CN104068302A - Enteromorpha polysaccharide oral liquid and preparation method thereof - Google Patents
Enteromorpha polysaccharide oral liquid and preparation method thereof Download PDFInfo
- Publication number
- CN104068302A CN104068302A CN201310122512.0A CN201310122512A CN104068302A CN 104068302 A CN104068302 A CN 104068302A CN 201310122512 A CN201310122512 A CN 201310122512A CN 104068302 A CN104068302 A CN 104068302A
- Authority
- CN
- China
- Prior art keywords
- grass polysaccharide
- sea grass
- enteromorpha
- sea
- oral liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000004676 glycans Chemical class 0.000 title claims abstract description 60
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 60
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 60
- 241000196252 Ulva Species 0.000 title claims abstract description 31
- 239000007788 liquid Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 15
- 239000003765 sweetening agent Substances 0.000 claims abstract description 15
- 238000001291 vacuum drying Methods 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 238000010298 pulverizing process Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 108090000790 Enzymes Proteins 0.000 claims abstract description 5
- 102000004190 Enzymes Human genes 0.000 claims abstract description 5
- 238000012856 packing Methods 0.000 claims abstract description 5
- 238000007789 sealing Methods 0.000 claims abstract description 5
- 230000001954 sterilising effect Effects 0.000 claims abstract description 5
- 238000005303 weighing Methods 0.000 claims abstract description 5
- 230000009849 deactivation Effects 0.000 claims abstract description 3
- 241000544058 Halophila Species 0.000 claims description 54
- 238000002386 leaching Methods 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 9
- 235000002722 Dioscorea batatas Nutrition 0.000 claims description 9
- 235000006536 Dioscorea esculenta Nutrition 0.000 claims description 9
- 240000001811 Dioscorea oppositifolia Species 0.000 claims description 9
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 claims description 9
- 244000241838 Lycium barbarum Species 0.000 claims description 9
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 7
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 7
- 235000010447 xylitol Nutrition 0.000 claims description 7
- 239000000811 xylitol Substances 0.000 claims description 7
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 7
- 229960002675 xylitol Drugs 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 108090000526 Papain Proteins 0.000 claims description 4
- 239000004365 Protease Substances 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 238000005516 engineering process Methods 0.000 claims description 4
- 229940088598 enzyme Drugs 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 235000012907 honey Nutrition 0.000 claims description 4
- 229940055729 papain Drugs 0.000 claims description 4
- 235000019834 papain Nutrition 0.000 claims description 4
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 239000013049 sediment Substances 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 235000021552 granulated sugar Nutrition 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 2
- 238000003809 water extraction Methods 0.000 claims description 2
- 235000011201 Ginkgo Nutrition 0.000 claims 1
- 244000194101 Ginkgo biloba Species 0.000 claims 1
- 235000008100 Ginkgo biloba Nutrition 0.000 claims 1
- 240000007164 Salvia officinalis Species 0.000 claims 1
- 235000005412 red sage Nutrition 0.000 claims 1
- 210000004369 blood Anatomy 0.000 abstract description 10
- 239000008280 blood Substances 0.000 abstract description 10
- 230000036039 immunity Effects 0.000 abstract description 7
- 206010028980 Neoplasm Diseases 0.000 abstract description 3
- 230000002708 enhancing effect Effects 0.000 abstract description 2
- 235000000346 sugar Nutrition 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- 241000512259 Ascophyllum nodosum Species 0.000 abstract 1
- 240000000599 Lentinula edodes Species 0.000 abstract 1
- 235000001715 Lentinula edodes Nutrition 0.000 abstract 1
- 244000241872 Lycium chinense Species 0.000 abstract 1
- 235000015468 Lycium chinense Nutrition 0.000 abstract 1
- 235000004879 dioscorea Nutrition 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000012869 ethanol precipitation Methods 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 230000035764 nutrition Effects 0.000 abstract 1
- 150000002632 lipids Chemical class 0.000 description 4
- 230000000259 anti-tumor effect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 241000195493 Cryptophyta Species 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 235000013376 functional food Nutrition 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000002218 hypoglycaemic effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 206010016654 Fibrosis Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 241000206607 Porphyra umbilicalis Species 0.000 description 1
- 210000001744 T-lymphocyte Anatomy 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000032677 cell aging Effects 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 230000007882 cirrhosis Effects 0.000 description 1
- 208000019425 cirrhosis of liver Diseases 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000011132 hemopoiesis Effects 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035772 mutation Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 230000004614 tumor growth Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention relates to an enteromorpha polysaccharide oral liquid and a preparation method thereof. The invention is characterized by adopting the following technical scheme: 1, obtaining enteromorpha polysaccharide by using enteromorpha as a raw material through purification, drying, pulverizing, extracting with hot water, enzymolysis, enzyme deactivation, centrifuging purification, ethanol precipitation and vacuum drying in sequence; 2, weighing 30-40% of lentinula edodes, 10-30% of kelp, 10-30% of yams and 10-30% of Chinese wolfberries in percentage by weight, and preparing a Chinese medicinal herb extract for later use through procedures of mixing, pulverizing, extracting in hot water, centrifuging, concentration, vacuum drying and the like; and 3, mixing 5-15% of enteromorpha polysaccharide, 5-15% of Chinese medicinal herb extract, 5-10% of sweetening agents and the balance of water in percentage by weight, and sterilizing, bottling, sealing, inspecting and packing the mixed liquid to obtain a finished product. The enteromorpha polysaccharide oral liquid is rich in nutrition and high in safety, and has multiple health-care functions of reducing blood sugar, reducing blood fat, enhancing the immunity, resisting tumors and the like.
