CN103950899A - 一种过氧化钙的制备方法 - Google Patents
一种过氧化钙的制备方法 Download PDFInfo
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- CN103950899A CN103950899A CN201410127248.4A CN201410127248A CN103950899A CN 103950899 A CN103950899 A CN 103950899A CN 201410127248 A CN201410127248 A CN 201410127248A CN 103950899 A CN103950899 A CN 103950899A
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- CN
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- Prior art keywords
- calcium
- peroxide
- hydrogen peroxide
- content
- calcium peroxide
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000004343 Calcium peroxide Substances 0.000 title claims abstract description 55
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 title claims abstract description 55
- 235000019402 calcium peroxide Nutrition 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 90
- 239000000843 powder Substances 0.000 claims abstract description 34
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 30
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 29
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 29
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 29
- 238000006243 chemical reaction Methods 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 27
- 239000012452 mother liquor Substances 0.000 claims abstract description 20
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000009413 insulation Methods 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 239000011259 mixed solution Substances 0.000 claims abstract description 6
- 229960004418 trolamine Drugs 0.000 claims description 18
- 239000011734 sodium Substances 0.000 claims description 16
- 229910052708 sodium Inorganic materials 0.000 claims description 16
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 16
- 238000000967 suction filtration Methods 0.000 claims description 14
- 101710194948 Protein phosphatase PhpP Proteins 0.000 claims description 12
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 238000010790 dilution Methods 0.000 claims description 2
- 239000012895 dilution Substances 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000010865 sewage Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 2
- 238000005086 pumping Methods 0.000 abstract 2
- 239000003381 stabilizer Substances 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 239000002994 raw material Substances 0.000 description 12
- 238000012423 maintenance Methods 0.000 description 10
- 238000001291 vacuum drying Methods 0.000 description 10
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical group [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 5
- 239000001110 calcium chloride Substances 0.000 description 5
- 229910001628 calcium chloride Inorganic materials 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 241000251468 Actinopterygii Species 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241000143060 Americamysis bahia Species 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000238557 Decapoda Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000006213 oxygenation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000003206 sterilizing agent Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN201410127248.4A CN103950899B (zh) | 2014-04-01 | 2014-04-01 | 一种过氧化钙的制备方法 |
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CN201410127248.4A CN103950899B (zh) | 2014-04-01 | 2014-04-01 | 一种过氧化钙的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN103950899A true CN103950899A (zh) | 2014-07-30 |
CN103950899B CN103950899B (zh) | 2016-01-20 |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105439101A (zh) * | 2015-12-28 | 2016-03-30 | 常熟市宏宇钙化物有限公司 | 一种高纯过氧化钙的制备方法 |
