CN103948164B - Buccal cigarette extract and preparation method thereof and buccal cigarette - Google Patents
Buccal cigarette extract and preparation method thereof and buccal cigarette Download PDFInfo
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- CN103948164B CN103948164B CN201410211617.8A CN201410211617A CN103948164B CN 103948164 B CN103948164 B CN 103948164B CN 201410211617 A CN201410211617 A CN 201410211617A CN 103948164 B CN103948164 B CN 103948164B
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Abstract
The invention discloses a kind of buccal cigarette extract and preparation method thereof and buccal cigarette, the preparation method of described buccal cigarette extract is by cured tobacco leaf sterilizing, extract with distilled water, filter, regulation filtrate pH to 9-10, then carry out filtrate distilling, condensing, collect distillate and be buccal cigarette extract.Tobacco is processed by the present invention, it is thus achieved that buccal cigarette extract, without pigment in this extract, will not deposit consumer oral cavity chromogenesis；Simultaneously possibly together with meeting consumer's demand to nicotine amount in extract, nicotine content can also control in safer scope；And without the harmful components such as condensed-nuclei aromatics, tobacco-specific nitrosamine in buccal cigarette extract.
Description
Technical field
The invention belongs to smokeless tobacco articles field, be specifically related to a kind of buccal cigarette extract and preparation method thereof
With suck liquid extract for preparing buccal cigarette.
Background technology
Along with the growing interest to consumer health, traditional cigarette consumption pattern increasingly by countries in the world and
The criticism of anti-cigarette tissue and restriction.But due to habituation feature and the consumption habit of tobacco, the total amount of smoking population
It is in ascendant trend.The sensory experience that tobacco is brought, the large-scale cigarette of external several families is obtained in order to meet consumer
Grass group company develops the smokeless tobacco articles substitute as traditional cigarette.China the most also develops one
A little smokeless tobacco articles, especially in the majority with mouth insertion tobacco goods.These buccal cigarette are typically directly former with tobacco
Material, is not only easily caused consumer's oral pigment deposition, and its nitrosamine compound contained and higher
Nicotine content also consumer can be produced health threat.Therefore by tobacco through certain process, look is removed
Element and some harmful compositions, make buccal cigarette significant the most again.
Summary of the invention
It is an object of the invention to develop the buccal cigarette that a kind of harmful substance contents is few, little to harm, this mouth
Containing cigarette, tobacco is carried out extract acquisition tobacco extract to add in buccal cigarette.
In order to reach above-mentioned technique effect, the present invention takes techniques below scheme:
The preparation method of a kind of buccal cigarette extract, comprises the following steps: by cured tobacco leaf sterilizing, uses
Distilled water extracts, and filters, and regulates filtrate pH to 9-10, then carries out filtrate distilling, condensing, and receives
Collection distillate is buccal cigarette extract.
In order to increase the taste of buccal cigarette, adding dried peppermint leaf in cured tobacco leaf, the weight of dried peppermint leaf is flue-cured tobacco
The 0-10% of tobacco leaf.
During extracting with distilled water, the quality of cured tobacco leaf and the volume of the distilled water for extraction
For (0.05g:1mL)-(0.2g:1mL).
During extracting with distilled water, the gross weight of cured tobacco leaf and dried peppermint leaf and the steaming for extraction
The volume ratio of distilled water is (0.05g:1mL)-(0.2g:1mL).
Cured tobacco leaf in the present invention be in delicate fragrance type, Luzhou-flavor, flat-flavor any one.
The mode of the extraction of this method is the one in ultrasonic extraction, supercritical extract, oscillation extraction.
A kind of buccal cigarette, including following components in parts by weight: buccal cigarette extract 1-3 part；Candy slurries 65-110
Part；Edible hydrogenated oil 2-4 part；Soybean lecithin 0.5-0.6 part；Honey essence 0.5-0.6 part.According to the present invention
An embodiment, candy slurries are made up of the granulated sugar of 60-70 weight portion and the syrup of 5-40 weight portion.
According to another embodiment of the present invention, a kind of buccal cigarette, including following components in parts by weight: buccal cigarette
Extract 1-3 part；Candy slurries 85-105 part；Edible hydrogenated oil 2.5-3.0 part；Soybean lecithin 0.5-0.6
Part；Honey essence 0.5-0.6 part.
According to another embodiment of the invention, a kind of buccal cigarette, including following components in parts by weight: suck
Cigarette extract 1-3 part；Granulated sugar 60-70 part；Syrup 25.8-36.5 part；Edible hydrogenated oil 2.5-3.0 part；Greatly
Fabaceous Lecithin 0.5-0.6 part；Honey essence 0.5-0.6 part.
In embodiments of the invention, the preparation method of buccal cigarette is: buccal cigarette extract adds to candy slurry
Liquid stirs, is subsequently adding edible hydrogenated oil, soybean lecithin and the mixing of honey essence, be in harmonious proportion to without viscous
Sexuality, is poured into mould, grain forming, the demoulding, cooling, packaging.