Description
Technical field
The invention belongs to functional food manufacture field, more particularly, relate to a kind of sea grass polysaccharide oral liquid and preparation method thereof.
Background technology
Enteromorpha (Enteromorpha) is a kind of large-scale green alga, is commonly called as tongue bar, green laver etc., is the algae of Chlorophyta Ulvales Ulvaceae Enteromorpha, is grown in intertidal zone.In China, Enteromorpha output is very high, especially East Coastal.In recent years, the Fast-propagation of Enteromorpha pollutes China coast, and the pollution causing for administering Enteromorpha excessive multiplication, need to expend a large amount of manpower and materials, therefore if Enteromorpha is used, not only can administers Enteromorpha and pollute, and can also turn waste into wealth simultaneously.Enteromorpha is edible and medicinal algae since ancient times, studies confirm that: the main component water-soluble polysaccharide of Enteromorpha is the composition that pharmacologically active is very strong, there is reducing blood lipid, anti-oxidant, antitumor and strengthen the BAs such as immunity, can effectively prevent and treat various diseases.
But up to the present, the sea grass polysaccharide of take is few as main functional food, and its medicinal health value is not also excavated fully.The tonifying Qi of the Traditional Chinese Medicine principle of enriching blood can be had complementary advantages, bring out the best in each other with the effect of sea grass polysaccharide.Through patent retrieval and data consultation, for the exploitation of sea grass polysaccharide, there is not yet the report that utilizes Chinese Traditional Medicine technology and biotechnology to combine to manufacture oral liquid.
Summary of the invention
The present invention is exactly for the problems referred to above, and a kind of sea grass polysaccharide oral liquid and preparation method thereof is provided, and product prepared by this technique is not only nutritious, safe, and has hypoglycemic, reducing blood lipid, enhancing immunity, the plurality of health care functions such as antitumor.
For solving the problems of the technologies described above, the component that a technical scheme of the present invention is described oral liquid and weight content are sea grass polysaccharide 5~15%, Chinese medical extract 5~15%, sweetener 5~10%, and surplus is water.Described sea grass polysaccharide is to adopt hot water lixiviate, enzyme process except step acquisitions such as albumen, alcohol precipitations; Described Chinese medical extract dry powder is to adopt hot water extraction to obtain.
Described sweetener is one or both in white granulated sugar, xylitol, FOS, honey.
The raw material of described acquisition Chinese medical extract is mushroom, sea-tangle, Chinese yam, matrimony vine.Percentage by weight during its compatibility is mushroom 30~40%, sea-tangle 10~30%, Chinese yam 10~30%, matrimony vine 10~30%.
A preparation method for sea grass polysaccharide oral liquid, comprises following preparation steps:
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to after 60~80 ℃ of oven dry, pulverize, sieve (20~60 order).
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 20~60 (w/v, g/ml), add distilled water, fully stir, 90~100 ℃ are soaked 4~6h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 1%~3%, regulating pH value is 5.0~6.0, at 50~60 ℃ of enzymolysis 1~2h of temperature, obtains sea grass polysaccharide the second leaching liquor.
4. Enteromorpha the second leaching liquor is heated to 90~100 ℃, residual enzyme is carried out to deactivation, fully stir and soak, process 30~60min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by sea grass polysaccharide the 3rd leaching liquor at the centrifugal 10~15min of 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 2~3 times of volumes of concentrate, after 4 ℃ of standing 3~4h, the centrifugal 10~15min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30~40%, sea-tangle 10~30%, Chinese yam 10~30%, matrimony vine 10~30%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying.
