CN103725394B - 一种稳定乳液型切削液及其制备方法 - Google Patents
一种稳定乳液型切削液及其制备方法 Download PDFInfo
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Abstract
一种稳定乳液型切削液，由下列重量份的原料制成：环氧大豆油12-15、聚乙二醇单甲醚10-12、铝酸酯偶联剂DL-411？2-3、双十四碳醇酯3-4、醋酸丁酯4-6、聚烷撑二醇10-12、十二烷基苯磺酸钠2-3、硼酸1-2、助剂6-8、水200。本发明切削液通过使用环氧大豆油等有机脂类，在溶剂和表面活性剂的作用下，形成的乳液不仅润滑剂性好，而且稳定，不易浑浊沉降，还具有优异的冷却性、清洗性、消泡性和防锈性能，本发明切削液适用于多种金属材料的切削及磨削加工工艺，使用寿命长，可实现零排放。
Description
技术领域
本发明涉及金属切削加工润滑领域，尤其涉及一种稳定乳液型切削液及其制备方法。
背景技术
切削液应具备良好的冷却性能、润滑性能、防锈性能、除油清洗功能、防腐功能、易稀释特点。目前切削液可分为两类，油溶性切削液和水溶性切削液。一般油溶性切削液润滑性能好，但冷却性能差，且含有大量有机物，污染环境。一些水溶性切削液虽然冷却性能好，又存在润滑性和防锈效果差的问题，因此研发兼具润滑性、冷却性、防锈性、易清洗、无毒、无味、对人体无侵蚀、对设备不腐蚀、对环境不污染的切削液就显得很重要。
发明内容
本发明的目的在于提供一种稳定乳液型切削液及其制备方法,该切削液具有稳定性好、润滑性好、清洗性好的特点。
本发明的技术方案如下：
一种稳定乳液型切削液，其特征在于由下列重量份的原料制成：环氧大豆油12-15、聚乙二醇单甲醚10-12、铝酸酯偶联剂DL-4112-3、双十四碳醇酯3-4、醋酸丁酯4-6、聚烷撑二醇10-12、十二烷基苯磺酸钠2-3、硼酸1-2、助剂6-8、水200；所述的助剂由下列重量份的原料制成：氧化铵1-2、吗啉2-3、纳米氮化铝0.1-0.2、硅酸钠1-2、硼砂2-3、2-氨基-2-甲基-1-丙醇1-2、聚氧乙烯山梨糖醇酐单油酸酯2-3、桃胶2-3、过硫酸铵1-2、水20-24；制备方法是将过硫酸铵溶于水后，再加入其它剩余物料，搅拌10-15分钟，加热至70-80℃，搅拌反应1-2小时，即得。
所述稳定乳液型切削液的制备方法，其特征在于包括以下步骤：将水、聚烷撑二醇、十二烷基苯磺酸钠混合，加热至40-50℃；在3000-4000转/分搅拌下，加入环氧大豆油、聚乙二醇单甲醚、铝酸酯偶联剂DL-411、双十四碳醇酯、醋酸丁酯、助剂，继续加热到70-80℃，继续搅拌10-15分钟；加入其他剩余成分，继续搅拌15-25分钟，即得。
本发明的有益效果
本发明切削液通过使用环氧大豆油等有机脂类，在溶剂和表面活性剂的作用下，形成的乳液不仅润滑剂性好，而且稳定，不易浑浊沉降，还具有优异的冷却性、清洗性、消泡性和防锈性能，本发明切削液适用于多种金属材料的切削及磨削加工工艺，使用寿命长，可实现零排放。
具体实施方式
一种稳定乳液型切削液，由下列重量份（公斤）的原料制成：环氧大豆油13、聚乙二醇单甲醚11、铝酸酯偶联剂DL-4112.5、双十四碳醇酯3.5、醋酸丁酯5、聚烷撑二醇11、十二烷基苯磺酸钠2.5、硼酸1.5、助剂7、水200；所述的助剂由下列重量份（公斤）的原料制成：氧化铵1、吗啉2、纳米氮化铝0.1、硅酸钠1、硼砂2、2-氨基-2-甲基-1-丙醇2、聚氧乙烯山梨糖醇酐单油酸酯3、桃胶2、过硫酸铵1、水20；制备方法是将过硫酸铵溶于水后，再加入其它剩余物料，搅拌10-15分钟，加热至70-80℃，搅拌反应1-2小时，即得。
所述稳定乳液型切削液的制备方法，包括以下步骤：将水、聚烷撑二醇、十二烷基苯磺酸钠混合，加热至45℃；在3500转/分搅拌下，加入环氧大豆油、聚乙二醇单甲醚、铝酸酯偶联剂DL-411、双十四碳醇酯、醋酸丁酯、助剂，继续加热到75℃，继续搅拌13分钟；加入其他剩余成分，继续搅拌20分钟，即得。
该实施例得到的稳定乳液型切削液试验数据如下：
Claims (1)
1.一种稳定乳液型切削液，其特征在于由下列重量份的原料制成：环氧大豆油12-15、聚乙二醇单甲醚10-12、铝酸酯偶联剂DL-4112-3、双十四碳醇酯3-4、醋酸丁酯4-6、聚烷撑二醇10-12、十二烷基苯磺酸钠2-3、硼酸1-2、助剂6-8、水200；所述的助剂由下列重量份的原料制成：氧化胺1-2、吗啉2-3、纳米氮化铝0.1-0.2、硅酸钠1-2、硼砂2-3、2-氨基-2-甲基-1-丙醇1-2、聚氧乙烯山梨糖醇酐单油酸酯2-3、桃胶2-3、过硫酸铵1-2、水20-24；制备方法是将过硫酸铵溶于水后，再加入其它剩余物料，搅拌10-15分钟，加热至70-80℃，搅拌反应1-2小时，即得；
所述稳定乳液型切削液的制备方法包括以下步骤：将水、聚烷撑二醇、十二烷基苯磺酸钠混合，加热至40-50℃；在3000-4000转/分搅拌下，加入环氧大豆油、聚乙二醇单甲醚、铝酸酯偶联剂DL-411、双十四碳醇酯、醋酸丁酯、助剂，继续加热到70-80℃，继续搅拌10-15分钟；加入其他剩余成分，继续搅拌15-25分钟，即得。
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1174489A1 (en) * | 2000-07-21 | 2002-01-23 | Nueva Fl Ibérica, S.A. | Process for preparing cutting lubricant fluids |
| CN101240217A (zh) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | 微乳型金属切削液组合物 |
| CN102618374A (zh) * | 2012-03-07 | 2012-08-01 | 东莞市安美润滑科技有限公司 | 硬脆性晶体材料切片加工的水基切削液及其制备方法 |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1174489A1 (en) * | 2000-07-21 | 2002-01-23 | Nueva Fl Ibérica, S.A. | Process for preparing cutting lubricant fluids |
| CN101240217A (zh) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | 微乳型金属切削液组合物 |
| CN102618374A (zh) * | 2012-03-07 | 2012-08-01 | 东莞市安美润滑科技有限公司 | 硬脆性晶体材料切片加工的水基切削液及其制备方法 |
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