CN104213403B - A kind of fabric insect protected antibacterial finishing agent and preparation method thereof - Google Patents
A kind of fabric insect protected antibacterial finishing agent and preparation method thereof Download PDFInfo
- Publication number
- CN104213403B CN104213403B CN201410427989.4A CN201410427989A CN104213403B CN 104213403 B CN104213403 B CN 104213403B CN 201410427989 A CN201410427989 A CN 201410427989A CN 104213403 B CN104213403 B CN 104213403B
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- Prior art keywords
- finishing agent
- insect protected
- antibacterial finishing
- fabric insect
- protected antibacterial
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- 239000004744 fabric Substances 0.000 title claims abstract description 36
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 33
- 241000238631 Hexapoda Species 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 30
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims abstract description 30
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 16
- RLLPVAHGXHCWKJ-UHFFFAOYSA-N permethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229960000490 permethrin Drugs 0.000 claims abstract description 16
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 16
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 16
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims abstract description 14
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 14
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 14
- -1 1.0 parts Chemical compound 0.000 claims description 4
- 241000588724 Escherichia coli Species 0.000 abstract description 2
- 230000001408 fungistatic effect Effects 0.000 abstract description 2
- 230000002401 inhibitory effect Effects 0.000 abstract description 2
- 244000045947 parasite Species 0.000 abstract description 2
- 238000005406 washing Methods 0.000 abstract description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 229960000846 camphor Drugs 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a kind of fabric insect protected antibacterial finishing agent, described fabric insect protected antibacterial finishing agent is made up of each material of following mass fraction: polyvinylpyrrolidone 5-8 part, ethyl-para-hydroxybenzoate 5-6 part, methyl acrylate 0.5-0.8 part, Permethrin 0.5-0.8 part, copper sulphate 0.8-1.2 part, sodium acid carbonate 0.2-0.3 part, ethanol 20-25 part, water 60-65 part. The present invention also provides the preparation method of this finishing agent. Fabric insect protected antibacterial finishing agent of the present invention has good deinsectization and antibacterial effect, effectively expelling parasite, the integrality of protection clothing; Can anti-bacteria and the growth of mould, especially high to the inhibiting rate of Escherichia coli and mould, repeatedly after washing, still there is good fungistatic effect.
Description
Technical field
The invention belongs to textile auxiliary technical field, be specifically related to a kind of fabric insect protected antibacterial finishing agent and preparation method thereof.
Background technology
General fabrics all can be carried out insect-prevention treatment in when storage, has the material of anthelmintic action, to prevent that clothes from being damaged by worms as placed camphor etc. in wardrobe. Some fabric can carry out insect-prevention treatment making before finished product, and these fabrics just do not need to carry out insect-prevention treatment in the time depositing again. Existing pest-control finishing agent vermins-proof effect is undesirable, and function singleness.
Summary of the invention
In order to solve problems of the prior art, the invention provides a kind of fabric insect protected antibacterial finishing agent, apply its well deinsectization and killing human body and the harmful microorganism of clothing. For this reason, the present invention also provides the preparation method of this fabric insect protected antibacterial finishing agent.
The invention provides a kind of fabric insect protected antibacterial finishing agent, described fabric insect protected antibacterial finishing agent is made up of each material of following mass fraction: polyvinylpyrrolidone 5-8 part, ethyl-para-hydroxybenzoate 5-6 part, methyl acrylate 0.5-0.8 part, Permethrin 0.5-0.8 part, copper sulphate 0.8-1.2 part, sodium acid carbonate 0.2-0.3 part, ethanol 20-25 part, water 60-65 part.
Preferably, described fabric insect protected antibacterial finishing agent is made up of each material of following mass fraction: 6 parts of polyvinylpyrrolidones, 5.5 parts of ethyl-para-hydroxybenzoates, 0.6 part of methyl acrylate, 0.6 part of Permethrin, 1.0 parts, copper sulphate, 0.2 part of sodium acid carbonate, 22 parts of ethanol, 62 parts, water.
The present invention also provides the preparation method of above-mentioned fabrics insect protected antibacterial finishing agent, and step is as follows:
(1) polyvinylpyrrolidone of formula ratio, ethyl-para-hydroxybenzoate, methyl acrylate, Permethrin and ethanol are mixed, be heated to 40-45 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
Fabric insect protected antibacterial finishing agent of the present invention has good deinsectization and antibacterial effect, effectively expelling parasite, the integrality of protection clothing; Can anti-bacteria and the growth of mould, especially high to the inhibiting rate of Escherichia coli and mould, repeatedly after washing, still there is good fungistatic effect.