(3) choose one or both in xylitol, FOS, honey as sweetener
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 5~15%, Chinese medical extract 5~15%, sweetener 5~10% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Beneficial effect of the present invention:
The main component containing in the present invention formula is sea grass polysaccharide, and sea grass polysaccharide has significant reducing blood lipid, antifatigue, antibacterial, antitumor and to strengthen the various biological such as immunity active.The compatibility raw material mushroom of its Chinese medical extract can have step-down, norcholesterol, reducing blood lipid, anticancer, improve immunity, can prevention of arterial sclerosis, the disease such as cirrhosis, cancer; Sea-tangle has hypoglycemic, fat-reducing, beauty treatment, inhibition tumour, step-down, lipopenicillinase, delaying sanility prevention cardiovascular and cerebrovascular diseases, improves immunity.Chinese yam can increase T lymphocytes in human body, strengthens immunologic function, and delaying cell aging reduces cholesterol and triglycerides, and the illnesss such as hypertension and high fat of blood are improved to effect.The adjustable body's immunity of matrimony vine, can effectively suppress tumor growth and cell mutation, have delay senility, the effect of AFL, adjusting blood fat and the aspect such as blood sugar, promotion hematopoiesis function,
Rich raw material sources used of the present invention, makes its more easily large-scale batch production.
The present invention's raw material used are all natural product, and safety has no side effect, and can eat for a long time.
The specific embodiment
Embodiment 1
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to 40 orders of pulverizing, sieve after 80 ℃ of oven dry.
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 60 (w/v, g/ml), add distilled water, fully stir, 90 ℃ of lixiviate 4h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 3%, regulating pH value is 5.0, at temperature 50 enzymolysis 1h, obtains sea grass polysaccharide the second leaching liquor.
4. sea grass polysaccharide the second leaching liquor is heated to 100 ℃, fully stirs and soak, process 30min, obtain sea grass polysaccharide the 3rd leaching liquor
5. by the centrifugal 10min of sea grass polysaccharide the 3rd leaching liquor 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 3 times of volumes of concentrate, after 4 ℃ of standing 3h, the centrifugal 10min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30%, sea-tangle 30%, Chinese yam 20%, matrimony vine 20%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose FOS as sweetener, standby.
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener (FOS) and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 10%, Chinese medical extract 10%, FOS 5% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Embodiment 2
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to 40 orders of pulverizing, sieve after 80 ℃ of oven dry.
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 60 (w/v, g/ml), add distilled water, fully stir, 90 ℃ of lixiviate 4h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 3%, regulating pH value is 5.0, at temperature 50 C enzymolysis 1h, obtains sea grass polysaccharide the second leaching liquor.
4. sea grass polysaccharide the second leaching liquor is heated to 100 ℃, fully stirs and soak, process 30min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by the centrifugal 10min of sea grass polysaccharide the 3rd leaching liquor 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 3 times of volumes of concentrate, after 4 ℃ of standing 3h, the centrifugal 10min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30%, sea-tangle 20%, Chinese yam 30%, matrimony vine 20%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose xylitol as sweetener, standby.
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener (xylitol) and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 10%, Chinese medical extract 15%, xylitol 5% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Claims (4)
1. a sea grass polysaccharide oral liquid, is characterized in that, the component of described oral liquid and weight content are sea grass polysaccharide 5~15%, Chinese medical extract 5~15%, sweetener 5~10%, and surplus is water.Described sea grass polysaccharide is to adopt hot water lixiviate, enzyme process except step acquisitions such as albumen, alcohol precipitations; Described Chinese medical extract is to adopt hot water extraction to obtain.
2. a kind of sea grass polysaccharide oral liquid according to claim 1, is characterized in that described sweetener is one or both in white granulated sugar, xylitol, FOS, honey.
3. a kind of sea grass polysaccharide oral liquid according to claim 1 and 2, the raw material that it is characterized in that obtaining Chinese medical extract is mushroom, sea-tangle, the red sage root, ginkgo leaf, Chinese yam, matrimony vine.Percentage by weight during its compatibility is mushroom 30~40%, sea-tangle 10~30%, Chinese yam 10~30%, matrimony vine 10~30%.
4. the preparation method of a kind of sea grass polysaccharide oral liquid according to claim 1, is characterized in that through following preparation technology:
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to after 60~80 ℃ of oven dry, pulverize, sieve (20~60 order).
2. take gained Enteromorpha powder, by solid-liquid ratio l: 20~60 (w/v, g/ml) add distilled water, fully stir, 90~100 ℃ are soaked 4~6h, obtain sea grass polysaccharide the first leaching liquor.
