CN103877418A - Traditional Chinese medicine granules for treating pterygium and detection method thereof - Google Patents
Traditional Chinese medicine granules for treating pterygium and detection method thereof Download PDFInfo
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- CN103877418A CN103877418A CN201410124140.XA CN201410124140A CN103877418A CN 103877418 A CN103877418 A CN 103877418A CN 201410124140 A CN201410124140 A CN 201410124140A CN 103877418 A CN103877418 A CN 103877418A
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Abstract
The invention discloses traditional Chinese medicine granules for treating pterygium. The traditional Chinese medicine granules are prepared from the following medicinal materials in parts by weight: 13-15 parts of raw rehmannia root, 8-10 parts of akebia stem, 5-6 parts of lophatherum, 8-10 parts of scutellaria root, 5-6 parts of coptis root, 8-10 parts of forsythia fruit, 13-15 parts of honeysuckle flower, 5-6 parts of cicada slough, 8-10 parts of tribulus terrestris, 8-10 parts of red peony root, 3-5 parts of licorice root, 5-6 parts of polygonum Chinese root, 0-5 parts of polystichum tsus-simense and 0-5 parts of mahonia leaf. The traditional Chinese medicine granules are detected by adopting a thin-layer chromatography identification method, and the detection method is simple, is reliable in detection result and is more beneficial to clinical diagnosis and treatment. Proved by clinical trials, through selecting appropriate medicinal materials and proportioning ratio thereof, the traditional Chinese medicine granules achieve a remarkable effect on treatment of pterygium, are safe and are free from toxic and side effects.
Description
Technical field
The present invention relates to a kind of Chinese medicine, be specifically related to one and be used for the treatment of pterygial Chinese medicinal granule and the method for inspection thereof.
Background technology
Pterygium is that a kind of because of the chronic oculopathy due to the degeneration of bulbar conjunctiva hypertrophy, clinical have the horizontal cornea of invading of a triangle sarcolemma as feature take corner of the eyes portion, and the traditional Chinese medical science is referred to as " pterygium ".Primary disease is more common in nasal side, also has in temporo side or both sides and sends out survivor, not only affects outward appearance, and husky puckery not easypro, and even bulbar conjunctiva polyp can hide pupil, affects one's power of vision.Primary disease is comparatively common with middle-aged and elderly people.The traditional Chinese medical science thinks that this cause of disease cardiopulmonary two are through wind heat heap soil or fertilizer over and around the roots Sheng; Or throw off restraint and have a liking for five pungent wine, taste accumulate long-pending damp and hot, on steam in order; Or heart deficiency of the kidney yin, hyperactivity of deficient fire, all can cause the venation stasis of blood stagnant, and obstruction of eye by blood becomes raw bulbar conjunctiva polyp.Still lack at present the effective medicine of generally recognized as safe for pterygial treatment.
Summary of the invention
The present invention aims to provide one and is used for the treatment of pterygial Chinese medicinal granule and the method for inspection thereof, by selecting suitable medical material and proportioning thereof, reach to contribute to the remarkable efficacy of patients with pterygium rehabilitation, and safe without toxic side effect.
In order to achieve the above object, the present invention is by the following technical solutions: one is used for the treatment of pterygial Chinese medicinal granule, is prepared from by the medical material of following weight proportion: 13～15 parts, the Radix Rehmanniae, 8～10 parts of Caulis Akebiaes, 5～6 parts of Herba Lophatheris, 8～10 parts of Radix Scutellariaes, 5～6 parts of Rhizoma Coptidis, 8～10 parts of Fructus Forsythiaes, 13～15 parts of Flos Lonicerae, 5～6 parts of Periostracum Cicadaes, 8～10 parts of Fructus Tribulis, 8～10 parts of Radix Paeoniae Rubra, 3～5 parts, Radix Glycyrrhizae, 5～6 parts of Radix Polygoni Chinensiss, 0～5 part of Polystichum tsussimense (Hook.) J. Sm., 0～5 part of Folium Mahoniae.
As preferably, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss.
As preferably, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Folium Mahoniaves.
As preferably, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm..