Detailed description of the invention
Following embodiment is convenient to understand better the present invention, but does not limit the present invention. Experimental technique in following embodiment, if no special instructions, is conventional method.
Embodiment 1
The formula of fabric insect protected antibacterial finishing agent of the present invention is as follows:
Polyvinylpyrrolidone 6kg, ethyl-para-hydroxybenzoate 5.5kg, methyl acrylate 0.6kg, Permethrin 0.6kg, copper sulphate 1.0kg, sodium acid carbonate 0.2kg, ethanol 22kg, water 62kg.
The preparation method of fabric insect protected antibacterial finishing agent of the present invention is:
(1) polyvinylpyrrolidone 6kg, ethyl-para-hydroxybenzoate 5.5kg, methyl acrylate 0.6kg, Permethrin 0.6kg and 22kg ethanol are mixed, be heated to 42 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
Embodiment 2
The formula of fabric insect protected antibacterial finishing agent of the present invention is as follows:
Polyvinylpyrrolidone 5kg, ethyl-para-hydroxybenzoate 5kg, methyl acrylate 0.8kg, Permethrin 0.8kg, copper sulphate 1.2kg, sodium acid carbonate 0.3kg, ethanol 25kg, water 60kg.
The preparation method of fabric insect protected antibacterial finishing agent of the present invention is:
(1) polyvinylpyrrolidone 5kg, ethyl-para-hydroxybenzoate 5kg, methyl acrylate 0.8kg, Permethrin 0.8kg and 25kg ethanol are mixed, be heated to 40 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
Embodiment 3
The formula of fabric insect protected antibacterial finishing agent of the present invention is as follows:
Polyvinylpyrrolidone 8kg, ethyl-para-hydroxybenzoate 6kg, methyl acrylate 0.5kg, Permethrin 0.5kg, copper sulphate 0.8kg, sodium acid carbonate 0.2kg, ethanol 20kg, water 65kg.
The preparation method of fabric insect protected antibacterial finishing agent of the present invention is:
(1) polyvinylpyrrolidone 8kg, ethyl-para-hydroxybenzoate 6kg, methyl acrylate 0.5kg, Permethrin 0.5kg and 20kg ethanol are mixed, be heated to 40 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
Embodiment 4
The formula of fabric insect protected antibacterial finishing agent of the present invention is as follows:
Polyvinylpyrrolidone 7kg, ethyl-para-hydroxybenzoate 6kg, methyl acrylate 0.7kg, Permethrin 0.5kg, copper sulphate 0.8kg, sodium acid carbonate 0.2kg, ethanol 23kg, water 63kg.
The preparation method of fabric insect protected antibacterial finishing agent of the present invention is:
(1) polyvinylpyrrolidone 7kg, ethyl-para-hydroxybenzoate 6kg, methyl acrylate 0.7kg, Permethrin 0.5kg, copper sulphate 0.8kg and 23kg ethanol are mixed, be heated to 43 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
The using method of fabric insect protected antibacterial finishing agent of the present invention is:
(1) preparation fabric insect protected antibiotic finishing solution: fabric insect protected antibacterial finishing agent prepared by embodiment 1-4 is dissolved in the water, and concentration is 25-30g/L;
(2) fabric is padded to pick-up 75-80% by fabric insect protected antibiotic finishing solution;
(3) dehydration, at 75-85 DEG C by fabric drying.
Finally it should be noted that: the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although the present invention is had been described in detail with reference to previous embodiment, for a person skilled in the art, its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement. Within the spirit and principles in the present invention all, any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (3)
1. a fabric insect protected antibacterial finishing agent, is characterized in that: described fabric insect protected antibacterial finishing agent is made up of each material of following mass fraction: polyvinylpyrrolidone 5-8 part, ethyl-para-hydroxybenzoate 5-6 part, methyl acrylate 0.5-0.8 part, Permethrin 0.5-0.8 part, copper sulphate 0.8-1.2 part, sodium acid carbonate 0.2-0.3 part, ethanol 20-25 part, water 60-65 part;
The preparation method of described fabric insect protected antibacterial finishing agent is: the polyvinylpyrrolidone of formula ratio, ethyl-para-hydroxybenzoate, methyl acrylate, Permethrin and ethanol are mixed, be heated to 40-45 DEG C, stir; Add all the other components, after stirring, be cooled to room temperature.
2. fabric insect protected antibacterial finishing agent according to claim 1, is characterized in that: described fabric insect protected antibacterial finishing agent is made up of each material of following mass fraction: 6 parts of polyvinylpyrrolidones, 5.5 parts of ethyl-para-hydroxybenzoates, 0.6 part of methyl acrylate, 0.6 part of Permethrin, 1.0 parts, copper sulphate, 0.2 part of sodium acid carbonate, 22 parts of ethanol, 62 parts, water.
