CN104072083A - Inorganic thermal insulation material containing silicon dioxide and preparation method of inorganic thermal insulation material - Google Patents
Inorganic thermal insulation material containing silicon dioxide and preparation method of inorganic thermal insulation material Download PDFInfo
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- CN104072083A CN104072083A CN201410315764.XA CN201410315764A CN104072083A CN 104072083 A CN104072083 A CN 104072083A CN 201410315764 A CN201410315764 A CN 201410315764A CN 104072083 A CN104072083 A CN 104072083A
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 103
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 51
- 239000012774 insulation material Substances 0.000 title claims abstract description 46
- 235000012239 silicon dioxide Nutrition 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 44
- 239000000463 material Substances 0.000 claims abstract description 33
- -1 polypropylene Polymers 0.000 claims abstract description 28
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 23
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 23
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 23
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004743 Polypropylene Substances 0.000 claims abstract description 21
- 229920001155 polypropylene Polymers 0.000 claims abstract description 21
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 20
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 20
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 20
- 235000012245 magnesium oxide Nutrition 0.000 claims abstract description 20
- 239000004111 Potassium silicate Substances 0.000 claims abstract description 15
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052913 potassium silicate Inorganic materials 0.000 claims abstract description 15
- 239000000835 fiber Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims abstract description 11
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000000498 ball milling Methods 0.000 claims abstract description 10
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 10
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims abstract description 10
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000002002 slurry Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 239000011805 ball Substances 0.000 claims description 25
- 229960001866 silicon dioxide Drugs 0.000 claims description 24
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 10
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 8
- 238000005086 pumping Methods 0.000 claims description 8
- 230000000694 effects Effects 0.000 abstract description 4
- 239000010451 perlite Substances 0.000 abstract description 3
- 235000019362 perlite Nutrition 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 238000009413 insulation Methods 0.000 abstract description 2
- 230000009967 tasteless effect Effects 0.000 abstract description 2
- 239000004115 Sodium Silicate Substances 0.000 abstract 2
- 239000010440 gypsum Substances 0.000 abstract 2
- 229910052602 gypsum Inorganic materials 0.000 abstract 2
- 239000000843 powder Substances 0.000 abstract 2
- 229910052911 sodium silicate Inorganic materials 0.000 abstract 2
- 239000004575 stone Substances 0.000 abstract 2
- SHFGJEQAOUMGJM-UHFFFAOYSA-N dialuminum dipotassium disodium dioxosilane iron(3+) oxocalcium oxomagnesium oxygen(2-) Chemical compound [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[Na+].[Na+].[Al+3].[Al+3].[K+].[K+].[Fe+3].[Fe+3].O=[Mg].O=[Ca].O=[Si]=O SHFGJEQAOUMGJM-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 231100000252 nontoxic Toxicity 0.000 abstract 1
- 230000003000 nontoxic effect Effects 0.000 abstract 1
- 235000019794 sodium silicate Nutrition 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 11
- 230000006835 compression Effects 0.000 description 4
- 238000007906 compression Methods 0.000 description 4
- 239000002994 raw material Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 229910002012 Aerosil® Inorganic materials 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000002528 anti-freeze Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- DDXLVDQZPFLQMZ-UHFFFAOYSA-M dodecyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)C DDXLVDQZPFLQMZ-UHFFFAOYSA-M 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Silicon Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
The invention discloses an inorganic thermal insulation material containing silicon dioxide and a preparation method of the inorganic thermal insulation material. The inorganic thermal insulation material comprises silicon dioxide, expanded perlite, magnesium oxide, sodium silicate, potassium silicate, stone waste, gypsum powder, polypropylene fiber, sodium carboxymethyl cellulose and calcium hydroxide. The preparation method comprises the following steps: preparing 1% sodium carboxymethyl cellulose aqueous liquor from sodium carboxymethyl cellulose, adding sodium silicate, potassium silicate, magnesium oxide and calcium hydroxide, and sufficiently stirring to obtain a gel material; placing the silicon dioxide, the expanded perlite, the stone waste, the gypsum powder and the polypropylene fiber in a mixer in proportion and stirring and mixing, then, placing in a ball mill for wet-process ball-milling and re-crushing, standing obtained slurry to remove upper-layer water and then sufficiently mixing uniformly with the gel material, and placing in a dryer for drying to obtain the inorganic thermal insulation material. The inorganic thermal insulation material disclosed by the invention is reasonable in formula, materials are easy to obtain, cost is lower, and the preparation method is simple; the prepared thermal insulation material is non-toxic and tasteless, green and environment-friendly, and good in thermal insulation effect.
