CN104371362B - 一种分散染料组合物、分散染料及其的制备方法和用途 - Google Patents
一种分散染料组合物、分散染料及其的制备方法和用途 Download PDFInfo
- Publication number
- CN104371362B CN104371362B CN201310752449.9A CN201310752449A CN104371362B CN 104371362 B CN104371362 B CN 104371362B CN 201310752449 A CN201310752449 A CN 201310752449A CN 104371362 B CN104371362 B CN 104371362B
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- component
- weight
- percentage
- formula
- disperse
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000986 disperse dye Substances 0.000 title claims abstract description 84
- 239000000203 mixture Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title abstract description 4
- 238000004043 dyeing Methods 0.000 claims abstract description 28
- 239000004744 fabric Substances 0.000 claims abstract description 23
- 239000000975 dye Substances 0.000 claims description 113
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- 238000000034 method Methods 0.000 claims description 26
- 150000001875 compounds Chemical class 0.000 claims description 17
- 239000002270 dispersing agent Substances 0.000 claims description 13
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 8
- -1 Hydrogen Chemical class 0.000 claims description 8
- 239000002671 adjuvant Substances 0.000 claims description 8
- 239000000460 chlorine Substances 0.000 claims description 8
- 229910052801 chlorine Inorganic materials 0.000 claims description 8
- 239000001257 hydrogen Substances 0.000 claims description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims description 8
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- 239000004576 sand Substances 0.000 claims description 7
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 6
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 6
- 229910052794 bromium Inorganic materials 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 4
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims description 4
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 229920001732 Lignosulfonate Polymers 0.000 claims description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- 230000000844 anti-bacterial effect Effects 0.000 claims description 2
- 125000001231 benzoyloxy group Chemical group C(C1=CC=CC=C1)(=O)O* 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 238000003801 milling Methods 0.000 claims 1
- 229920000728 polyester Polymers 0.000 abstract description 21
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 36
- 239000000047 product Substances 0.000 description 36
- 230000000052 comparative effect Effects 0.000 description 32
- 239000000725 suspension Substances 0.000 description 24
- 239000000835 fiber Substances 0.000 description 12
- 238000011056 performance test Methods 0.000 description 12
- 238000005070 sampling Methods 0.000 description 12
- 238000010998 test method Methods 0.000 description 12
- 238000003756 stirring Methods 0.000 description 7
- 239000012467 final product Substances 0.000 description 6
- 229920005610 lignin Polymers 0.000 description 5
- 238000005406 washing Methods 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- NAWXUBYGYWOOIX-SFHVURJKSA-N (2s)-2-[[4-[2-(2,4-diaminoquinazolin-6-yl)ethyl]benzoyl]amino]-4-methylidenepentanedioic acid Chemical compound C1=CC2=NC(N)=NC(N)=C2C=C1CCC1=CC=C(C(=O)N[C@@H](CC(=C)C(O)=O)C(O)=O)C=C1 NAWXUBYGYWOOIX-SFHVURJKSA-N 0.000 description 1
- YLZOPXRUQYQQID-UHFFFAOYSA-N 3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]propan-1-one Chemical compound N1N=NC=2CN(CCC=21)CCC(=O)N1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F YLZOPXRUQYQQID-UHFFFAOYSA-N 0.000 description 1
- MVKMKUHSGHKEDT-UHFFFAOYSA-N 3-[n-butyl-4-[(4-nitrophenyl)diazenyl]anilino]propanenitrile Chemical compound C1=CC(N(CCC#N)CCCC)=CC=C1N=NC1=CC=C([N+]([O-])=O)C=C1 MVKMKUHSGHKEDT-UHFFFAOYSA-N 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/19—Nitro dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
Description
名称 | 强度 |
实施例1 | 102% |
对比例1 | 100% |
名称 | 日晒牢度(40h) |
实施例2 | 3 |
对比例2 | 2 |
名称 | 强度 | 日晒牢度 | 配伍性 |
实施例3 | 105% | 2~3 | Ⅱ |
对比例3 | 100% | 2 | III |
名称 | 强度 | pH值稳定范围 |
实施例4 | 107% | 3~9 |
对比例4 | 100% | 3~7 |
名称 | 强度 | pH值稳定范围 |
实施例5 | 107% | 3~9 |
对比例5 | 100% | 3~7 |
名称 | 强度 |
实施例6 | 102% |
对比例6 | 100% |
名称 | 水洗牢度 |
实施例7 | 4~5 |
对比例7 | 4 |
名称 | 强度 | 日晒牢度(40h) |
实施例8 | 103.5% | 2~3 |
对比例8 | 100% | 2 |
实施例 | 日晒牢度 |
9 | 3 |
实施例 | 日晒牢度 | 配伍性 |