The present invention compared with prior art, has a following beneficial effect:
Tobacco is processed by the present invention, it is thus achieved that buccal cigarette extract, without pigment in this extract, and will not
Consumer oral cavity chromogenesis is deposited；Simultaneously possibly together with meeting consumer to nicotine amount in extract
Demand, nicotine content can also control in safer scope；And without thick in buccal cigarette extract
The harmful components such as PAH, tobacco-specific nitrosamine.
Detailed description of the invention
Below in conjunction with embodiments of the invention, the invention will be further elaborated.
Embodiment 1
After red big tobacco leaf removes stalk, dry 2 hours in 40 DEG C of baking ovens, pulverize and cross 40 mesh sieves, weighing offal
1kg, after ultraviolet-sterilization, adds 12L distilled water, ultrasonic extraction 1 hour, filters, add hydrogen-oxygen in filtrate
Changing sodium is 10 to pH value, pours in steam distillation apparatus that (distilling apparatus is through autoclave sterilization and purple into
Outer sterilization process), collect 4000mL distillate, obtain buccal cigarette extract.Distilling apparatus is high through high temperature
The step of pressure sterilizing is as follows: the concentrated sulfuric acid soaks 24h flowing water and rinses distilled water flushing 3 times 100 DEG C
Dry 100 DEG C of dry for standby of high pressure steam sterilization.
Embodiment 2
After red big tobacco leaf removes stalk, dry 2 hours in 40 DEG C of baking ovens, pulverize and cross 40 mesh sieves, weighing offal
1kg, after ultraviolet-sterilization, adds 12L distilled water, ultrasonic extraction 1 hour, filters, add in filtrate
1kg offal, repeat the above steps 3 times.By repeat extraction filtrate in add NaOH to pH value be 10,
Pour into (distilling apparatus is through autoclave sterilization and ultraviolet-sterilization process) in steam distillation apparatus, collect
4000mL distillate, obtains the buccal cigarette extract of high-nicotine content.
Embodiment 3
After red big tobacco leaf removes stalk, dry 2 hours in 40 DEG C of baking ovens, pulverize and cross 40 mesh sieves, weighing offal
1kg, adds 50g dried peppermint leaf end, after ultraviolet-sterilization, adds 12L distilled water, ultrasonic extraction 1 hour, mistake
Filter, adding NaOH in filtrate is 10 to pH value, pours (distilling apparatus warp in steam distillation apparatus into
Cross autoclave sterilization and ultraviolet-sterilization process), collect 4000mL distillate, obtain containing peppermint note
Buccal cigarette extract.
Embodiment 4
Adding in candy slurries by the buccal cigarette extract of the above embodiments 3, stirring-type mixes 20 minutes
After, add edible hydrogenated oil, soybean lecithin, the mixing of honey essence, be in harmonious proportion to inviscid sense, be poured into mould
Tool, grain forming, the demoulding, cooling, it is packaged into finished product.
According to one embodiment of present invention, buccal cigarette includes buccal cigarette extract 1-3 part；Granulated sugar 60-70 part；
Syrup 5-40 part；Edible hydrogenated oil 2-4 part；Soybean lecithin 0.5-0.6 part；Honey essence 0.5-0.6 part.
In the specific embodiment of the present invention, buccal cigarette includes buccal cigarette extract 1 part；Granulated sugar 60 parts；Syrup
28.5 parts；Edible hydrogenated oil 3.0 parts；Soybean lecithin 0.5 part；0.5 part of honey essence.
The preparation method of buccal cigarette is as follows: buccal cigarette extract adds in candy slurries stirring, so
Rear addition edible hydrogenated oil, soybean lecithin and the mixing of honey essence, be in harmonious proportion to inviscid sense, be poured into mould,
Grain forming, the demoulding, cooling, packaging.
The buccal cigarette finished product of the above embodiments 4 is carried out nicotine, condensed-nuclei aromatics, tobacco peculiar N-nitrosamine
And Anionic recognition.Detection method is with reference to YC/T246-2008 " the mensuration gas of tobacco and tobacco product nicotine
Phase chromatography ", GB/T21130-2007 " mensuration of benzene [а] pyrene, YC/T in cigarette smoke condensates
184-2004 " tobacco and the mensuration of tobacco product tobacco peculiar N-nitrosamine ", YC/T296-2009 " tobacco
And the mensuration continuous flow method of tobacco product nitrate ".Testing result is shown in Table 1.From table 1 it follows that
The buccal cigarette that this buccal cigarette extract is made, does not contains benzene [а] pyrene, nitrate ion；Tobacco peculiar N-nitrous
Amine is in addition to NAT trace, and NNN, NAB, NNK all do not contain；Nicotine content is in medicine safe range
In.Compared with certain buccal cigarette commercially available, the buccal cigarette that this buccal cigarette extract is made is safer.
