Summary of the invention
Technical problem to be solved by this invention is the manufacture method providing the colorful environmental protection heat insulating coatings of aqueousance artificial granite, and the coating made can reflective insulation effectively, high insulating effect, and heat-insulating property is stablized, corrosion-resistant, long service life, environment friendly and pollution-free.
For solving above-mentioned existing technical problem, the present invention adopts following scheme: the manufacture method of the colorful environmental protection heat insulating coatings of aqueousance artificial granite, comprises the following steps:
Step one: the preparation of the pre-solution of base glue: be that the rubber powder of 5-15 part joins in the deionized water of 85-95 part by mass fraction in No. 1 dispersion machine, first low speed again middling speed dispersion stirs 20-45 minute, make deionized water and rubber powder fully fused, phase melt into is transparent or semitransparent watery, without particle gel-free state in fused liquid, be prepared into the pre-solution for standby of base glue;
Step 2: the preparation of coating base slurry: add deionized water, the dispersion agent of 0.5-0.8 part, the wetting agent of 0.08-0.12 part, the defoamer of 0.25-0.5 part, the sterilant of 0.08-0.12 part, the film coalescence aid of 0.3-0.7 part, the propylene glycol of 0.8-1.2 part that mass fraction is 38-45 part in No. 2 dispersion machines successively, high speed dispersion stirs 2-5 minute; Add the titanium dioxide of 1.8-2.3 part, the ultrafine kaolin of 10-13 part, the aluminum oxide powder of 3.5-8 part, the heat-insulating powder of 2-5 part again, high speed dispersion stirs 5-8 minute; Add the PH conditioning agent of 0.1-0.3 part while middling speed dispersion stirring in the mode of airborne dust, then high speed dispersion stirs 13-18 minute, make surperficial shinny bubble-free, pH value is between 8-9; Be sequentially added into the Mierocrystalline cellulose of the linking agent of 0.3-0.7 part, 0.3-0.7 part, high speed dispersion stirs 3-8 minute; Middling speed dispersion adds the flexible silicon acrylic emulsion of 23-27 part, the defoamer of 0.13-0.18 part while stirring, and high speed dispersion stirs 8-12 minute, makes bubble-free without curdled milk phenomenon; Middling speed dispersion adds the negatively charged ion wetting agent of 0.1-0.3 part while stirring, high speed dispersion stirs 5-8 minute, adds the pre-solution of base glue be prepared in the step one of 12-15 part, and high speed dispersion stirs 8-12 minute, add the flow agent of 0.08-0.12 part again, high speed dispersion stirs 2-4 minute; Add the thickening material of 0.8-1.2 part, high speed dispersion stirs 2-4 minute, makes coating base slurry for subsequent use;
Step 3: the preparation of colorful bag paste colors grain: add the pre-solution of base glue be prepared in the step one of coloured slurry that mass fraction is 90-150 part, 90-100 part in No. 3 dispersion machines, high speed dispersion stirs 30-40 minute, then carry out granulation by 10-40 order mesh sheet, be prepared into colorful bag paste colors grain for subsequent use;
Step 4: the preparation of the colorful environmental protection heat insulating coatings of aqueousance artificial granite: add film coalescence aid, the sterilant of 0.1-0.8 part, the propylene glycol of 1-3 part, the defoamer of 0.2-0.6 part, the ceramic fine bead of 5-8 part that mass fraction is 1.3-1.8 part in No. 4 dispersion machines successively, after low speed dispersion stirs, 1-2 minute is stirred in the thickening material middling speed dispersion adding 0.8-1.2 part again, make bubble-free phenomenon, pH value is between 8-9; Then add be prepared in the step 3 of 15-20 part colorful bag paste colors grain, 95-105 part step 2 in be prepared into coating base slurry, 85-100 part step one in the pre-solution of base glue that is prepared into, 10-15 minute is stirred in low speed dispersion, is prepared into the colorful environmental protection heat insulating coatings of aqueousance artificial granite.
As preferably, in step 2 neutralization procedure four when pH value has slight deviation, adopt organic amino or ammoniacal liquor adjustment difference pH value.
As preferably, when dispersion is stirred in step one, step 2, step 3 and step 4, disperse machine knife oar along casing wall upset dispersion.Ensure that the uniformity coefficient of stirring and the accurate proportioning of each component, avoid the mixing ratio error that casing wall residual component causes each component.
As preferably, when in step one, step 2, step 3 and step 4, dispersion is stirred, low speed adopts 150-250 rev/min, and middling speed adopts 300-500 rev/min, adopts 800-1300 rev/min at a high speed.