Description
Technical field
The present invention relates to a kind of silica containing inorganic heat insulation material and preparation method thereof, belong to inorganic heat insulation material field.
Background technology
Inorganic heat insulation material has energy-conserving profit waste, heat insulating, antifreeze, the ageing-resistant feature such as excellent properties and cheap price of fire prevention, has the market requirement widely.Inorganic heat insulation material unit weight is slightly large, heat preservation hot less efficient, but fire protection flame retarding, deformation coefficient is little, anti-aging, stable performance, be combined better with plinth course and float coat, safety and firmness is good, and thermal insulation layer intensity and weather resistance are higher than organic insulation material, long service life, difficulty of construction is little, engineering cost is lower, and eco-environmental prote is good, can cycling and reutilization.The following development along with low-carbon economy, the building energy conservation of China requires more and more to come high, and the application of inorganic heat insulation material also will be more and more extensive.
Application number is that 201310014752.9 " a kind of inorganic heat insulation materials and preparation method thereof " disclose a kind of inorganic heat insulation material, is infiltrated to obtaining on glass mat by aerosil, soluble silicate, tin-antiomony oxide, hollow glass micropearl and Dodecyl trimethyl ammonium chloride after coupling agent modified.This invention has good water resisting property, good heat insulating, but cost is high, is not suitable for applying on a large scale.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, inorganic heat insulation material of a kind of high insulating effect and preparation method thereof is provided.
The present invention is achieved through the following technical solutions:
A kind of silica containing inorganic heat insulation material, by weight percentage, comprise silicon-dioxide 30-50 part, pearlstone 16-30 part, magnesium oxide 6-12 part, water glass 12-18 part, potassium silicate 12-18 part, aggregate chips 3-7 part, terra alba 2-5 part, polypropylene fibre 3-6 part, Xylo-Mucine 5-10 part and calcium hydroxide 4-8 part; The granularity of described silicon-dioxide and pearlstone is 200 orders.
The silica containing inorganic heat insulation material of described one, described water glass and the weight ratio of potassium silicate are 1: 1.
The silica containing inorganic heat insulation material of described one, by weight percentage, comprise 6 parts, 42 parts of silicon-dioxide, 24 parts of pearlstones, 8 parts, magnesium oxide, 16 parts of water glass, 16 parts of potassium silicates, 5 parts of aggregate chips, 3 parts of terra albas, 4 parts of polypropylene fibres, 8 parts of Xylo-Mucines and calcium hydroxide.
The preparation method of described a kind of silica containing inorganic heat insulation material, Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, add water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material, by silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in mixing machine and are uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 70-80 DEG C of condition, dry and obtain inorganic heat insulation material.
The preparation method of described a kind of silica containing inorganic heat insulation material, when ball milling, the weight ratio of material, water and ball is 1: 2-3: 4-5.
The preparation method of described a kind of silica containing inorganic heat insulation material, drying time is 6-8h.
Expanded perlite thermal-nsulation is effective, but its maximum operation (service) temperature is 800 DEG C, and poor water resistance, so content is too much unsuitable, magnesium oxide has extremely fireproof insulating property, but easily absorb moisture and carbonic acid gas, so magnesium oxide can not be too much, otherwise water-intake rate variation, but can not be very few, otherwise flame retardant properties is not good, and silica chemistry is stable, there is strong adsorptivity, can be adsorbed on pearlstone and magnesian surrounding, prevent that pearlstone and magnesium oxide from absorbing moisture, cause material property to reduce.