As preferably, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm., 5 parts of Folium Mahoniaves.
A kind of method of inspection that is used for the treatment of pterygial Chinese medicinal granule, comprise the steps: successively 1) get this product powder 0.5g, solubilizer 25～35ml, refluxes 25～35 minutes, filter, collect filtrate solvent evaporated, the residue 20ml that adds water dissolves, and is adding 15～25ml ethyl acetate to extract 2 times at every turn, merge extractive liquid,, evaporate to dryness ethyl acetate, residue adds methanol 1ml and dissolves, as need testing solution; 2) separately get control medicinal material 5g, the 45～55ml that adds water, boils 30 minutes, filter, and filtrate water bath method, residue solubilizer 25～35ml, is made in the same way of control medicinal material solution; 3) according to thin layer chromatography test, draw the each 5 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, take toluene-ethyl acetate-formic acid as developing solvent, launch, take out, dry, spray, with 10% ethanol solution of sulfuric acid, is heated to speckle colour developing at 105 ℃ clear, puts under ultra-violet lamp and inspects; 4) in test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, blueness, the green fluorescence speckle of aobvious same color.
The pharmacology analysis of the each Chinese medicinal ingredients of the present invention is as follows:
Fresh or the dried root that the Radix Rehmanniae [source] this product is scrophulariaceae rehmannia glutinosa plant.[nature and flavor] Radix Rehmanniae: sweet, cold.[return through] GUIXIN, liver, kidney channel.[function cures mainly] clearing away heat and cooling blood, yin nourishing, promotes the production of body fluid.For calentura crimson tongue excessive thirst, yin asthenia generating intrinsic heat, hectic fever due to YIN-deficiency consumptive fever, interior-heat is quenched one's thirst, and spits blood, and epistaxis, sends out speckle dermexanthesis.
Caulis Akebiae [source] is the woody stems of plants of Lardizabalaceae Caulis Akebiae or threeleaf akebia, Caulis Akebiae.[nature and flavor] hardship; Cold in nature.[return through] heart; Spleen; Kidney; Small intestinal; Urinary bladder channel.[function cures mainly] clearing away heat and promoting diuresis; Blood circulation and channel invigorating.Main red urine is red; Stranguria with turbid discharge; Edema; Irritable feverish sensation in the chest; Larynx larynx pain; Aphtha of the mouth and tongue; Rheumatic arthralgia; Galactostasis; Amenorrhea; Dysmenorrhea.
Herba Lophatheri [source] this product is the dry stem and leaf of grass Herba Lophatheri.[nature and flavor] are sweet, light, cold.[return through] GUIXIN, stomach, small intestine meridian.[function cures mainly] clearing heat and relieving fidgetness, diuresis.For calentura excessive thirst, hot urination drenches pain, aphtha of the mouth and tongue.
Radix Scutellariae [source] this product is the dry root of labiate Radix Scutellariae.[nature and flavor] hardship, cold.[return through] returns lung, gallbladder, spleen, large intestine, small intestine meridian.[function cures mainly] heat clearing and damp drying, eliminating fire and detoxication, hemostasis, antiabortive.For hygropyrexia, fever disease in summer vomiting and nausea uncomfortable in chest, damp and hot feeling of fullness, dysentery, jaundice, cough due to lung-heat, high hot excessive thirst, heat in blood is told nosebleed, carbuncle sore tumefacting virus, frequent fetal movement.
The dry rhizome of Rhizoma Coptidis [source] ranunculaceae plant Rhizoma Coptidis, Coptis deltoidea C.Y.Cheng et Hsiao or Coptis Teeta Wall.[function cures mainly] heat clearing and damp drying, eliminating fire and detoxication.For damp and hot feeling of fullness, vomiting acid regurgitation, dysentery, jaundice, unconsciousness due to high fever, hyperactivity of heart-fire, dysphoria and insomnia, heat in blood is told nosebleed, conjunctival congestion, toothache, quenches one's thirst, carbuncle furuncle; External treatment eczema, eczema, auditory meatus is suppurated.The kind clear part of the body cavity above the diaphragm housing the heart and lungs of Rhizoma Coptidis (processed with wine) is burning hot.For conjunctival congestion, aphtha.Prepared RHIZOMA COPTIDIS with rhizoma zingiberis recens juice clearing stomach stomach function regulating preventing or arresting vomiting.Tie mutually damp and hot middle resistance, feeling of fullness vomiting for cold and heat.Cornel Rhizoma Coptidis soothing liver-QI stomach function regulating preventing or arresting vomiting.For incoordination between the liver and stomach, vomiting acid regurgitation.
