CN104371668B - A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof - Google Patents
A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof Download PDFInfo
- Publication number
- CN104371668B CN104371668B CN201410573720.7A CN201410573720A CN104371668B CN 104371668 B CN104371668 B CN 104371668B CN 201410573720 A CN201410573720 A CN 201410573720A CN 104371668 B CN104371668 B CN 104371668B
- Authority
- CN
- China
- Prior art keywords
- cooling liquid
- sodium
- freeze cooling
- water
- vaporization prevention
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/20—Antifreeze additives therefor, e.g. for radiator liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Thermal Sciences (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Lubricants (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：50 60%, water：30 40%, sodium tetraborate：1 2%, natrium nitrosum：1 2%, sodium hydroxide：0.1 0.3%, BTA：0.07 0.1%, calgon：0.1 0.2%, sodium metasilicate：0.2 0.5%, ﹣ 50# light diesel fuels or the machine oil of SN5W 30：4 5%, methanol or ethanol 0.08 1%；It is scattered 30 minutes in 400 turns/min with dispersion machine after each component is added when preparing the anti-freeze cooling liquid, it is filling that filtering is then carried out again.The present invention can effectively reduce the evaporation capacity of anti-freeze cooling liquid, and remaining index also complies with the regulation of concerned countries standard, and other performance parameters of anti-freeze cooling liquid are not interfered with while vaporization prevention, and engine will not be caused to damage.
Description
Technical field
The present invention relates to Antifreezing/Cooling Fluids for Automotives field, and in particular to a kind of vaporization prevention type anti-freeze cooling liquid and its preparation side
Method.
Background technology
The anti-freeze cooling liquid of enterprise's production both at home and abroad is generally ethylene glycol and water and adds some additives again at present, is starting
Machine is normal in use, because the temperature of engine is more than 80 DEG C, the water in anti-icing fluid can slowly evaporate, if can not and
When supplement water, then be likely to form potential safety hazard, it is therefore desirable to frequent moisturizing, certain trouble brought to user.
The content of the invention
The purpose of the present invention is to be directed to above-mentioned technical problem there is provided a kind of vaporization prevention type anti-freeze cooling liquid, and provides its system
Preparation Method.
The technical scheme that the present invention takes：
A kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：50-60%, water：30-40%, tetraboric acid
Sodium：1-2%, natrium nitrosum：1-2%, sodium hydroxide：0.1-0.3%, BTA：0.07-0.1%, calgon：0.1-
0.2%, sodium metasilicate：0.2-0.5%, ﹣ 50# light diesel fuels or SN5W-30 machine oil：4-5%, methanol or ethanol 0.08-1%；Above percentage
Than being mass percent.
The preparation method of vaporization prevention type anti-freeze cooling liquid of the present invention, it is comprised the following steps that：Water is first put into appearance
Add and stirred in the water in container in device, after calgon is dissolved with 60 DEG C of hot water, add sodium tetraborate, it is sub-
BTA dissolving is added container with methanol or ethanol, adds glycerine by sodium nitrate, sodium hydroxide, sodium metasilicate, with
After upper composition stirs, ﹣ 50# light diesel fuels or SN5W-30 machine oil are added, stirs while adding, after adding completely, uses dispersion machine
It is filling in filtering after 400 turns/min is scattered 30 minutes.
The positive effect of the present invention is as follows：
The manufacturer of domestic anti-icing fluid is typically using chemical industry such as borate, nitrate, molybdate, phosphate, silicate
Raw material does not do vaporization prevention processing typically as the preservative of engine coolant, antirust agent, antisludging agent, corrosion inhibitor etc..Because state
There is no vaporization prevention catalogue among family's standard, although the anti-icing fluid of above material production can reach GB standard, do not possess anti-steaming
Send out function.The present invention solves user in the worry evaporated using the engine coolant encountered in coolant.