Add polypropylene fibre can improve the ultimate compression strength of material, fully stick together by water glass, potassium silicate and Xylo-Mucine, ensure homogeneity and the stability of material.
Beneficial effect of the present invention is as follows:
The present invention adopts inorganics as raw material, and formula is reasonable, and raw material all easily obtains, cost is lower, preparation method is simple, and the lagging material preparing is nonpoisonous and tasteless, environmental protection, high insulating effect, its thermal conductivity is 0.01-0.08w/ (m.k), and burning grade is A level, and maximum operation (service) temperature is 1000 DEG C, ultimate compression strength is 0.8-1.0MPa, and water-intake rate is less than or equal to 0.1%.
Embodiment
Embodiment 1
In the present embodiment, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 6 parts, 42 parts of silicon-dioxide, 24 parts of pearlstones, 8 parts, magnesium oxide, 16 parts of water glass, 16 parts of potassium silicates, 5 parts of aggregate chips, 3 parts of terra albas, 4 parts of polypropylene fibres, 8 parts of Xylo-Mucines and calcium hydroxide.
Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, adds water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material; Silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in to mixing machine to be uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 80 DEG C of conditions, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 3: 5, and drying time is 8h.
Embodiment 2
In the present embodiment, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 4 parts, 30 parts of silicon-dioxide, 30 parts of pearlstones, 6 parts, magnesium oxide, 12 parts of water glass, 12 parts of potassium silicates, 3 parts of aggregate chips, 2 parts of terra albas, 6 parts of polypropylene fibres, 10 parts of Xylo-Mucines and calcium hydroxide; The granularity of described silicon-dioxide and pearlstone is 200 orders.
Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, add water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material, silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in to mixing machine to be uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 70 DEG C of conditions, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 2: 4, and drying time is 6h.
Embodiment 3
In the present embodiment, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 8 parts, 50 parts of silicon-dioxide, 16 parts of pearlstones, 12 parts, magnesium oxide, 18 parts of water glass, 18 parts of potassium silicates, 7 parts of aggregate chips, 5 parts of terra albas, 3 parts of polypropylene fibres, 5 parts of Xylo-Mucines and calcium hydroxide; The granularity of described silicon-dioxide and pearlstone is 200 orders.
The preparation method of described a kind of silica containing inorganic heat insulation material, Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, add water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material, by silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in mixing machine and are uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 70-80 DEG C of condition, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 3: 4, and drying time is 8h.
Comparative example 1
In this comparative example, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 10 parts, 60 parts of silicon-dioxide, 10 parts of pearlstones, 15 parts, magnesium oxide, 20 parts of water glass, 10 parts of potassium silicates, 10 parts of aggregate chips, 8 parts of terra albas, 10 parts of polypropylene fibres, 12 parts of Xylo-Mucines and calcium hydroxide.
The preparation method of described a kind of silica containing inorganic heat insulation material, Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, add water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material, by silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in mixing machine and are uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 80 DEG C of conditions, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 4: 6, and drying time is 8h.
Comparative example, compared with embodiment 1,2,3, is the composition difference of each raw material, although there is no the effect of embodiment 1,2,3, still good than general performance of heat protective material, ultimate compression strength is high, and water-intake rate is low.
Comparative example 2
In the present embodiment, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 4 parts, 30 parts of silicon-dioxide, 30 parts of pearlstones, 6 parts, magnesium oxide, 12 parts of water glass, 12 parts of potassium silicates, 3 parts of aggregate chips, 2 parts of terra albas, 6 parts of polypropylene fibres, 10 parts of Xylo-Mucines and calcium hydroxide; The granularity of described silicon-dioxide and pearlstone is 200 orders.
Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, adds water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material; Silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in to mixing machine to be uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 80 DEG C of conditions, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 4: 6, and drying time is 8h.
Comparative example 2 is different from embodiment 2 while being ball milling, the weight ratio of material, water and ball.