3. in described Enteromorpha the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 1%~3%, regulating pH value is 5.0~6.0, at 50~60 ℃ of enzymolysis 1~2h of temperature, obtains sea grass polysaccharide the second leaching liquor.
4. Enteromorpha the second leaching liquor is heated to 90~100 ℃, residual enzyme is carried out to deactivation, fully stir and soak, process 30~60min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by sea grass polysaccharide the 3rd leaching liquor at the centrifugal 10~15min of 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 2~3 times of volumes of concentrate, after 4 ℃ of standing 3~4h, the centrifugal 10~15min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30~40%, sea-tangle 10~30%, Chinese yam 10~30%, matrimony vine 10~30%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose one or both in white granulated sugar, xylitol, FOS, honey as sweetener
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 5~15%, Chinese medical extract 5~15%, sweetener 5~10% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310122512.0A CN104068302A (en) | 2013-03-29 | 2013-03-29 | Enteromorpha polysaccharide oral liquid and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310122512.0A CN104068302A (en) | 2013-03-29 | 2013-03-29 | Enteromorpha polysaccharide oral liquid and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN104068302A true CN104068302A (en) | 2014-10-01 |
Family
ID=51590221
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310122512.0A Pending CN104068302A (en) | 2013-03-29 | 2013-03-29 | Enteromorpha polysaccharide oral liquid and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104068302A (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105011150A (en) * | 2015-08-26 | 2015-11-04 | 缪雪峰 | Preparation technology of seaweed healthcare oral liquid |
CN105055616A (en) * | 2015-08-12 | 2015-11-18 | 蔡婷婷 | Seaweed-containing healthcare oral liquid |
CN106819704A (en) * | 2017-03-07 | 2017-06-13 | 桂林理工大学 | Pyrus nivalis local flavor sea grass polysaccharide reducing blood lipid and function of blood sugar reduction beverage and preparation method |
CN108003199A (en) * | 2017-07-12 | 2018-05-08 | 中国科学院过程工程研究所 | A kind of Enteromorpha oligosaccharide with function of blood sugar reduction and its preparation method and application |
CN108409877A (en) * | 2017-07-12 | 2018-08-17 | 中国科学院过程工程研究所 | Sea grass polysaccharide, enteromorpha oligosaccharide, medical composition and its use |
CN109393451A (en) * | 2017-08-18 | 2019-03-01 | 青岛瑞思德生物科技有限公司 | A kind of health food that immunity can be improved containing Enteromorpha |
WO2019100843A1 (en) * | 2017-08-17 | 2019-05-31 | 福建海兴保健食品有限公司 | Enteromorpha prolifera polysaccharide composite blood lipid-lowering health care product and preparation method therefor |
WO2021078297A1 (en) * | 2019-10-25 | 2021-04-29 | 运鸿集团股份有限公司 | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
CN114376233A (en) * | 2022-03-23 | 2022-04-22 | 青岛海大生物集团股份有限公司 | Enteromorpha polysaccharide health food with immunity enhancing function and preparation method thereof |
CN114672235A (en) * | 2022-04-25 | 2022-06-28 | 山东中胜涂料有限公司 | High-wear-resistance quick-drying water-based acrylic polyurethane finish paint and preparation method thereof |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1977865A (en) * | 2005-11-30 | 2007-06-13 | 广东省农业科学院农业生物技术研究所 | Method for preparing domestic fungus health care oral liquid |
CN102100322A (en) * | 2011-01-11 | 2011-06-22 | 福建农林大学 | Composite food glue containing enteromorpha gel polysaccharide and preparation method thereof |
-
2013
- 2013-03-29 CN CN201310122512.0A patent/CN104068302A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1977865A (en) * | 2005-11-30 | 2007-06-13 | 广东省农业科学院农业生物技术研究所 | Method for preparing domestic fungus health care oral liquid |
CN102100322A (en) * | 2011-01-11 | 2011-06-22 | 福建农林大学 | Composite food glue containing enteromorpha gel polysaccharide and preparation method thereof |
Non-Patent Citations (3)
Title |
---|
徐大伦等: "《浒苔多糖脱蛋白方法的研究》", 《水产科学》 * |
徐大伦等: "《浒苔水溶性多糖提取的工艺研究》", 《浙江海洋学院学报)自然科学版》 * |
陈达妙等: "《浒苔多糖脱蛋白脱盐方法的优选》", 《中国食物与营养》 * |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105055616A (en) * | 2015-08-12 | 2015-11-18 | 蔡婷婷 | Seaweed-containing healthcare oral liquid |
CN105011150A (en) * | 2015-08-26 | 2015-11-04 | 缪雪峰 | Preparation technology of seaweed healthcare oral liquid |