The dry fruit of Fructus Forsythiae [source] Oleaceae plants Fructus Forsythiae.[function cures mainly] heat-clearing and toxic substances removing, dispersing swelling and dissipating binds.For carbuncle, scrofula, acute mastitis, erysipelas, anemopyretic cold, epidemic febrile disease is from the beginning of, warm joining the army, high hot excessive thirst, coma is sent out speckle, pyretic stranguria urine retention.
Flos Lonicerae [source] this product is the dry flower of caprifoliaceae plant Radix Ophiopogonis or the flower that band is just opened.[nature and flavor] are sweet, cold.[return through] returns lung, the heart, stomach warp.[function cures mainly] heat-clearing and toxic substances removing, wind-heat dissipating.For carbuncle furuncle, sore throat, erysipelas, toxic-heat and blood stasis, anemopyretic cold, epidemic febrile disease heating.
Periostracum Cicadae [source] this product is the larva of cicada Cryptotympana atrata Fabr. exuviae shell while sprouting wings.[nature and flavor] are sweet, cold.[return through] returns lung, Liver Channel.[function cures mainly] the wind heat extraction that falls apart, sore-throat relieving, rash, nebula removing, spasmolytic.For anemopyretic cold, pharyngalgia, hoarseness, measles without adequate eruption, rubella pruritus, conjunctival congestion cataracta, convulsion with spasms, tetanus.
The fruit of Fructus Tribuli [source] zygophyllaceae plant Fructus Tribuli.[nature and flavor] bitter in the mouth; Pungent; Property is put down.[return through] liver; Lung; Kidney; Heart channel.[function cures mainly] suppressing the hyperactive liver; Resolving depression; Dispelling pathogenic wind for improving eyesight.Main headache; Dizzy; Distending pain in the chest and hypochondrium; Distending pain of the breast; Breast closes obstructed; Amenorrhea; Conjunctival congestion cataracta; Rubella pruritus; Vitiligo; Skin ulcer cellulitis; Scrofula.
The dry root of Radix Paeoniae Rubra [source] ranunculaceae plant Radix Paeoniae or river Radix Paeoniae Rubra.[nature and flavor] hardship, is slightly cold.[return through] returns Liver Channel.[function cures mainly] clearing away heat and cooling blood, eliminating stasis to stop pain.For maculae caused by violent heat pathogen, hematemesis and epistaxis, conjunctival congestion and swelling pain, hypochondriac pain due to stagnation of liverQI, amenorrhea dysmenorrhea, lump in the abdomen stomachache, injury from falling down, carbuncle skin infection.
The dry root of Radix Glycyrrhizae [source] glycyrrhizic legume.[nature and flavor] are sweet, flat.[return through] GUIXIN, lung, spleen, stomach warp.[function cures mainly] invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain, coordinating the actions of various ingredients in a prescription.
The root of Radix Polygoni Chinensis [source] polygonaceae plant Herb Polygoni Chinensis.[nature and flavor] are pungent; Sweet; Property is put down.[function cures mainly] invigorating spleen and kidney; Pancake liver-yang; Heat-clearing and toxic substances removing; Promoting blood circulation and detumescence.Main body void is weak; Hiccough and deaf; The vertigo; Leucorrhea; Acute mastitis; Lung abscess; Traumatic injury damages.