Comparative example 3
In the present embodiment, a kind of silica containing inorganic heat insulation material, by weight percentage, comprise 8 parts, 50 parts of silicon-dioxide, 16 parts of pearlstones, 12 parts, magnesium oxide, 18 parts of water glass, 18 parts of potassium silicates, 7 parts of aggregate chips, 5 parts of terra albas, 3 parts of polypropylene fibres, 5 parts of Xylo-Mucines and calcium hydroxide; The granularity of described silicon-dioxide and pearlstone is 200 orders.
By Xylo-Mucine, water glass, potassium silicate, magnesium oxide, calcium hydroxide, silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre be proportionally placed in to mixing machine be uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 80 DEG C of conditions, dry and obtain inorganic heat insulation material.Wherein, when ball milling, the weight ratio of material, water and ball is 1: 3: 5, and drying time is 8h.
Comparative example 3 is pulverized after directly mixing from different being of embodiment 3.
The performance of the lagging material that each embodiment and comparative example obtain sees the following form:
| ? | Thermal conductivity | Burning grade | Maximum operation (service) temperature | Ultimate compression strength | Water-intake rate |
| Embodiment 1 | 0.01w/(m.k) | A level | 1000℃ | 1.0MPa | 0.08％ |
| Embodiment 2 | 0.05w/(m.k) | A level | 1000℃ | 1.0MPa | 0.1％ |
| Embodiment 3 | 0.08w/(m.k) | A level | 1000℃ | 0.8MPa | 0.09％ |
| Comparative example 1 | 0.15w/(m.k) | B level | 800℃ | 0.5MPa | 0.12％ |
| Comparative example 2 | 0.15w/(m.k) | B level | 800℃ | 0.3MPa | 0.09％ |
| Comparative example 3 | 0.15w/(m.k) | B level | 800℃ | 0.8MPa | 0.15％ |
More than show and described ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and specification sheets, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (6)
1. a silica containing inorganic heat insulation material, it is characterized in that, by weight percentage, comprise silicon-dioxide 30-50 part, pearlstone 16-30 part, magnesium oxide 6-12 part, water glass 12-18 part, potassium silicate 12-18 part, aggregate chips 3-7 part, terra alba 2-5 part, polypropylene fibre 3-6 part, Xylo-Mucine 5-10 part and calcium hydroxide 4-8 part; The granularity of described silicon-dioxide and pearlstone is 200 orders.
2. the silica containing inorganic heat insulation material of one according to claim 1, is characterized in that, described water glass and the weight ratio of potassium silicate are 1: 1.
3. the silica containing inorganic heat insulation material of one according to claim 1, it is characterized in that, by weight percentage, comprise 6 parts, 42 parts of silicon-dioxide, 24 parts of pearlstones, 8 parts, magnesium oxide, 16 parts of water glass, 16 parts of potassium silicates, 5 parts of aggregate chips, 3 parts of terra albas, 4 parts of polypropylene fibres, 8 parts of Xylo-Mucines and calcium hydroxide.
4. the preparation method of a kind of silica containing inorganic heat insulation material according to claim 1, it is characterized in that, Xylo-Mucine is mixed with to 1% sodium carboxymethyl cellulose solution, add water glass, potassium silicate, magnesium oxide and calcium hydroxide, fully stir, obtain gel material, by silicon-dioxide, pearlstone, aggregate chips, terra alba and polypropylene fibre are proportionally placed in mixing machine and are uniformly mixed, then being placed in ball mill wet ball grinding pulverizes again, the slurry obtaining is left standstill after pumping upper strata moisture and fully mixed with gel material, be placed in dryer, under 70-80 DEG C of condition, dry and obtain inorganic heat insulation material.
5. the preparation method of a kind of silica containing inorganic heat insulation material according to claim 4, is characterized in that, when ball milling, the weight ratio of material, water and ball is 1: 2-3: 4-5.