Beneficial effect:
The present invention adopts technique scheme to provide the manufacture method of the colorful environmental protection heat insulating coatings of aqueousance artificial granite, the coating made can reflective insulation effectively, high insulating effect, and heat-insulating property is stablized, corrosion-resistant, long service life, environment friendly and pollution-free, and have employed coloured slurry, the proportioning of multiple color can be produced, add the aesthetics of coating.
Embodiment
Embodiment one:
The manufacture method of the colorful environmental protection heat insulating coatings of aqueousance artificial granite, comprises the following steps:
Step one: the preparation of the pre-solution of base glue: be that the rubber powder of 5 parts joins in the deionized water of 85 parts by mass fraction in No. 1 dispersion machine, first low speed again middling speed disperses stirring 20 minutes, make deionized water and rubber powder fully fused, phase melt into is transparent or semitransparent watery, without particle gel-free state in fused liquid, be prepared into the pre-solution for standby of base glue;
Step 2: the preparation of coating base slurry: adding mass fraction in No. 2 dispersion machines is successively the deionized water of 38 parts, the dispersion agent of 0.5 part, the wetting agent of 0.08 part, the defoamer of 0.25 part, the sterilant of 0.08 part, the film coalescence aid of 0.3 part, the propylene glycol of 0.8 part, and high speed dispersion stirs 2 minutes; Add the titanium dioxide of 1.8 parts, the ultrafine kaolin of 10 parts, the aluminum oxide powder of 3.5 parts, the heat-insulating powder of 2 parts again, high speed dispersion stirs 5 minutes; Add the PH conditioning agent of 0.1 part while middling speed dispersion stirring in the mode of airborne dust, then high speed dispersion stirs 13 minutes, makes surperficial shinny bubble-free, pH value is between 8-9; Be sequentially added into the linking agent of 0.3 part, the Mierocrystalline cellulose of 0.3 part, high speed dispersion stirs 3 minutes; Middling speed dispersion adds the flexible silicon acrylic emulsion of 23 parts, the defoamer of 0.13 part while stirring, and high speed dispersion stirs 8 minutes, makes bubble-free without curdled milk phenomenon; Middling speed dispersion adds the negatively charged ion wetting agent of 0.1 part while stirring, high speed dispersion stirs 5 minutes, and add the pre-solution of base glue be prepared in the step one of 12 parts, high speed dispersion stirs 8 minutes, then adds the flow agent of 0.08 part, and high speed dispersion stirs 2 minutes; Add the thickening material of 0.8 part, high speed dispersion stirs 2 minutes, makes coating base slurry for subsequent use;
Step 3: the preparation of colorful bag paste colors grain: adding mass fraction in No. 3 dispersion machines is the pre-solution of base glue be prepared in coloured slurry of 90 parts, the step one of 90 parts, high speed dispersion stirs 30 minutes, then carry out granulation by 10-40 order mesh sheet, be prepared into colorful bag paste colors grain for subsequent use;
Step 4: the preparation of the colorful environmental protection heat insulating coatings of aqueousance artificial granite: adding mass fraction in No. 4 dispersion machines is successively the film coalescence aid of 1.3 parts, the sterilant of 0.1 part, the propylene glycol of 1 part, the defoamer of 0.2 part, the ceramic fine bead of 5 parts, after low speed dispersion stirs, the thickening material middling speed adding 0.8 part again disperses stirring 1 minute, make bubble-free phenomenon, pH value is between 8-9; Then the pre-solution of base glue be prepared in the coating base slurry be prepared in the colorful bag paste colors grain be prepared in the step 3 of 15 parts, the step 2 of 95 parts, the step one of 85 parts is added, low speed dispersion stirring 10 minutes, is prepared into the colorful environmental protection heat insulating coatings of aqueousance artificial granite.
In step 2 neutralization procedure four when pH value has slight deviation, adopt organic amino or ammoniacal liquor adjustment difference pH value.When in step one, step 2, step 3 and step 4, dispersion is stirred, dispersion machine knife oar is along casing wall upset dispersion.When in step one, step 2, step 3 and step 4, dispersion is stirred, low speed adopts 150 revs/min, and middling speed adopts 300 revs/min, adopts 800 revs/min at a high speed.