CN105668521A (zh) * | 2016-01-06 | 2016-06-15 | 华东交通大学 | 一种高纯度纳米粒径表面光滑的过氧化钙的制备方法 |
CN111115585A (zh) * | 2019-12-26 | 2020-05-08 | 重庆新申世纪新材料科技有限公司 | 一种制备高堆密度过氧化锶的方法及其产品 |
CN112480935A (zh) * | 2020-12-17 | 2021-03-12 | 河北省地质实验测试中心 | 一种过氧化钙缓释复合材料及其制备方法和应用 |
CN113548916A (zh) * | 2021-06-25 | 2021-10-26 | 山东农大肥业科技有限公司 | 含增氧剂和腐植酸的笼养鸡粪专用腐熟剂及其应用 |
CN114634165A (zh) * | 2022-01-20 | 2022-06-17 | 常熟理工学院 | 一种利用垃圾焚烧飞灰制备过氧化钙的方法 |
-
2014
- 2014-04-01 CN CN201410127248.4A patent/CN103950899B/zh active Active
Non-Patent Citations (3)
Title |
---|
梅允福: "过氧化钙的制备和应用", 《四川化工与腐蚀控制》, vol. 3, no. 4, 31 December 2000 (2000-12-31), pages 42 * |
王卫兵等: "生产工艺条件对过氧化钙产率影响实验研究", 《陕西理工学院学报(自然科学版)》, vol. 24, no. 4, 31 December 2008 (2008-12-31) * |
王卫兵等: "过氧化钙的研制", 《应用化工》, vol. 42, no. 3, 31 March 2013 (2013-03-31), pages 5 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105439101A (zh) * | 2015-12-28 | 2016-03-30 | 常熟市宏宇钙化物有限公司 | 一种高纯过氧化钙的制备方法 |
CN105668521A (zh) * | 2016-01-06 | 2016-06-15 | 华东交通大学 | 一种高纯度纳米粒径表面光滑的过氧化钙的制备方法 |
CN111115585A (zh) * | 2019-12-26 | 2020-05-08 | 重庆新申世纪新材料科技有限公司 | 一种制备高堆密度过氧化锶的方法及其产品 |
CN111115585B (zh) * | 2019-12-26 | 2023-06-30 | 重庆新申世纪新材料科技有限公司 | 一种制备高堆密度过氧化锶的方法及其产品 |
CN112480935A (zh) * | 2020-12-17 | 2021-03-12 | 河北省地质实验测试中心 | 一种过氧化钙缓释复合材料及其制备方法和应用 |
CN113548916A (zh) * | 2021-06-25 | 2021-10-26 | 山东农大肥业科技有限公司 | 含增氧剂和腐植酸的笼养鸡粪专用腐熟剂及其应用 |
CN114634165A (zh) * | 2022-01-20 | 2022-06-17 | 常熟理工学院 | 一种利用垃圾焚烧飞灰制备过氧化钙的方法 |
CN114634165B (zh) * | 2022-01-20 | 2023-08-29 | 常熟理工学院 | 一种利用垃圾焚烧飞灰制备过氧化钙的方法 |
Also Published As
Publication number | Publication date |
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CN103950899B (zh) | 2016-01-20 |
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C06 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee | ||
CP01 | Change in the name or title of a patent holder |
Address after: 312369 Shangyu Industrial Park, Hangzhou Bay, Zhejiang, Shaoxing Patentee after: Zhejiang Jinke entertainment Limited by Share Ltd. Address before: 312369 Shangyu Industrial Park, Hangzhou Bay, Zhejiang, Shaoxing Patentee before: ZHEJIANG JINKE CHEMICALS Co.,Ltd. |
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CP03 | Change of name, title or address |
Address after: 312369 Hangzhou Bay Shangyu economic and Technological Development Zone, Zhejiang Province Patentee after: Zhejiang Jinke cultural industry Limited by Share Ltd. Address before: 312369 Shangyu Industrial Park, Hangzhou Bay, Zhejiang, Shaoxing Patentee before: Zhejiang Jinke entertainment Limited by Share Ltd. |
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TR01 | Transfer of patent right |
Effective date of registration: 20180926 Address after: 312369 Shangyu economic and Technological Development Zone, Hangzhou Bay, Zhejiang Patentee after: ZHEJIANG JINKE HOUSEHOLD CHEMICAL MATERIALS Co.,Ltd. Address before: 312369 Shangyu economic and Technological Development Zone, Hangzhou Bay, Zhejiang Patentee before: Zhejiang Jinke cultural industry Limited by Share Ltd. |
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TR01 | Transfer of patent right | ||
CP03 | Change of name, title or address |
Address after: 312300 Hangzhou Shangyu economic and Technological Development Zone, Shaoxing, Zhejiang Patentee after: Zhejiang Jinke Daily Chemical New Materials Co.,Ltd. Address before: 312369 Shangyu economic and Technological Development Zone, Hangzhou Bay, Zhejiang Patentee before: ZHEJIANG JINKE HOUSEHOLD CHEMICAL MATERIALS Co.,Ltd. |
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CP03 | Change of name, title or address |