.
The solid content 15～50wt% of polythene wax emulsion, preferably 20～40wt%, most preferably 30wt%.In described polythene wax emulsion
Tissuemat E molecular weight ranges 500～1000, emulsifying agent is sodium lauryl sulphate.
In use, it is configured at above-mentioned resistant slide finishing agent to pad and uses in working solution, preferably using in working solution
Amount is 3～8g/L, can also add softening agent 20～40g/L to improve fabric feeling in working solution, and softening agent is preferably sun
Ion or nonionic softening agent.
Use above-mentioned padding with the finishing technique of working solution, regenerated celulose fibre fabric can be padded place in working solution
Reason, then through shaping process.Pad process preferably 1 leaching 1 to roll, pick-up 70～80%.The temperature model of shaping process
Enclose preferably 160～170 DEG C.
Unit " part " described in following example, in the case of without special instruction, is all weight portion.
Embodiment 1
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 50 DEG C and stirring well, the silicon dioxide gel (solid content 30wt%) of 20 parts is added slowly
In the sodium silicate of 30 parts (content 10wt%) potassium silicate solution (content 30wt%) with 15 parts, it is simultaneously introduced the hydroxyl of 10 parts
Aluminum, stirs, and prepares solution A.Secondly, by the polythene wax emulsions of 5 parts (solid content 20%, molecular weight ranges 500～
1000, wherein emulsifying agent is agent sodium lauryl sulphate) join in 20 parts of water, under high-temperature and high-pressure conditions, carry out emulsifying, system
Obtain B emulsion.Finally it is added slowly to solution A in B emulsion be stirred uniformly, obtaining the resistant slide finishing agent of the present invention.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
Reference examples 1
Difference with embodiment 1 is: do not add silicate solutions (replacing with water) in the composition of resistant slide finishing agent, remaining step
Rapid the most identical.More specifically, as follows:
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 50 DEG C and stirring well, the silicon dioxide gel (solid content 30wt%) of 20 parts is added slowly
In 45 parts of water, it is simultaneously introduced the hydroxy Al of 10 parts, stirs, prepare solution A.Secondly, by the Tissuemat E of 5 parts
Emulsion (wherein emulsifying agent is agent sodium lauryl sulphate for solid content 20%, molecular weight ranges 500～1000) joins 20 parts
In water, under high-temperature and high-pressure conditions, carry out emulsifying, prepare B emulsion.Finally it is added slowly to solution A B emulsion is stirred
Uniformly, resistant slide finishing agent is obtained.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
Reference examples 2
Difference with embodiment 1 is: do not add polythene wax emulsion (replacing with water) in the composition of resistant slide finishing agent, remaining
Step is the most identical.More specifically, as follows:
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 50 DEG C and stirring well, the silicon dioxide gel (solid content 30wt%) of 20 parts is added slowly
In the sodium silicate of 30 parts (content 10wt%) potassium silicate solution (content 30wt%) with 15 parts, it is simultaneously introduced the hydroxyl of 10 parts
Aluminum, stirs, and prepares solution A.Solution A is joined in 25 parts of water, be stirred uniformly, obtain resistant slide and arrange
Agent.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
Performance test
1. slip property test result
According to GB/T 13772.2-2008 " the mensuration part 2 of textile woven fabric seam crossing yarn resistant slide: constant load
Method " measure fabric anti-slipping property
The slip property test result of table 1 fabric
2. feel detection
Pliability and smooth degree according to AATCC feel testing standard (AATCC Test Method 202-2012) test fabric.
Table 2 fabric feeling test result
By in table 1 it can be seen that the resistant slide effect of resistant slide finishing agent that the present invention uses is better than the anti-of common film forming class
Sliding agent, and contrasted it can be seen that pass through to add silicate solutions in finishing agent by reference examples 1 and embodiment 1, can
To avoid slippage further；Contrasted by reference examples 2 and embodiment 1 it can be seen that gather by adding in finishing agent
Ethylene waxes, can promote the performance of resistant slide performance and anti-fluffing and anti-pilling simultaneously.From Table 2, it can be seen that what the present invention provided
Resistant slide finishing agent, while improve and doing slip property, also can guarantee that have preferable fabric feeling.