Adopt cellulose paint in the present invention, substantially increase the rapid-curing cutback performance of whole thermal insulation coatings, ensure that the job schedule of brushing.Propylene glycol coordinates with dispersion agent, flow agent, thickening material, make thermal insulation coatings be easy to film forming in brushing, and film forming is thin, reduces use cost.Mierocrystalline cellulose and flexible silicon acrylic emulsion substantially increase the heat-proof quality of heat-insulating powder in whole thermal insulation coatings.Titanium dioxide and aluminum oxide powder mating reaction, both added the transparency of whole thermal insulation coatings, turn increases the stability of whole thermal insulation coatings.Ultrafine kaolin adds the erosion resistance of whole lagging material, with ceramic fine bead with the use of, substantially increase corrosion resistance nature.Have employed coloured slurry, the proportioning of multiple color can be produced, add the aesthetics of coating.
The colorful environmental protection heat insulating coatings of the aqueousance artificial granite adopting manufacture method of the present invention to make, can reflective insulation effectively, high insulating effect, and heat-insulating property is stablized, corrosion-resistant, and long service life is environment friendly and pollution-free.
Embodiment two:
The manufacture method of the colorful environmental protection heat insulating coatings of aqueousance artificial granite, comprises the following steps:
Step one: the preparation of the pre-solution of base glue: be that the rubber powder of 10 parts joins in the deionized water of 90 parts by mass fraction in No. 1 dispersion machine, first low speed again middling speed disperses stirring 30 minutes, make deionized water and rubber powder fully fused, phase melt into is transparent or semitransparent watery, without particle gel-free state in fused liquid, be prepared into the pre-solution for standby of base glue;
Step 2: the preparation of coating base slurry: adding mass fraction in No. 2 dispersion machines is successively the deionized water of 40 parts, the dispersion agent of 0.6 part, the wetting agent of 0.1 part, the defoamer of 0.4 part, the sterilant of 0.1 part, the film coalescence aid of 0.5 part, the propylene glycol of 1 part, and high speed dispersion stirs 4 minutes; Add the titanium dioxide of 2 parts, the ultrafine kaolin of 11 parts, the aluminum oxide powder of 6 parts, the heat-insulating powder of 4 parts again, high speed dispersion stirs 6 minutes; Add the PH conditioning agent of 0.2 part while middling speed dispersion stirring in the mode of airborne dust, then high speed dispersion stirs 15 minutes, makes surperficial shinny bubble-free, pH value is between 8-9; Be sequentially added into the linking agent of 0.5 part, the Mierocrystalline cellulose of 0.5 part, high speed dispersion stirs 6 minutes; Middling speed dispersion adds the flexible silicon acrylic emulsion of 25 parts, the defoamer of 0.15 part while stirring, and high speed dispersion stirs 10 minutes, makes bubble-free without curdled milk phenomenon; Middling speed dispersion adds the negatively charged ion wetting agent of 0.2 part while stirring, high speed dispersion stirs 6 minutes, and add the pre-solution of base glue be prepared in the step one of 14 parts, high speed dispersion stirs 10 minutes, then adds the flow agent of 0.1 part, and high speed dispersion stirs 3 minutes; Add the thickening material of 1 part, high speed dispersion stirs 3 minutes, makes coating base slurry for subsequent use;
Step 3: the preparation of colorful bag paste colors grain: adding mass fraction in No. 3 dispersion machines is the pre-solution of base glue be prepared in coloured slurry of 120 parts, the step one of 95 parts, high speed dispersion stirs 35 minutes, then carry out granulation by 10-40 order mesh sheet, be prepared into colorful bag paste colors grain for subsequent use;
Step 4: the preparation of the colorful environmental protection heat insulating coatings of aqueousance artificial granite: adding mass fraction in No. 4 dispersion machines is successively the film coalescence aid of 1.5 parts, the sterilant of 0.5 part, the propylene glycol of 2 parts, the defoamer of 0.4 part, the ceramic fine bead of 6 parts, after low speed dispersion stirs, the thickening material middling speed adding 1 part again disperses stirring 1.5 minutes, make bubble-free phenomenon, pH value is between 8-9; Then the pre-solution of base glue be prepared in the coating base slurry be prepared in the colorful bag paste colors grain be prepared in the step 3 of 18 parts, the step 2 of 100 parts, the step one of 95 parts is added, low speed dispersion stirring 13 minutes, is prepared into the colorful environmental protection heat insulating coatings of aqueousance artificial granite.
In step 2 neutralization procedure four when pH value has slight deviation, adopt organic amino or ammoniacal liquor adjustment difference pH value.When in step one, step 2, step 3 and step 4, dispersion is stirred, dispersion machine knife oar is along casing wall upset dispersion.When in step one, step 2, step 3 and step 4, dispersion is stirred, low speed adopts 200 revs/min, and middling speed adopts 400 revs/min, adopts 1000 revs/min at a high speed.