Polystichum tsussimense (Hook.) J. Sm. [source] is rhizome or the tender leaf of Dryopteridaceae plant Polystichum tsussimense (Hook.) J. Sm..Rhizome all can be gathered the whole year, to gather better autumn.After digging out, except defoliation, clean using fresh herb or dry; Tender leaf gathers spring, using fresh herb.[function cures mainly] heat-clearing and toxic substances removing; Cool the blood dissipate blood stasis.Main dysentery; Conjunctival congestion and swelling pain; Acute mastitis; Furuncle toxic swelling; Bleeding hemorrhoids; Burn and scald.
The leaf of Folium Mahoniae [source] holly plant Ilex cornuta Lindl..[nature and flavor] hardship; Cool.[return through] liver; Kidney channel.[function cures mainly] clearind deficient heat; Liver and kidney tonifying; Wind-damp dispelling.Main hectic fever due to deficiency of YIN; Cough spitting of blood; Have a dizzy spell; Soreness of the waist and knees; Rheumatic arthralgia; Vitiligo.
Below in conjunction with clinical experiment data declaration beneficial effect of the present invention:
Accept pterygial patient's 123 examples for medical treatment through clinical, take the oral agents of making according to embodiment 1, two doses of every days, use continuously 15-20 days.Therapeutic evaluation: cure: transference cure; Effective: symptom alleviates, but do not disappear completely; Invalid: symptom does not disappear, without obviously changing.
Therapeutic outcome: cure and effective totally 105 examples, effective percentage, up to 85.4%, is followed up a case by regular visits to after March again, all without recurrence.
The specific embodiment
In order to understand better and to implement the present invention, further illustrate the present invention below in conjunction with specific embodiment.
Embodiment 1
Take: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm., 5 parts of Folium Mahoniaves, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
The method of inspection: comprise the steps: successively 1) get this product powder 0.5g, solubilizer 25～35ml, reflux 25～35 minutes, filter, collect filtrate solvent evaporated, residue add water 20ml dissolve, adding 15～25ml ethyl acetate to extract 2 times, merge extractive liquid,, evaporate to dryness ethyl acetate at every turn, residue adds methanol 1ml and dissolves, as need testing solution; 2) separately get control medicinal material 5g, the 45～55ml that adds water, boils 30 minutes, filter, and filtrate water bath method, residue solubilizer 25～35ml, is made in the same way of control medicinal material solution; 3) according to thin layer chromatography test, draw the each 5 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, take toluene-ethyl acetate-formic acid as developing solvent, launch, take out, dry, spray, with 10% ethanol solution of sulfuric acid, is heated to speckle colour developing at 105 ℃ clear, puts under ultra-violet lamp and inspects; 4) in test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, blueness, the green fluorescence speckle of aobvious same color.
Be used for the treatment of pterygium.Oral, two doses of every days.
Embodiment 2
Take: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm., 5 parts of Folium Mahoniaves, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
Be used for the treatment of pterygium.Oral, two doses of every days.
The method of inspection is with embodiment 1.
Embodiment 3
Take: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm., 5 parts of Folium Mahoniaves, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
Be used for the treatment of pterygium.Oral, two doses of every days.
The method of inspection is with embodiment 1.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here cannot give exhaustive to all embodiments.Everyly belong to apparent variation or the still row in protection scope of the present invention of variation that technical scheme of the present invention extends out.
Claims (6)
1. one kind is used for the treatment of pterygial Chinese medicinal granule, it is characterized in that, be prepared from by the medical material of following weight proportion: 13～15 parts, the Radix Rehmanniae, 8～10 parts of Caulis Akebiaes, 5～6 parts of Herba Lophatheris, 8～10 parts of Radix Scutellariaes, 5～6 parts of Rhizoma Coptidis, 8～10 parts of Fructus Forsythiaes, 13～15 parts of Flos Lonicerae, 5～6 parts of Periostracum Cicadaes, 8～10 parts of Fructus Tribulis, 8～10 parts of Radix Paeoniae Rubra, 3～5 parts, Radix Glycyrrhizae, 5～6 parts of Radix Polygoni Chinensiss, 0～5 part of Polystichum tsussimense (Hook.) J. Sm., 0～5 part of Folium Mahoniae.
2. one according to claim 1 is used for the treatment of pterygial Chinese medicinal granule, it is characterized in that, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss.