Embodiment 2
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 60 DEG C and stirring well, the silicon dioxide gel (solid content 30wt%) of 40 parts is added slowly
In the sodium silicate of 20 parts (content 25wt%) potassium silicate solution (content 20wt%) with 25 parts, it is simultaneously introduced the hydroxy Al of 5 parts,
Stir, prepare solution A.Secondly, by the polythene wax emulsions of 8 parts (solid content is respectively adopted 15%, 20%, 30%,
40%, molecular weight ranges 500～1000, wherein emulsifying agent is agent sodium lauryl sulphate) join in 12 parts of water, at high temperature
Carry out emulsifying under condition of high voltage, prepare B emulsion.Finally it is added slowly to solution A in B emulsion be stirred uniformly, obtaining this
The resistant slide finishing agent of invention.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
Under conditions of the solid content of different Tissuemat Es, fabric property testing result is as follows:
The slip property test result of table 3 fabric
| 15% | 20% | 30% | 40% | |
| Warp-wise sliding (mm) | 4.05 | 4.10 | 3.86 | 4.09 |
| Broadwise sliding (mm) | 4.11 | 4.06 | 3.78 | 4.12 |
| Anti-fluffing and anti-pilling (level) | 3.0 | 3.0 | 3.5 | 3.0 |
Table 4 fabric feeling test result
As can be seen from the table, control the solid content of Tissuemat E, in the range of preferably, can ensure that fabric has further
More preferably anti-slipping property and feel.
Embodiment 3
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 60 DEG C and stirring well by the silicon dioxide gel of 20 parts (solid content be respectively 5wt%, 10wt%,
20wt%, 25wt%, 30wt%, 45wt%) it is added slowly to the sodium silicate (content 15wt%) of 20 parts and the silicic acid of 35 parts
In potassium solution (content 10wt%), it is simultaneously introduced the hydroxy Al of 5 parts, stirs, prepare solution A.Secondly, by 5 parts
Polythene wax emulsion (wherein emulsifying agent is agent sodium lauryl sulphate for solid content 30%, molecular weight ranges 500～1000) adds
Enter in 15 parts of water, under high-temperature and high-pressure conditions, carry out emulsifying, prepare B emulsion.Finally solution A is added slowly to B emulsion
In be stirred uniformly, obtaining the resistant slide finishing agent of the present invention.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
Fabric performance is as follows:
The slip property test result of table 5 fabric
Table 6 fabric feeling test result
As can be seen from the table, when being controlled by the solid content of silicon dioxide gel in the range of preferably, fabric can be made to have more preferably
Feel and anti-slipping property.
Embodiment 4
Difference with embodiment 3 is: silicate solutions refers to the solution through being acidified through persalt, and its pH is about 5.5～6.0.
The fabric used is: Modal 40S* Modal 40S/133*76 printed fabric
First, under 60 DEG C and stirring well, the silicon dioxide gel (solid content is 20wt%) of 20 parts is added slowly
The sodium silicate (content 15wt%) entered to 20 parts, with the potassium silicate solution (content 10wt%) of 35 parts, is simultaneously introduced the hydroxyl of 5 parts
Aluminum, stirs, and prepares solution A.Secondly, by the polythene wax emulsions of 5 parts (solid content 30%, molecular weight ranges 500～
1000, wherein emulsifying agent is agent sodium lauryl sulphate) join in 15 parts of water, under high-temperature and high-pressure conditions, carry out emulsifying, system
Obtain B emulsion.Finally it is added slowly to solution A in B emulsion be stirred uniformly, obtaining the resistant slide finishing agent of the present invention.
The preparation of housekeeping liquid is: in working solution use resistant slide finishing agent 3g/L, softening agent 20g/L, with formic acid, acetic acid,
Or the pH of citric acid regulating solution is 5.0, by Modal printed fabric immersing and rolling in working solution, pick-up 70%, 160
DEG C × 50s shapes.
After testing: fabric warp-wise sliding (mm) 3.22, broadwise sliding (mm) 3.11, anti-fluffing and anti-pilling (level) 3.5 grades,
Stiffness 10.21, pliability 14.32, planarization, 18.07.
Claims (10)
1. a regenerated celulose fibre fabric resistant slide finishing agent, it is characterized in that, it is made up of following component in percentage by weight: silicon dioxide gel 20～40%, silicate solutions 30～60%, hydroxy Al 5～10%, polythene wax emulsion 5～8%, remaining is water.
Regenerated celulose fibre fabric resistant slide finishing agent the most according to claim 1, it is characterised in that: described silicate solutions refers to the arbitrary proportion mixture of the one or two kinds of in sodium silicate solution or potassium silicate solution.
