CN103882422B - 一种制备二硅化钽块体材料的方法 - Google Patents
一种制备二硅化钽块体材料的方法 Download PDFInfo
- Publication number
- CN103882422B CN103882422B CN201410125984.6A CN201410125984A CN103882422B CN 103882422 B CN103882422 B CN 103882422B CN 201410125984 A CN201410125984 A CN 201410125984A CN 103882422 B CN103882422 B CN 103882422B
- Authority
- CN
- China
- Prior art keywords
- tantalum silicide
- block materials
- silicide block
- powder
- spray
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000463 material Substances 0.000 title claims abstract description 80
- 229910021332 silicide Inorganic materials 0.000 title claims abstract description 72
- FVBUAEGBCNSCDD-UHFFFAOYSA-N silicide(4-) Chemical compound [Si-4] FVBUAEGBCNSCDD-UHFFFAOYSA-N 0.000 title claims abstract description 72
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 title claims abstract description 72
- 229910052715 tantalum Inorganic materials 0.000 title claims abstract description 71
- 238000000034 method Methods 0.000 title claims abstract description 43
- 239000007921 spray Substances 0.000 claims abstract description 36
- 239000000843 powder Substances 0.000 claims abstract description 26
- 239000007789 gas Substances 0.000 claims abstract description 16
- 238000000576 coating method Methods 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 12
- 238000007750 plasma spraying Methods 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 6
- 239000012159 carrier gas Substances 0.000 claims abstract description 5
- 238000005516 engineering process Methods 0.000 claims description 18
- 238000005507 spraying Methods 0.000 claims description 15
- 229910004217 TaSi2 Inorganic materials 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 229910045601 alloy Inorganic materials 0.000 claims description 3
- 239000000956 alloy Substances 0.000 claims description 3
- 238000005422 blasting Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000004576 sand Substances 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000011261 inert gas Substances 0.000 claims 2
- 239000011159 matrix material Substances 0.000 description 9
- 238000000280 densification Methods 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 230000003026 anti-oxygenic effect Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000009826 distribution Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001902 propagating effect Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000010189 synthetic method Methods 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005049 combustion synthesis Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000007499 fusion processing Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910000765 intermetallic Inorganic materials 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000007712 rapid solidification Methods 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
Landscapes
- Coating By Spraying Or Casting (AREA)
- Powder Metallurgy (AREA)
Abstract
Description
等离子体气体Ar | 30-50slpm | 粉末载气Ar | 1.5-5slpm |
等离子体气体H2 | 8-18slpm | 喷涂距离 | 100-350mm |
喷涂功率 | 30-58kW | 送粉速率 | 8-30g·min-1 |
喷涂压力 | 100-800mbar |
等离子体气体Ar45slpm | 粉末载气Ar3slpm |
等离子体气体H215slpm | 喷涂距离200mm |
喷涂功率36kW | 送粉速率8.0g·min-1 |
喷涂压力200mbar |
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410125984.6A CN103882422B (zh) | 2014-03-31 | 2014-03-31 | 一种制备二硅化钽块体材料的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410125984.6A CN103882422B (zh) | 2014-03-31 | 2014-03-31 | 一种制备二硅化钽块体材料的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103882422A CN103882422A (zh) | 2014-06-25 |
CN103882422B true CN103882422B (zh) | 2016-05-18 |
Family
ID=50951533