3. one according to claim 1 is used for the treatment of pterygial Chinese medicinal granule, it is characterized in that, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Folium Mahoniaves.
4. one according to claim 1 is used for the treatment of pterygial Chinese medicinal granule, it is characterized in that, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm..
5. one according to claim 1 is used for the treatment of pterygial Chinese medicinal granule, it is characterized in that, be prepared from by the medical material of following weight proportion: 15 parts, the Radix Rehmanniae, 10 parts of Caulis Akebiaes, 6 parts of Herba Lophatheris, 10 parts of Radix Scutellariaes, 6 parts of Rhizoma Coptidis, 10 parts of Fructus Forsythiaes, 15 parts of Flos Lonicerae, 6 parts of Periostracum Cicadaes, 10 parts of Fructus Tribulis, 10 parts of Radix Paeoniae Rubra, 3 parts, Radix Glycyrrhizae, 6 parts of Radix Polygoni Chinensiss, 5 parts of Polystichum tsussimense (Hook.) J. Sm., 5 parts of Folium Mahoniaves.
6. a method of inspection that is used for the treatment of pterygial Chinese medicinal granule, is characterized in that, comprises the steps: successively 1) get this product powder 0.5g, solubilizer 25～35ml, reflux 25～35 minutes, filter, collect filtrate solvent evaporated, residue add water 20ml dissolve, adding 15～25ml ethyl acetate to extract 2 times, merge extractive liquid,, evaporate to dryness ethyl acetate at every turn, residue adds methanol 1ml and dissolves, as need testing solution; 2) separately get control medicinal material 5g, the 45～55ml that adds water, boils 30 minutes, filter, and filtrate water bath method, residue solubilizer 25～35ml, is made in the same way of control medicinal material solution; 3) according to thin layer chromatography test, draw the each 5 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, take toluene-ethyl acetate-formic acid as developing solvent, launch, take out, dry, spray, with 10% ethanol solution of sulfuric acid, is heated to speckle colour developing at 105 ℃ clear, puts under ultra-violet lamp and inspects; 4) in test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, blueness, the green fluorescence speckle of aobvious same color.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104207123A (en) * | 2014-08-21 | 2014-12-17 | 席安胜 | Dietary therapy formula for treating pterygium |
| CN105030892A (en) * | 2015-08-25 | 2015-11-11 | 何萍萍 | Traditional Chinese medicine for treating pterygium |
| CN106822788A (en) * | 2017-03-02 | 2017-06-13 | 董新芳 | It is a kind of to treat pteryium medicine and preparation method thereof |
-
2014
- 2014-03-28 CN CN201410124140.XA patent/CN103877418A/en active Pending
Non-Patent Citations (5)
| Title |
|---|
| 余杰为等: "中医眼科割烙术联合加味导赤散治疗翼状胬肉的临床疗效评价 ", 《江西中医药》 * |
| 余杰为等: "中医眼科割烙术联合加味导赤散治疗翼状胬肉的临床疗效评价", 《江西中医药》, vol. 42, no. 08, 31 August 2011 (2011-08-31), pages 35 - 37 * |
| 张颖: "中国中医科学院眼科医院眼科用药规律探讨", 《中国优秀硕士学位论文全文数据库 医药卫生科技辑 》 * |
| 沈丽珍: "加味导赤散联合球结膜转位术治疗复发性翼状胬肉 ", 《中国中医眼科杂志》 * |
| 沈丽珍: "加味导赤散联合球结膜转位术治疗复发性翼状胬肉", 《中国中医眼科杂志》, vol. 12, no. 02, 11 May 2002 (2002-05-11), pages 110 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104207123A (en) * | 2014-08-21 | 2014-12-17 | 席安胜 | Dietary therapy formula for treating pterygium |
| CN105030892A (en) * | 2015-08-25 | 2015-11-11 | 何萍萍 | Traditional Chinese medicine for treating pterygium |
| CN106822788A (en) * | 2017-03-02 | 2017-06-13 | 董新芳 | It is a kind of to treat pteryium medicine and preparation method thereof |
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Application publication date: 20140625 |