CN104450277A - Preparation method for electroplating cleaning degreasing agent - Google Patents
Preparation method for electroplating cleaning degreasing agent Download PDFInfo
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- CN104450277A CN104450277A CN201410695215.XA CN201410695215A CN104450277A CN 104450277 A CN104450277 A CN 104450277A CN 201410695215 A CN201410695215 A CN 201410695215A CN 104450277 A CN104450277 A CN 104450277A
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Abstract
The invention relates to a preparation method for an electroplating cleaning degreasing agent. The preparation method is characterized by comprising the following steps: (1) weighing raw materials in parts by weight; (2) screening, namely screening the solid raw materials by using a vibrating sieve respectively; (3) mixing, namely weighing alkylphenol polyoxy diethyl ether, sodium carbonate, sodium metasilicate and trisodium phosphate in parts by weight and pouring the above components into a mixer for mixing for 5-10 minutes to obtain a mixture A; (4) stirring, namely stirring the mixture A with an anion active agent, a nonionic surfactant, a metal anti-rusting agent and a cleaning inhibitor by virtue of a stirrer for 25-30 minutes to obtain the cleaning degreasing agent. The cleaning degreasing agent prepared by the invention is convenient to use, and can quickly remove dirt such as grease, polishing paste, and handprints on the surface of a workpiece and meanwhile can remove the oxide layer on the surface of a copper layer. The degreasing agent is extremely excellent in cleaning effect, the manual work is saved, the reworking probability is reduced, and the product quality is improved and the service life is prolonged.
Description
Technical field
The present invention relates to field of electroplating, particularly a kind of compound method of electroplating with cleaning degreaser.
Background technology
When carrying out plating copper facing to workpiece, often because of reason that is various or artificial or technique, cause copper-plated, the goods and materials such as a large amount of greasy dirt, dust are adhered at workpiece surface, also can there is oxidation in various degree in workpiece surface simultaneously, produces zone of oxidation, thus need clean workpiece after copper facing, and when using traditional cleaning degreaser to clean, not only cleaning performance is bad, and residue is many, wastes time and energy simultaneously, very lost labor, and have a strong impact on quality product.
Summary of the invention
For the problems referred to above, the invention provides a kind of compound method of electroplating with cleaning degreaser.
For solving above technical problem, technical scheme provided by the invention is:
Electroplate the compound method with cleaning degreaser, it is characterized in that, described preparation method is as follows:
(1) starting material are taken by weight as follows:
Anion active agent 5-8 part, tween 3-5 part, alkylphenol polyoxy ether 8-10, part sodium carbonate 15-20 part, Starso 17-23 part, metal antirusting agent 15-18 part and cleaning inhibiter 2-5 part;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out alkylphenol polyoxy ether, sodium carbonate, Starso and tertiary sodium phosphate by weight, and all pour in mixing machine and mix, mixing time is 5-10 minute, obtains compound A;
(4) stir: compound A and anion active agent, tween, metal antirusting agent and cleaning inhibiter are stirred by stirrer, churning time is 25-30 minute, obtains cleaning degreaser.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, described anion active agent is that sodium laurylsulfonate and sodium lauryl sulphate mix in 1-1.5:1.5-1.8 ratio.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, described tween is that alkylphenol polyoxyethylene and fatty alcohol-polyoxyethylene ether mix in 1-1.3:1.5-1.6 ratio.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, the purity of described sodium carbonate is 98%.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, the purity of described tertiary sodium phosphate is 98%.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, described cleaning inhibiter is thiocarbamide.
Above-mentioned a kind of compound method of electroplating with cleaning degreaser, wherein, metal antirusting agent is tertiary sodium phosphate.
A kind of cleaning degreaser of being made of compound method electroplated with cleaning degreaser provided by the invention, not only easy to use, and the dirt such as grease, rubbing paste, impression of the hand of workpiece surface can be removed fast, the zone of oxidation on layers of copper surface can be removed simultaneously, cleaning performance is splendid, not only save artificial, reduce probability of doing over again, and improve quality and the work-ing life of product.