Table 1 buccal cigarette testing result
Although reference be made herein to invention has been described for the explanatory embodiment of the present invention, and above-described embodiment is only
For the present invention preferably embodiment, embodiments of the present invention are also not restricted to the described embodiments, it should
Understanding, those skilled in the art can be designed that a lot of other amendments and embodiment, and these are revised and real
The mode of executing will fall within spirit disclosed in the present application and spirit.
Claims (4)
1. a buccal cigarette, it is characterised in that include following components in parts by weight: buccal cigarette extract 1-3 part；
Candy slurries 65-110 part；Edible hydrogenated oil 2-4 part；Soybean lecithin 0.5-0.6 part；Honey essence 0.5-0.6
Part；Described candy slurries are made up of the granulated sugar of 60-70 weight portion and the syrup of 5-40 weight portion；
The preparation method of described buccal cigarette extract comprises the following steps: by cured tobacco leaf sterilizing, uses
Distilled water extracts, and filters, and regulates filtrate pH to 9-10, then carries out filtrate distilling, cold
Solidifying, collect distillate and be buccal cigarette extract；The quality of cured tobacco leaf and the distilled water for extraction
Volume be (0.05g:1mL)-(0.2g:1mL)；The mode of described extraction be ultrasonic extraction,
One in supercritical extract, oscillation extraction.
Buccal cigarette the most according to claim 1, it is characterised in that include following components in parts by weight: suck
Cigarette extract 1-3 part；Candy slurries 85-105 part；Edible hydrogenated oil 2.5-3.0 part；Soybean lecithin 0.5-0.6
Part；Honey essence 0.5-0.6 part.
Buccal cigarette the most according to claim 1, it is characterised in that add dried peppermint leaf in described cured tobacco leaf,
The weight of dried peppermint leaf is the 0-10% of cured tobacco leaf.
Buccal cigarette the most according to claim 3, it is characterised in that the gross weight of cured tobacco leaf and dried peppermint leaf with
Volume ratio for the distilled water of extraction is (0.05g:1mL)-(0.2g:1mL).
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| CN201410211617.8A CN103948164B (en) | 2014-05-19 | 2014-05-19 | Buccal cigarette extract and preparation method thereof and buccal cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410211617.8A CN103948164B (en) | 2014-05-19 | 2014-05-19 | Buccal cigarette extract and preparation method thereof and buccal cigarette |
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| CN103948164A CN103948164A (en) | 2014-07-30 |
| CN103948164B true CN103948164B (en) | 2016-08-24 |
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| CN201410211617.8A Active CN103948164B (en) | 2014-05-19 | 2014-05-19 | Buccal cigarette extract and preparation method thereof and buccal cigarette |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104489910B (en) * | 2014-11-24 | 2016-06-29 | 安徽中烟工业有限责任公司 | A kind of fire-cured tobacco type electronic cigarette liquid |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2226826Y (en) * | 1995-06-26 | 1996-05-15 | 张继岭 | Unharmful imitation cigarette |
| CN101233892A (en) * | 2008-02-29 | 2008-08-06 | 中国烟草总公司郑州烟草研究院 | Chewing gum containing tobacco component |
| CN101254026A (en) * | 2008-03-13 | 2008-09-03 | 中国烟草总公司郑州烟草研究院 | Bagging mouth-sucked drying tobacco products and method of preparing the same |
| CN103549648A (en) * | 2013-11-11 | 2014-02-05 | 云南烟草科学研究院 | Novel tabletting type smokeless tobacco product and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080286340A1 (en) * | 2007-05-16 | 2008-11-20 | Sven-Borje Andersson | Buffered nicotine containing products |
| US20130125904A1 (en) * | 2011-11-18 | 2013-05-23 | R.J. Reynolds Tobacco Company | Smokeless tobacco product comprising pectin component |
| US11944114B2 (en) * | 2012-06-20 | 2024-04-02 | Altria Client Services Llc | Smokeless tobacco lipid granules |
-
2014
- 2014-05-19 CN CN201410211617.8A patent/CN103948164B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2226826Y (en) * | 1995-06-26 | 1996-05-15 | 张继岭 | Unharmful imitation cigarette |
| CN101233892A (en) * | 2008-02-29 | 2008-08-06 | 中国烟草总公司郑州烟草研究院 | Chewing gum containing tobacco component |
| CN101254026A (en) * | 2008-03-13 | 2008-09-03 | 中国烟草总公司郑州烟草研究院 | Bagging mouth-sucked drying tobacco products and method of preparing the same |
| CN103549648A (en) * | 2013-11-11 | 2014-02-05 | 云南烟草科学研究院 | Novel tabletting type smokeless tobacco product and preparation method thereof |
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| CN103948164A (en) | 2014-07-30 |
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Effective date of registration: 20161222 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |
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