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410125984.6A Active CN103882422B (zh) | 2014-03-31 | 2014-03-31 | 一种制备二硅化钽块体材料的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103882422B (zh) |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101328064A (zh) * | 2007-06-22 | 2008-12-24 | 中国科学院金属研究所 | 一种原位反应热压合成TaC-TaSi2陶瓷复合材料及其制备方法 |
CN102041499A (zh) * | 2009-10-18 | 2011-05-04 | 中国科学院上海硅酸盐研究所 | 二硅化钼复合涂层及其制备方法 |
CN102703971A (zh) * | 2012-06-01 | 2012-10-03 | 西北工业大学 | 一种制备Si基二元共晶自生复合材料的方法 |
CN103132005A (zh) * | 2011-12-05 | 2013-06-05 | 湖南科技大学 | 二硅化钼基耐磨复合涂层及其制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8673400B2 (en) * | 2009-07-31 | 2014-03-18 | General Electric Company | Methods of improving surface roughness of an environmental barrier coating and components comprising environmental barrier coatings having improved surface roughness |
-
2014
- 2014-03-31 CN CN201410125984.6A patent/CN103882422B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101328064A (zh) * | 2007-06-22 | 2008-12-24 | 中国科学院金属研究所 | 一种原位反应热压合成TaC-TaSi2陶瓷复合材料及其制备方法 |
CN102041499A (zh) * | 2009-10-18 | 2011-05-04 | 中国科学院上海硅酸盐研究所 | 二硅化钼复合涂层及其制备方法 |
CN103132005A (zh) * | 2011-12-05 | 2013-06-05 | 湖南科技大学 | 二硅化钼基耐磨复合涂层及其制备方法 |
CN102703971A (zh) * | 2012-06-01 | 2012-10-03 | 西北工业大学 | 一种制备Si基二元共晶自生复合材料的方法 |
Non-Patent Citations (4)
Title |
---|
等离子喷涂工艺参数对二硅化钼涂层微观结构的影响;颜建辉 等;《材料热处理技术》;20120531;第41卷(第10期);第136-140页 * |
等离子喷涂成形技术制造薄壁零件;徐文冀 等;《材料保护》;20021130;第35卷(第11期);第46页右栏第1段 * |
粉末粒度对喷涂二硅化钼涂层微观结构的影响;颜建辉 等;《材料导报B:研究篇》;20120930;第26卷(第9期);第34-37页 * |
难熔金属硅化物TaSi2的研究进展;崔春娟 等;《材料热处理技术》;20100930;第39卷(第18期);第72-74页 * |
Also Published As
Publication number | Publication date |
---|---|
CN103882422A (zh) | 2014-06-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102554242B (zh) | 微细球形钛粉末的制造方法 | |
CN107309434B (zh) | 一种高纯致密球形钼粉的制备方法及应用 | |
CN108315628A (zh) | 基于(Ti,Me)CN-Co的涂层喷涂和3D打印金属陶瓷材料及其制备方法 | |
CN104475745B (zh) | 球形黄铜合金粉末的制造方法 | |
CN106001594A (zh) | 一种超粗球形钨粉的制备方法 | |
CN110407213B (zh) | 一种(Ta, Nb, Ti, V)C高熵碳化物纳米粉体及其制备方法 | |
CN104744047A (zh) | 一种反应烧结制备氮化硅坩埚的方法 | |
CN102010231A (zh) | 一种低密度炭/炭复合材料表面涂层的方法 | |
CN103882368A (zh) | 一种制备二硅化钽涂层的方法 | |
CN111778424A (zh) | 一种有效可控的具有多极孔结构的骨架的制备方法 | |
CN104788083A (zh) | 一种多晶硅还原炉用高抗热震性氧化铝陶瓷环及制备方法 | |
CN102259189A (zh) | 一种多孔阴极基底的制备方法 | |
CN102924087B (zh) | 一种立方氮化硼-碳化硅复相陶瓷材料的制备方法及其产品 | |
CN106747468B (zh) | 用于气雾化钛及钛合金粉末的导液管材料及其制备方法 | |
CN107602139A (zh) | 一种熔炼钛及钛合金用坩埚的材料及坩埚的制备方法 | |
CN104357785A (zh) | 一种快速制备等离子刻蚀机用高纯氧化钇涂层的方法 | |
CN103882422B (zh) | 一种制备二硅化钽块体材料的方法 | |
CN103789592A (zh) | 一种钨合金材料及其制备方法和在制备铝液过滤盘中的应用 | |
CN104072190B (zh) | 一种SiC多孔陶瓷的制备方法 | |
CN101239844A (zh) | 一种复合阻碳涂层材料及其在基体上制备复合阻碳涂层的方法 | |
CN105801141B (zh) | 澳斯麦特炉炉底用宏孔刚玉-尖晶石砖及其制备方法 | |
CN105130439A (zh) | 一种高强度碳化硅棚板及其制备方法 | |
CN101984115B (zh) | 一种制备银稀土氧化物电接触材料的方法 | |
CN106220188A (zh) | 一种窄粒度分布高纯氮化硅粉体的制备方法 | |
CN109161836B (zh) | 一种热喷涂多孔陶瓷涂层的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200426 Address after: 215400 No. 6 Liangfu Road, Taicang City, Suzhou City, Jiangsu Province Patentee after: SUZHOU Research Institute SHANGHAI INSTITUTE OF CERAMICS CHINESE ACADEMY OF SCIENCES Address before: 200050 No. 1295 Dingxi Road, Shanghai, Changning District Patentee before: SHANGHAI INSTITUTE OF CERAMICS, CHINESE ACADEMY OF SCIENCES |
|
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 215400 No.6 Liangfu Road, Taicang City, Suzhou City, Jiangsu Province Patentee after: Jiangsu Institute of advanced inorganic materials Address before: 215400 No.6 Liangfu Road, Taicang City, Suzhou City, Jiangsu Province Patentee before: SUZHOU Research Institute SHANGHAI INSTITUTE OF CERAMICS CHINESE ACADEMY OF SCIENCES |