Embodiment
Embodiment one
Electroplate the compound method with cleaning degreaser, it is characterized in that, described preparation method is as follows:
(1) starting material are taken by weight as follows:
Anion active agent 5 parts, tween 5 parts, alkylphenol polyoxy ether 8 parts, 20 parts, sodium carbonate, Starso 17 parts, metal antirusting agent 18 parts and cleaning inhibiter 2 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out alkylphenol polyoxy ether, sodium carbonate, Starso and tertiary sodium phosphate by weight, and all pour in mixing machine and mix, mixing time is 8 minutes, obtains compound A;
(4) stir: compound A and anion active agent, tween, metal antirusting agent and cleaning inhibiter are stirred by stirrer, churning time is 25 minutes, obtains cleaning degreaser.
Wherein, anion active agent is that sodium laurylsulfonate and sodium lauryl sulphate mix in 1.3:1.5 ratio, described tween is that alkylphenol polyoxyethylene and fatty alcohol-polyoxyethylene ether mix in 1:1.6 ratio, the purity of described sodium carbonate is 98%, the purity of described tertiary sodium phosphate is 98%, described cleaning inhibiter is thiocarbamide, and metal antirusting agent is tertiary sodium phosphate.
Embodiment two
Electroplate the compound method with cleaning degreaser, it is characterized in that, described preparation method is as follows:
(1) starting material are taken by weight as follows:
Anion active agent 6 parts, tween 4 parts, alkylphenol polyoxy ether 9 parts, 19 parts, sodium carbonate, Starso 18 parts, metal antirusting agent 17 parts and cleaning inhibiter 3 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out alkylphenol polyoxy ether, sodium carbonate, Starso and tertiary sodium phosphate by weight, and all pour in mixing machine and mix, mixing time is 10 minutes, obtains compound A;
(4) stir: compound A and anion active agent, tween, metal antirusting agent and cleaning inhibiter are stirred by stirrer, churning time is 27 minutes, obtains cleaning degreaser.
Wherein, anion active agent is that sodium laurylsulfonate and sodium lauryl sulphate mix in 1.2:1.5 ratio, described tween is that alkylphenol polyoxyethylene and fatty alcohol-polyoxyethylene ether mix in 1.1:1.6 ratio, the purity of described sodium carbonate is 98%, the purity of described tertiary sodium phosphate is 98%, described cleaning inhibiter is thiocarbamide, and metal antirusting agent is tertiary sodium phosphate.
Embodiment three
Electroplate the compound method with cleaning degreaser, it is characterized in that, described preparation method is as follows:
(1) starting material are taken by weight as follows:
Anion active agent 7 parts, tween 4 parts, alkylphenol polyoxy ether 10,18 parts, sodium carbonate, Starso 19 parts, metal antirusting agent 16 parts and cleaning inhibiter 4 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out alkylphenol polyoxy ether, sodium carbonate, Starso and tertiary sodium phosphate by weight, and all pour in mixing machine and mix, mixing time is 8 minutes, obtains compound A;
(4) stir: compound A and anion active agent, tween, metal antirusting agent and cleaning inhibiter are stirred by stirrer, churning time is 28 minutes, obtains cleaning degreaser.
Wherein, anion active agent is that sodium laurylsulfonate and sodium lauryl sulphate mix in 1.3:1.7 ratio, described tween is that alkylphenol polyoxyethylene and fatty alcohol-polyoxyethylene ether mix in 1.1:1.7 ratio, the purity of described sodium carbonate is 98%, the purity of described tertiary sodium phosphate is 98%, described cleaning inhibiter is thiocarbamide, and metal antirusting agent is tertiary sodium phosphate.
A kind of cleaning degreaser of being made of compound method electroplated with cleaning degreaser, not only easy to use, and the dirt such as grease, rubbing paste, impression of the hand of workpiece surface can be removed fast, the zone of oxidation on layers of copper surface can be removed simultaneously, cleaning performance is splendid, not only save artificial, reduce probability of doing over again, and improve quality and the work-ing life of product.
The above; be only the present invention's preferably embodiment, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.
Claims (7)
1. electroplate the compound method with cleaning degreaser, it is characterized in that, described preparation method is as follows:
(1) starting material are taken by weight as follows:
Anion active agent 5-8 part, tween 3-5 part, alkylphenol polyoxy ether 8-10, part sodium carbonate 15-20 part, Starso 17-23 part, metal antirusting agent 15-18 part and cleaning inhibiter 2-5 part;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out alkylphenol polyoxy ether, sodium carbonate, Starso and tertiary sodium phosphate by weight, and all pour in mixing machine and mix, mixing time is 5-10 minute, obtains compound A;
(4) stir: compound A and anion active agent, tween, metal antirusting agent and cleaning inhibiter are stirred by stirrer, churning time is 25-30 minute, obtains cleaning degreaser.
2. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, described anion active agent is that sodium laurylsulfonate and sodium lauryl sulphate mix in 1-1.5:1.5-1.8 ratio.
3. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, described tween is that alkylphenol polyoxyethylene and fatty alcohol-polyoxyethylene ether mix in 1-1.3:1.5-1.6 ratio.
4. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, the purity of described sodium carbonate is 98%.
5. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, the purity of described tertiary sodium phosphate is 98%.
6. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, described cleaning inhibiter is thiocarbamide.
7. a kind of compound method of electroplating with cleaning degreaser as claimed in claim 1, it is characterized in that, metal antirusting agent is tertiary sodium phosphate.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410695215.XA CN104450277A (en) | 2014-11-27 | 2014-11-27 | Preparation method for electroplating cleaning degreasing agent |
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| CN201410695215.XA CN104450277A (en) | 2014-11-27 | 2014-11-27 | Preparation method for electroplating cleaning degreasing agent |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105331472A (en) * | 2015-11-20 | 2016-02-17 | 金川集团股份有限公司 | Alkaline electrolytic cleaning agent and cleaning method for electroplated parts |
| CN105542989A (en) * | 2015-12-09 | 2016-05-04 | 深圳市正天伟科技有限公司 | Acidic degreaser for preventing rack from being electroplated with copper and preparation method and application method of acidic degreaser |
| CN107227210A (en) * | 2017-06-20 | 2017-10-03 | 合肥尚涵装饰工程有限公司 | A kind of deoiling method of workpiece |
| CN109320761A (en) * | 2018-08-22 | 2019-02-12 | 佛山麟博科技新材料有限公司 | The preparation method of silicon rubber collection method, silica gel cloth separating liquid and separating liquid |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103710161A (en) * | 2013-12-31 | 2014-04-09 | 上海交通大学 | Cleaning agent for removing heavy dirt and greasy dirt |
| CN103805369A (en) * | 2014-03-04 | 2014-05-21 | 东莞市常晋凹版模具有限公司 | Copper-plated layer washing degreaser applied in electroplating industry |
| CN103911625A (en) * | 2014-04-25 | 2014-07-09 | 湖南大学 | Neutral oil removal rust remover and preparation method thereof |
| CN104047006A (en) * | 2014-06-23 | 2014-09-17 | 梧州恒声电子科技有限公司 | Method for removing oxide film from surface of copper |
-
2014
- 2014-11-27 CN CN201410695215.XA patent/CN104450277A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103710161A (en) * | 2013-12-31 | 2014-04-09 | 上海交通大学 | Cleaning agent for removing heavy dirt and greasy dirt |
| CN103805369A (en) * | 2014-03-04 | 2014-05-21 | 东莞市常晋凹版模具有限公司 | Copper-plated layer washing degreaser applied in electroplating industry |
| CN103911625A (en) * | 2014-04-25 | 2014-07-09 | 湖南大学 | Neutral oil removal rust remover and preparation method thereof |
| CN104047006A (en) * | 2014-06-23 | 2014-09-17 | 梧州恒声电子科技有限公司 | Method for removing oxide film from surface of copper |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105331472A (en) * | 2015-11-20 | 2016-02-17 | 金川集团股份有限公司 | Alkaline electrolytic cleaning agent and cleaning method for electroplated parts |
| CN105542989A (en) * | 2015-12-09 | 2016-05-04 | 深圳市正天伟科技有限公司 | Acidic degreaser for preventing rack from being electroplated with copper and preparation method and application method of acidic degreaser |
| CN105542989B (en) * | 2015-12-09 | 2018-07-31 | 深圳市正天伟科技有限公司 | A kind of acid deoiling agent preventing copper on hanger and its preparation and application |
| CN107227210A (en) * | 2017-06-20 | 2017-10-03 | 合肥尚涵装饰工程有限公司 | A kind of deoiling method of workpiece |
| CN109320761A (en) * | 2018-08-22 | 2019-02-12 | 佛山麟博科技新材料有限公司 | The preparation method of silicon rubber collection method, silica gel cloth separating liquid and separating liquid |
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Application publication date: 20150325 |