The present invention is by lot of experiments, and comprehensive considering various effects successively test many kinds of substance, have carried out thousands of
Secondary experiment, finally determines the anti-freeze cooling liquid formula containing -50# light diesel fuels or SN5W-30 machine oil, and should match somebody with somebody can effectively reduce anti-
Freeze the evaporation capacity of coolant, and remaining index also complies with the regulation of concerned countries standard, is not interfered with while vaporization prevention
Other performance parameters of anti-freeze cooling liquid, will not cause to damage to engine.
Embodiment
Following examples are that the present invention is further illustrated, rather than limit its scope.
Embodiment 1
A kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：50.7%, water：40%, sodium tetraborate：
2%, natrium nitrosum：2%, sodium hydroxide：0.22%, BTA：0.09%, calgon：0.1%, sodium metasilicate：0.5%, ﹣
50# light diesel fuels：4.31%, methanol 0.08%.
The preparation method of vaporization prevention type anti-freeze cooling liquid described in the present embodiment, is comprised the following steps that：Water is first put into appearance
In device, it is added to the water after calgon is dissolved with 60 DEG C of hot water and stirs, adds sodium tetraborate, natrium nitrosum,
BTA dissolving is added container with methanol, adds glycerine, above composition is stirred equal by sodium hydroxide, sodium metasilicate
After even, addition ﹣ 50# light diesel fuels are slowly added into, are stirred while adding, after adding completely, with dispersion machine in 400 turns/min scattered 30
It is filling in filtering after minute.
4.31% -50# light diesel fuels have been used in the present embodiment, its boiling point more than 180-370 degree, freezing point -44 degree with
Under, the boiling point of water is 100 degree, takes the present embodiment anti-icing fluid 222.6g（The wherein 9.6g containing -50# light diesel fuels）3 are dried in 100 DEG C of baking boxs
Hour, its experimental result is as shown in " sample " column in table 1, while with the anti-freeze cooling liquid for being not added with -50# light diesel fuels（Remaining component
It is identical with the present embodiment）As a comparison, experimental result is as shown in " reference substance " column in table 1：
Table 1 adds the vaporization prevention experimental result of the anti-freeze cooling liquid of -50# light diesel fuels
。
The assay of other performance indications of the present embodiment anti-freeze cooling liquid is shown in Table 2.
The survey report of table 2
。
Embodiment 2
A kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：53%, water：40%, sodium tetraborate：1%,
Natrium nitrosum：1.2%, sodium hydroxide：0.13%, BTA：0.07%, calgon：0. 2%, sodium metasilicate：0.3%,
SN5W-30 machine oil：4%, methanol 0.1%.
The preparation method of vaporization prevention type anti-freeze cooling liquid described in the present embodiment, is comprised the following steps that：Water is first put into appearance
In device, it is added to the water after calgon is dissolved with 60 DEG C of hot water and stirs, adds sodium tetraborate, natrium nitrosum,
BTA dissolving is added container with methanol, adds glycerine, above composition is stirred equal by sodium hydroxide, sodium metasilicate
After even, addition SN5W-30 machine oil is slowly added into, is stirred while adding, it is scattered in 400 turns/min with dispersion machine after adding completely
It is filling in filtering after 30 minutes.
4 SN5W-30 machine oil has been used in the present embodiment, its boiling point more than 240-400 degree, add after the machine oil
Dried 3 hours in 100 DEG C of baking boxs, its experimental result is as shown in " sample " column in table 3, while with being not added with the antifreeze of SN5W-30 machine oil
As a comparison, experimental result is as shown in " reference substance " column in table 3 for coolant：
Table 3 adds the vaporization prevention experimental result of the anti-freeze cooling liquid of SN5W-30 machine oil
The assay of other performance indications of the present embodiment anti-freeze cooling liquid is suitable with embodiment 1.
Embodiment 3
A kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：56%, water：35.3%, sodium tetraborate：
1.5%, natrium nitrosum：2%, sodium hydroxide：0.2%, BTA：0.08%, calgon：0.12%, sodium metasilicate：0.2%,
SN5W-30 machine oil：4.51%, ethanol 0.09%.