6. the preparation method of a kind of silica containing inorganic heat insulation material according to claim 4, is characterized in that, drying time is 6-8h.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105731879A (en) * | 2014-12-12 | 2016-07-06 | 朱亚迪 | Inorganic thermal insulation material and preparation method thereof |
| CN106116428A (en) * | 2016-06-29 | 2016-11-16 | 合肥广能新材料科技有限公司 | Silica containing inorganic heat insulation material and preparation method thereof |
| CN106187021A (en) * | 2016-06-30 | 2016-12-07 | 合肥广能新材料科技有限公司 | Inorganic heat insulation material and preparation method thereof |
| CN106747488A (en) * | 2016-11-03 | 2017-05-31 | 联合矿产（天津）有限公司 | By stabilized fire proofing composition |
| WO2019042105A1 (en) * | 2017-09-01 | 2019-03-07 | 陆宇皇金建材（河源）有限公司 | Sound insulation material, sound insulation plate, and partition structure of locomotive carriage |
| CN112441608A (en) * | 2019-08-28 | 2021-03-05 | 西南科技大学 | Preparation method of nano calcium hydroxide whisker |
| CN113896499A (en) * | 2021-09-17 | 2022-01-07 | 西安欧盛达科技有限公司 | Method for manufacturing novel heat-insulating fireproof material |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265262A (en) * | 2013-04-19 | 2013-08-28 | 安徽相变保温材料有限公司 | Inorganic composite insulation board and preparation method thereof |
| CN103723991A (en) * | 2013-12-12 | 2014-04-16 | 青岛无为保温材料有限公司 | Novel thermal insulating and energy-saving material |
| CN103787642A (en) * | 2013-12-12 | 2014-05-14 | 青岛无为保温材料有限公司 | Efficient thermal insulation energy-saving material |
-
2014
- 2014-06-27 CN CN201410315764.XA patent/CN104072083B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265262A (en) * | 2013-04-19 | 2013-08-28 | 安徽相变保温材料有限公司 | Inorganic composite insulation board and preparation method thereof |
| CN103723991A (en) * | 2013-12-12 | 2014-04-16 | 青岛无为保温材料有限公司 | Novel thermal insulating and energy-saving material |
| CN103787642A (en) * | 2013-12-12 | 2014-05-14 | 青岛无为保温材料有限公司 | Efficient thermal insulation energy-saving material |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105731879A (en) * | 2014-12-12 | 2016-07-06 | 朱亚迪 | Inorganic thermal insulation material and preparation method thereof |
| CN106116428A (en) * | 2016-06-29 | 2016-11-16 | 合肥广能新材料科技有限公司 | Silica containing inorganic heat insulation material and preparation method thereof |
| CN106187021A (en) * | 2016-06-30 | 2016-12-07 | 合肥广能新材料科技有限公司 | Inorganic heat insulation material and preparation method thereof |
| CN106747488A (en) * | 2016-11-03 | 2017-05-31 | 联合矿产（天津）有限公司 | By stabilized fire proofing composition |
| CN106747488B (en) * | 2016-11-03 | 2019-09-27 | 联合矿产（天津）有限公司 | By stabilized fire proofing composition |
| US11554994B2 (en) | 2016-11-03 | 2023-01-17 | Allied Mineral Products, Llc | Stabilized refractory compositions |
| WO2019042105A1 (en) * | 2017-09-01 | 2019-03-07 | 陆宇皇金建材（河源）有限公司 | Sound insulation material, sound insulation plate, and partition structure of locomotive carriage |
| US11479508B2 (en) | 2017-09-01 | 2022-10-25 | Luyu Royal Gold Building Materials (Heyuan) Co., Ltd | Sound insulating material, sound insulating plate and partition structure of train carriage |
| CN112441608A (en) * | 2019-08-28 | 2021-03-05 | 西南科技大学 | Preparation method of nano calcium hydroxide whisker |
| CN112441608B (en) * | 2019-08-28 | 2023-06-16 | 西南科技大学 | Preparation method of nano calcium hydroxide whisker |
| CN113896499A (en) * | 2021-09-17 | 2022-01-07 | 西安欧盛达科技有限公司 | Method for manufacturing novel heat-insulating fireproof material |
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| CN104072083B (en) | 2016-01-20 |
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