The preparation time of this embodiment is medium, medium by doses, and relative to embodiment one, energy consumption increases, but dispersed homogeneous degree is better, and work-ing life increases.
Embodiment three:
The manufacture method of the colorful environmental protection heat insulating coatings of aqueousance artificial granite, comprises the following steps:
Step one: the preparation of the pre-solution of base glue: be that the rubber powder of 15 parts joins in the deionized water of 95 parts by mass fraction in No. 1 dispersion machine, first low speed again middling speed disperses stirring 45 minutes, make deionized water and rubber powder fully fused, phase melt into is transparent or semitransparent watery, without particle gel-free state in fused liquid, be prepared into the pre-solution for standby of base glue;
Step 2: the preparation of coating base slurry: adding mass fraction in No. 2 dispersion machines is successively the deionized water of 45 parts, the dispersion agent of 0.8 part, the wetting agent of 0.12 part, the defoamer of 0.5 part, the sterilant of 0.12 part, the film coalescence aid of 0.7 part, the propylene glycol of 1.2 parts, and high speed dispersion stirs 5 minutes; Add the titanium dioxide of 2.3 parts, the ultrafine kaolin of 13 parts, the aluminum oxide powder of 8 parts, the heat-insulating powder of 5 parts again, high speed dispersion stirs 8 minutes; Add the PH conditioning agent of 0.3 part while middling speed dispersion stirring in the mode of airborne dust, then high speed dispersion stirs 18 minutes, makes surperficial shinny bubble-free, pH value is between 8-9; Be sequentially added into the linking agent of 0.7 part, the Mierocrystalline cellulose of 0.7 part, high speed dispersion stirs 8 minutes; Middling speed dispersion adds the flexible silicon acrylic emulsion of 27 parts, the defoamer of 0.18 part while stirring, and high speed dispersion stirs 12 minutes, makes bubble-free without curdled milk phenomenon; Middling speed dispersion adds the negatively charged ion wetting agent of 0.3 part while stirring, high speed dispersion stirs 8 minutes, and add the pre-solution of base glue be prepared in the step one of 15 parts, high speed dispersion stirs 12 minutes, then adds the flow agent of 0.12 part, and high speed dispersion stirs 4 minutes; Add the thickening material of 1.2 parts, high speed dispersion stirs 4 minutes, makes coating base slurry for subsequent use;
Step 3: the preparation of colorful bag paste colors grain: adding mass fraction in No. 3 dispersion machines is the pre-solution of base glue be prepared in coloured slurry of 150 parts, the step one of 100 parts, high speed dispersion stirs 40 minutes, then carry out granulation by 10-40 order mesh sheet, be prepared into colorful bag paste colors grain for subsequent use;
Step 4: the preparation of the colorful environmental protection heat insulating coatings of aqueousance artificial granite: adding mass fraction in No. 4 dispersion machines is successively the film coalescence aid of 1.8 parts, the sterilant of 0.8 part, the propylene glycol of 3 parts, the defoamer of 0.6 part, the ceramic fine bead of 8 parts, after low speed dispersion stirs, the thickening material middling speed adding 1.2 parts again disperses stirring 2 minutes, make bubble-free phenomenon, pH value is between 8-9; Then the pre-solution of base glue be prepared in the coating base slurry be prepared in the colorful bag paste colors grain be prepared in the step 3 of 20 parts, the step 2 of 105 parts, the step one of 100 parts is added, low speed dispersion stirring 15 minutes, is prepared into the colorful environmental protection heat insulating coatings of aqueousance artificial granite.
In step 2 neutralization procedure four when pH value has slight deviation, adopt organic amino or ammoniacal liquor adjustment difference pH value.When in step one, step 2, step 3 and step 4, dispersion is stirred, dispersion machine knife oar is along casing wall upset dispersion.When in step one, step 2, step 3 and step 4, dispersion is stirred, low speed adopts 250 revs/min, and middling speed adopts 500 revs/min, adopts 1300 revs/min at a high speed.
The preparation time of this embodiment is long, and consumption is large, and relative to embodiment one and embodiment two, the dispersed homogeneous degree of each moiety is best, and work-ing life is the longest, but energy consumption is also maximum, and cost is higher.
Specific embodiment described herein is only to the explanation for example of the present invention's spirit.Those skilled in the art can make various amendment or supplement or adopt similar mode to substitute to described specific embodiment, but can't depart from spirit of the present invention or surmount the scope that appended claims defines.