The preparation method of vaporization prevention type anti-freeze cooling liquid described in the present embodiment, is comprised the following steps that：Water is first put into appearance
In device, it is added to the water after calgon is dissolved with 60 DEG C of hot water and stirs, adds sodium tetraborate, natrium nitrosum,
BTA dissolving is added container with ethanol, adds glycerine, above composition is stirred equal by sodium hydroxide, sodium metasilicate
After even, addition SN5W-30 machine oil is slowly added into, is stirred while adding, it is scattered in 400 turns/min with dispersion machine after adding completely
It is filling in filtering after 30 minutes.
The present embodiment evaporation capacity and other performance indications are suitable with embodiment 2.
Embodiment 4
A kind of vaporization prevention type anti-freeze cooling liquid, it includes following component：Glycerine：60%, water：31%, sodium tetraborate：2%,
Natrium nitrosum：1%, sodium hydroxide：0.3%, BTA：0.09%, calgon：0.1%, sodium metasilicate：0.5%, ﹣ 50# are light
Diesel oil：4.93%, ethanol 0.08%.
The preparation method of vaporization prevention type anti-freeze cooling liquid described in the present embodiment, is comprised the following steps that：Water is first put into appearance
In device, it is added to the water after calgon is dissolved with 60 DEG C of hot water and stirs, adds sodium tetraborate, natrium nitrosum,
BTA dissolving is added container with ethanol, adds glycerine, above composition is stirred equal by sodium hydroxide, sodium metasilicate
After even, addition ﹣ 50# light diesel fuels are slowly added into, are stirred while adding, after adding completely, with dispersion machine in 400 turns/min scattered 30
It is filling in filtering after minute.
The present embodiment evaporation capacity and other performance indications are suitable with embodiment 1.
Claims (2)
1. a kind of vaporization prevention type anti-freeze cooling liquid, it is characterised in that it includes following component：Glycerine：50-60%, water：30-
40%, sodium tetraborate：1-2%, natrium nitrosum：1-2%, sodium hydroxide：0.1-0.3%, BTA：0.07-0.1%, six inclined phosphorus
Sour sodium：0.1-0.2%, sodium metasilicate：0.2-0.5%, ﹣ 50# light diesel fuels or SN5W-30 machine oil：4-5%, methanol or ethanol 0.08-1%；
Above percentage is mass percent.
2. the preparation method of the vaporization prevention type anti-freeze cooling liquid described in claim 1, it is characterised in that comprise the following steps that：First will
Water is put into container, is added to the water after calgon is dissolved with 60 DEG C of hot water and is stirred, and adds sodium tetraborate, sub-
BTA dissolving is added container with methanol or ethanol, adds glycerine by sodium nitrate, sodium hydroxide, sodium metasilicate, with
After upper composition stirs, ﹣ 50# light diesel fuels or SN5W-30 machine oil are added, stirs while adding, after adding completely, uses dispersion machine
It is filling in filtering after 400 turns/min is scattered 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410573720.7A CN104371668B (en) | 2014-10-24 | 2014-10-24 | A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410573720.7A CN104371668B (en) | 2014-10-24 | 2014-10-24 | A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104371668A CN104371668A (en) | 2015-02-25 |
| CN104371668B true CN104371668B (en) | 2017-08-25 |
Family
ID=52550872
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410573720.7A Active CN104371668B (en) | 2014-10-24 | 2014-10-24 | A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104371668B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110746942A (en) * | 2019-11-18 | 2020-02-04 | 蒋华鹏 | High-boiling-point automobile cooling liquid |
| CN112175589A (en) * | 2020-11-24 | 2021-01-05 | 湘潭市润金新材料有限公司 | Cooling liquid for preventing high-temperature denaturation |