10 | 3 | Ⅱ |
11 | 2~3 | Ⅱ |
12 | 3 | Ⅱ |
13 | 2~3 | Ⅱ |
14 | 3 | Ⅱ |
15 | 2~3 | Ⅱ |
16 | 2~3 | Ⅱ |
17 | 3 | Ⅱ |
实施例 | 日晒牢度 |
18 | 3 |
19 | 3 |
实施例 | 日晒牢度 | 配伍性 |
20 | 2~3 | Ⅱ |
21 | 2~3 | Ⅱ |
22 | 2~3 | Ⅰ |
23 | 3 | Ⅱ |
24 | 3 | Ⅱ |
25 | 3 | Ⅰ |
26 | 2~3 | Ⅰ |
27 | 3 | Ⅰ |
28 | 2~3 | Ⅱ |
29 | 2~3 | Ⅱ |
30 | 2~3 | Ⅱ |
31 | 2~3 | Ⅱ |
32 | 3 | Ⅱ |
33 | 2~3 | Ⅱ |
34 | 3 | Ⅱ |
35 | 3 | Ⅱ |
Claims (21)
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710188860.6A CN106947288B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
CN201310752449.9A CN104371362B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
EP14876649.6A EP3147333B1 (en) | 2013-12-30 | 2014-12-30 | Disperse dye composition, disperse dye and preparation method and use thereof |
KR1020167020366A KR101702513B1 (ko) | 2013-12-30 | 2014-12-30 | 분산 염료 조성물, 분산 염료 및 그의 제조 방법 및 용도 |
PCT/CN2014/095585 WO2015101290A1 (zh) | 2013-12-30 | 2014-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
ES14876649.6T ES2653737T3 (es) | 2013-12-30 | 2014-12-30 | Composición de tinte disperso, tinte disperso y método de preparación y uso de los mismos |
US15/102,669 US10151062B2 (en) | 2013-12-30 | 2014-12-30 | Disperse dye composition, disperse dye and preparation method and use thereof |
BR112016012058A BR112016012058B8 (pt) | 2013-12-30 | 2014-12-30 | Composição de corante disperso e corante disperso |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310752449.9A CN104371362B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
Related Child Applications (1)
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CN201710188860.6A Division CN106947288B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
Publications (2)
Publication Number | Publication Date |
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CN104371362A CN104371362A (zh) | 2015-02-25 |
CN104371362B true CN104371362B (zh) | 2017-04-12 |
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CN201310752449.9A Active CN104371362B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
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CN201710188860.6A Active CN106947288B (zh) | 2013-12-30 | 2013-12-30 | 一种分散染料组合物、分散染料及其的制备方法和用途 |
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Country | Link |
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CN (2) | CN106947288B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112608622B (zh) * | 2020-12-07 | 2023-05-23 | 浙江龙盛集团股份有限公司 | 一种蓝至黑色分散染料组合物和染料制品 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3793305A (en) * | 1970-09-14 | 1974-02-19 | Du Pont | One-step process of preparing azo dyes by simultaneous diazotization |
CN1696204A (zh) * | 2005-06-07 | 2005-11-16 | 浙江闰土股份有限公司 | 复合环保型分散灰染料 |
CN101280122A (zh) * | 2008-05-16 | 2008-10-08 | 浙江闰土股份有限公司 | 一种黑、蓝系列的环保分散染料组合物 |
CN101760045A (zh) * | 2009-12-30 | 2010-06-30 | 浙江闰土股份有限公司 | 一种中低温环保型分散染料组合物 |
CN101768376A (zh) * | 2009-12-30 | 2010-07-07 | 浙江闰土股份有限公司 | 一种环保型的分散染料组合物 |
-
2013
- 2013-12-30 CN CN201710188860.6A patent/CN106947288B/zh active Active
- 2013-12-30 CN CN201310752449.9A patent/CN104371362B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3793305A (en) * | 1970-09-14 | 1974-02-19 | Du Pont | One-step process of preparing azo dyes by simultaneous diazotization |
CN1696204A (zh) * | 2005-06-07 | 2005-11-16 | 浙江闰土股份有限公司 | 复合环保型分散灰染料 |
CN101280122A (zh) * | 2008-05-16 | 2008-10-08 | 浙江闰土股份有限公司 | 一种黑、蓝系列的环保分散染料组合物 |
CN101760045A (zh) * | 2009-12-30 | 2010-06-30 | 浙江闰土股份有限公司 | 一种中低温环保型分散染料组合物 |
CN101768376A (zh) * | 2009-12-30 | 2010-07-07 | 浙江闰土股份有限公司 | 一种环保型的分散染料组合物 |
Also Published As
Publication number | Publication date |
---|---|
CN106947288B (zh) | 2019-11-22 |
CN104371362A (zh) | 2015-02-25 |
CN106947288A (zh) | 2017-07-14 |
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Inventor after: Ruan Jingbo Inventor after: Zhao Guosheng Inventor after: Gu Weidi Inventor after: Ruan Haixing Inventor after: Ye Huaming Inventor after: Jing Xueping Inventor before: Chen Bailong |
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Effective date of registration: 20171108 Address after: Shangyu District of Zhejiang city in Shaoxing Province town road 312368 called mountain Patentee after: Zhejiang Runtu Co., Ltd. Address before: 312368 No. 231 village, Zhenjiang village, Shaoxing, Zhejiang Patentee before: Chen Bailong |
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