Regenerated celulose fibre fabric resistant slide finishing agent the most according to claim 2, it is characterised in that: described silicate solutions processed through acid cation-exchanger, or acidified；Described acidifying refers to add mineral acid in silicate solutions；The described mineral acid one or several mixture in sulphuric acid, hydrochloric acid, phosphoric acid, nitric acid.
Regenerated celulose fibre fabric resistant slide finishing agent the most according to claim 1, it is characterised in that: the content of the described sodium silicate in sodium silicate solution is 10～30wt%, and the content of the described potassium silicate in potassium silicate solution is 10～30wt%；Described silicate solutions is according to weight ratio (0.5～2) by sodium silicate solution and potassium silicate solution: form mixed by 1.
Regenerated celulose fibre fabric resistant slide finishing agent the most according to claim 1, it is characterised in that: the range of solid content of described silicon dioxide gel is 5～45wt%；Silicon dioxide particle diameter in described silicon dioxide gel is 1～15nm.
Regenerated celulose fibre fabric resistant slide finishing agent the most according to claim 1, it is characterised in that: the solid content 15～50wt% of described polythene wax emulsion；Tissuemat E molecular weight ranges 500～1000 in described polythene wax emulsion, emulsifying agent is sodium lauryl sulphate.
7. include the textile pad working solution of resistant slide finishing agent described in any one of claim 1 to 6.
Textile pad working solution the most according to claim 7, it is characterised in that: the content of the resistant slide finishing agent in described working solution is 3～8g/L；Described working solution also includes softening agent 20～40g/L；Described softening agent is cation or nonionic softening agent.
9. a regenerated celulose fibre fabric resistant slide finishing technique, it is characterized in that, comprise the steps: in the textile pad working solution of the resistant slide finishing agent described in claim 7, regenerated celulose fibre fabric is padded process, then through shaping process.
Regenerated celulose fibre fabric resistant slide finishing technique the most according to claim 9, it is characterised in that: pad and be processed as 1 leaching 1 and roll, pick-up 70～80%；The temperature range 160 of described shaping process～170 DEG C.
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| CN201410717859.4A CN104480696B (en) | 2014-12-01 | 2014-12-01 | A kind of regenerated celulose fibre fabric resistant slide finishing agent, working solution and resistant slide finishing technique |
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| CN106592035B (en) * | 2016-11-23 | 2018-12-28 | 江西服装学院 | A kind of production technology of llama yarn |
| CN106757663B (en) * | 2016-11-23 | 2018-06-15 | 江西服装学院 | A kind of llama fabric and by its clothes obtained |
| CN109554922A (en) * | 2018-12-04 | 2019-04-02 | 江苏金太阳纺织科技股份有限公司 | A kind of fabric wet keeping finishing agent and its application |
| CN110106696A (en) * | 2019-05-30 | 2019-08-09 | 成都新柯力化工科技有限公司 | A kind of airsetting adhesive plaster meeting human skin soft comfortable degree and preparation method |
| CN111485425A (en) * | 2020-04-30 | 2020-08-04 | 烟台源明纺织科技有限公司 | Fiber anti-slippage agent and preparation method thereof |
| CN113969502B (en) * | 2021-11-18 | 2023-09-01 | 桐庐荣盛针织有限公司 | Anti-pilling knitted cap and manufacturing process thereof |
| CN115821588A (en) * | 2022-12-13 | 2023-03-21 | 周权有 | Fabric finishing agent for modal fabric and finishing method |
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| DE19502514A1 (en) * | 1994-02-03 | 1995-08-10 | Sandoz Ag | New finishing agent for textile fibres |
| CN101289540B (en) * | 2008-06-12 | 2011-12-14 | 广东纺织职业技术学院 | Method for preparing oxidic polyethylene wax microemulsion |
| CN101864634A (en) * | 2009-04-15 | 2010-10-20 | 东丽纤维研究所（中国）有限公司 | Fabric for airbags |
| CN102454106B (en) * | 2010-10-18 | 2014-02-12 | 南通斯恩特纺织科技有限公司 | Stiffening agent and production method thereof |
| CN103061105B (en) * | 2012-12-26 | 2015-02-11 | 安徽中天印染股份有限公司 | Printing anti-sliding process for ultrathin full-cotton wrinkle fabric |
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