CN106819704A (en) * | 2017-03-07 | 2017-06-13 | 桂林理工大学 | Pyrus nivalis local flavor sea grass polysaccharide reducing blood lipid and function of blood sugar reduction beverage and preparation method |
CN108003199A (en) * | 2017-07-12 | 2018-05-08 | 中国科学院过程工程研究所 | A kind of Enteromorpha oligosaccharide with function of blood sugar reduction and its preparation method and application |
CN108409877A (en) * | 2017-07-12 | 2018-08-17 | 中国科学院过程工程研究所 | Sea grass polysaccharide, enteromorpha oligosaccharide, medical composition and its use |
CN108409877B (en) * | 2017-07-12 | 2020-02-18 | 中国科学院过程工程研究所 | Enteromorpha polysaccharide, enteromorpha oligosaccharide, pharmaceutical composition and application thereof |
WO2019100843A1 (en) * | 2017-08-17 | 2019-05-31 | 福建海兴保健食品有限公司 | Enteromorpha prolifera polysaccharide composite blood lipid-lowering health care product and preparation method therefor |
CN109393451A (en) * | 2017-08-18 | 2019-03-01 | 青岛瑞思德生物科技有限公司 | A kind of health food that immunity can be improved containing Enteromorpha |
WO2021078297A1 (en) * | 2019-10-25 | 2021-04-29 | 运鸿集团股份有限公司 | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
GB2605893A (en) * | 2019-10-25 | 2022-10-19 | China Yunhong Holdings Co Ltd | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
GB2605893B (en) * | 2019-10-25 | 2023-12-06 | China Yunhong Holdings Co Ltd | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
CN114376233A (en) * | 2022-03-23 | 2022-04-22 | 青岛海大生物集团股份有限公司 | Enteromorpha polysaccharide health food with immunity enhancing function and preparation method thereof |
CN114672235A (en) * | 2022-04-25 | 2022-06-28 | 山东中胜涂料有限公司 | High-wear-resistance quick-drying water-based acrylic polyurethane finish paint and preparation method thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104068302A (en) | Enteromorpha polysaccharide oral liquid and preparation method thereof | |
CN102273680B (en) | Flammulina velutipes polysaccharide composite beverage and preparation method thereof | |
CN102965237B (en) | Mulberry-ganoderma fruit wine and production method thereof | |
CN103610165B (en) | Preparation method of artemisia halodendron beverage | |
CN103740566B (en) | Rosa roxbunghii medicinal liquor and preparation method thereof | |
CN102614499B (en) | Yak skin collagen compound traditional Tibetan medicine with anti-fatigue effect and preparation process thereof | |
CN105368688A (en) | Grape vinegar | |
CN105495578A (en) | Abalone-sea cucumber compounded liquid as well as preparation method and application thereof | |
CN104928140A (en) | Compound fermentation type winter-jujube health care wine and production technology thereof | |
CN102715390A (en) | Liver-protecting functional food and preparation method thereof | |
CN104888046B (en) | A kind of herbal health care oral liquid for having effects that improve anaemia | |
CN102229877B (en) | Brewing method for pine pollen wine | |
CN1051714C (en) | Traditional Chinese patent medicine for strengthening spleen and appetizing and its preparation method | |
CN106107340A (en) | A kind of antioxidation resisting fatigue Radix Astragali drinks and preparation technology thereof | |
CN105852063A (en) | Sargassum fusiforme polysaccharide-rich nutrition and health care product | |
CN105030858A (en) | Cynomorium songaricum healthcare tablet and preparation method thereof | |
CN104877882A (en) | Astaxanthin composite mixed liquor with blood glucose reducing function | |
CN104911056B (en) | Cofermentation method maca yellow wine and processing method thereof | |
CN106072365A (en) | A kind of yellow mushroom mushroom essence with health-care effect and preparation method thereof | |
CN103960486A (en) | Poultry forage for producing health-care eggs | |
CN103271351B (en) | Oral giant salamander liquid for brain strengthening, and preparation method thereof | |
CN103589569B (en) | Production technique of compound fermented ulva health wine | |
KR101450827B1 (en) | Allium hookeri drink and its manufacturing method | |
CN103859377A (en) | Formula and preparation method of life cultivation and health preservation food helpful for reducing radiation injury | |
CN108095111B (en) | Nutritional composition containing deep seawater minerals and its application in promoting lactation after delivery |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20141001 |
|
WD01 | Invention patent application deemed withdrawn after publication |