3. the preparation method of the fabric insect protected antibacterial finishing agent described in claim 1 or 2, is characterized in that: step is as follows:
(1) polyvinylpyrrolidone of formula ratio, ethyl-para-hydroxybenzoate, methyl acrylate, Permethrin and ethanol are mixed, be heated to 40-45 DEG C, stir;
(2) add all the other components, after stirring, be cooled to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410427989.4A CN104213403B (en) | 2014-08-28 | 2014-08-28 | A kind of fabric insect protected antibacterial finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410427989.4A CN104213403B (en) | 2014-08-28 | 2014-08-28 | A kind of fabric insect protected antibacterial finishing agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104213403A CN104213403A (en) | 2014-12-17 |
| CN104213403B true CN104213403B (en) | 2016-05-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410427989.4A Active CN104213403B (en) | 2014-08-28 | 2014-08-28 | A kind of fabric insect protected antibacterial finishing agent and preparation method thereof |
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| CN (1) | CN104213403B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105755798A (en) * | 2016-04-29 | 2016-07-13 | 江苏苏扬服帽有限公司 | Multifunctional finishing agent for knitting and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| EP2434048A1 (en) * | 2010-09-28 | 2012-03-28 | Rohm and Haas Company | Antimicrobial fabric finish |
| CN102851952A (en) * | 2012-09-19 | 2013-01-02 | 吴江市意胜纺织有限公司 | Fabric antibacterial agent |
| CN103696249A (en) * | 2013-11-28 | 2014-04-02 | 南通市通州区大达麻纺织有限公司 | Insect-proofing and antibacterial finishing agent for fabric |
| CN103726341A (en) * | 2013-12-09 | 2014-04-16 | 常熟市爱博尔服饰有限公司 | Down feather mothproof nursing agent |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH07310284A (en) * | 1994-05-12 | 1995-11-28 | Toray Ind Inc | Antimicrobial fibrous structure |
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2014
- 2014-08-28 CN CN201410427989.4A patent/CN104213403B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| EP2434048A1 (en) * | 2010-09-28 | 2012-03-28 | Rohm and Haas Company | Antimicrobial fabric finish |
| CN102851952A (en) * | 2012-09-19 | 2013-01-02 | 吴江市意胜纺织有限公司 | Fabric antibacterial agent |
| CN103696249A (en) * | 2013-11-28 | 2014-04-02 | 南通市通州区大达麻纺织有限公司 | Insect-proofing and antibacterial finishing agent for fabric |
| CN103726341A (en) * | 2013-12-09 | 2014-04-16 | 常熟市爱博尔服饰有限公司 | Down feather mothproof nursing agent |
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| Publication number | Publication date |
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| CN104213403A (en) | 2014-12-17 |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
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| C14 | Grant of patent or utility model | ||
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| TR01 | Transfer of patent right |
Effective date of registration: 20191220 Address after: 314409 Xucun township government, Haining City, Jiaxing City, Zhejiang Province Patentee after: Haining Home Textile Industrial Base Investment Development Co.,Ltd. Address before: 214000 Jiangsu Province, Wuxi city Xishan District Yang Jian Zhen Li an Cun Xi Hu Lu Bei Patentee before: WUXI QISHENG KNITTING GLOVES FACTORY |
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| EE01 | Entry into force of recordation of patent licensing contract | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20141217 Assignee: Zhejiang Jinyu Textile Technology Co.,Ltd. Assignor: Haining Home Textile Industrial Base Investment Development Co.,Ltd. Contract record no.: X2022330000255 Denomination of invention: An insect proof and antibacterial finishing agent for fabric and its preparation method Granted publication date: 20160518 License type: Common License Record date: 20220629 |
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| EE01 | Entry into force of recordation of patent licensing contract | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20141217 Assignee: Haining buyancheng Textile Co.,Ltd. Assignor: Haining Home Textile Industrial Base Investment Development Co.,Ltd. Contract record no.: X2022330000908 Denomination of invention: An insect resistant and antibacterial finishing agent for fabrics and its preparation method Granted publication date: 20160518 License type: Common License Record date: 20221228 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A fabric anti insect and antibacterial finishing agent and its preparation method Effective date of registration: 20231227 Granted publication date: 20160518 Pledgee: Bank of Huzhou Co.,Ltd. Pledgor: Haining Home Textile Industrial Base Investment Development Co.,Ltd. Registration number: Y2023980073645 |