| CN113980658A (en) * | 2021-11-24 | 2022-01-28 | 青岛莱伊迪光电科技有限公司 | LEDUV cooling liquid and LEDUV equipment |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4687590A (en) * | 1985-11-01 | 1987-08-18 | First Brands Corporation | Oil-in-alcohol microemulsion containing oil-soluble corrosion inhibitor in antifreeze |
| CA2546332A1 (en) * | 2003-11-13 | 2005-05-26 | Vladisav Milovanovic | The nontoxic watery solution against freezing and corrosion and the regenerator for the utilized antifreeze |
| CN101210171A (en) * | 2006-12-27 | 2008-07-02 | 天津大学 | Low-freezing point corrosion-resisting cooling liquid for engine |
| CN101481603A (en) * | 2008-01-08 | 2009-07-15 | 姚明忠 | Pro type anti-scale flame-retardant non-corrosion long-acting anti-boiling anti-freezing fluid and preparing technology thereof |
| CN102260485A (en) * | 2010-05-25 | 2011-11-30 | M·阿伦博里 | Heat exchange medium |
-
2014
- 2014-10-24 CN CN201410573720.7A patent/CN104371668B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4687590A (en) * | 1985-11-01 | 1987-08-18 | First Brands Corporation | Oil-in-alcohol microemulsion containing oil-soluble corrosion inhibitor in antifreeze |
| CA2546332A1 (en) * | 2003-11-13 | 2005-05-26 | Vladisav Milovanovic | The nontoxic watery solution against freezing and corrosion and the regenerator for the utilized antifreeze |
| CN101210171A (en) * | 2006-12-27 | 2008-07-02 | 天津大学 | Low-freezing point corrosion-resisting cooling liquid for engine |
| CN101481603A (en) * | 2008-01-08 | 2009-07-15 | 姚明忠 | Pro type anti-scale flame-retardant non-corrosion long-acting anti-boiling anti-freezing fluid and preparing technology thereof |
| CN102260485A (en) * | 2010-05-25 | 2011-11-30 | M·阿伦博里 | Heat exchange medium |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104371668A (en) | 2015-02-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101302424B (en) | Anti-freezing fluid | |
| CN104371668B (en) | A kind of vaporization prevention type anti-freeze cooling liquid and preparation method thereof | |
| CN102250591A (en) | Water-free coolant for engine | |
| CN103497740B (en) | Antifreeze fluid by taking composite corrosion inhibitor as main raw material | |
| CN104845595B (en) | A kind of automobile engine water-free cooling composition | |
| CN105482857A (en) | Methanol gasoline with stable performance | |
| CN103484219A (en) | Long-acting antirust oil and preparation method thereof | |
| CN104250545B (en) | A kind of glyceryl anti-icing fluid | |
| CN104673200A (en) | Novel long-acting coolant | |
| CN102888259A (en) | Efficient compound additive of methanol gasoline and preparation method thereof | |
| CN107987803B (en) | Phosphorus-containing engine coolant and preparation method thereof | |
| CN107892957B (en) | Alcohol-based liquid fuel and preparation method thereof | |
| CN104021939A (en) | Sparking voltage boosting agent, preparation method thereof and electrolyte of high-voltage electrolytic capacitor | |
| CN104178233A (en) | M60-M85 methanol gasoline additive for high cleaning vehicles and methanol gasoline thereof | |
| CN102634323A (en) | Heating anti-freezing agent | |
| CN104312547B (en) | A kind of anti-cavitation pitting anti-freeze cooling liquid and preparation method thereof | |
| CN105018047A (en) | Automobile cooling fluid and preparation method thereof | |
| CN104194901A (en) | Line cutting emulsified oil | |
| CN104673207A (en) | Anti-freezing solution with high stability | |
| CN103666566A (en) | Preparation method of petroleum corrosion inhibitor | |
| CN106833549A (en) | A kind of machining coolant | |
| CN104673197A (en) | Special antifreezing fluid for automobiles | |
| CN104327887A (en) | Novel environment-friendly oil | |
| CN104371669A (en) | Antifreezing fluid for vehicles | |
| CN103695037A (en) | Petroleum corrosion inhibitor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 050800 East Village, Zhengding County, Hebei, Shijiazhuang Patentee after: Hebei platinum run industry and Trade Technology Co., Ltd Address before: 050800 East Village, Zhengding County, Hebei, Shijiazhuang Patentee before: HEBEI BO RUN CHEMICAL TECHNOLOGY Co.,Ltd. |