CN103708976A - Composite medicinal fertilizer and preparation method thereof - Google Patents

Composite medicinal fertilizer and preparation method thereof Download PDF

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Publication number
CN103708976A
CN103708976A CN201310682100.2A CN201310682100A CN103708976A CN 103708976 A CN103708976 A CN 103708976A CN 201310682100 A CN201310682100 A CN 201310682100A CN 103708976 A CN103708976 A CN 103708976A
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China
Prior art keywords
fertilizer
percentage composition
quality percentage
magnesium slag
parts
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CN201310682100.2A
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Inventor
孟凡伍
李世忠
刘振红
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Jinzhou Shuofeng Pesticide Group Co Ltd
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Jinzhou Shuofeng Pesticide Group Co Ltd
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Abstract

The invention discloses a composite medicinal fertilizer and a preparation method thereof. The composite medicinal fertilizer consists of the following components in percentage by weight: 30-40 percent of a nitrogen-phosphorus-potassium mixed fertilizer, 22-30 percent of imidacloprid, 0.1-1 percent of difenoconazole, 0.1-0.5 percent of agritol, 5-8 percent of a wrapping agent and 24-36 percent of boric magnesium slag. The preparation method comprises the steps of crushing the boric magnesium slag to 80-100 meshes to obtain boric magnesium slag particles, adding the agritol into the boric magnesium slag particles, uniformly mixing the agritol and the boric magnesium slag particles, then mixing the mixture with nitrogen-phosphorus-potassium mixed fertilizer particles to obtain boric magnesium slag and nitrogen-phosphorus-potassium mixed fertilizer mixed particles, adding the imidacloprid and the difenoconazole into water for uniform stirring, uniformly spraying the imidacloprid and difenoconazole mixed aqueous solution on the surfaces of the boric magnesium slag and nitrogen-phosphorus-potassium mixed fertilizer mixed particles, wrapping the particles through the wrapping agent, and performing screening to obtain the composite medicinal fertilizer. The composite medicinal fertilizer has the advantages that the fertilizer has rich nutritional components; in a production process, high-temperature drying is not needed, so that pesticide components can be effectively guaranteed; the composite medicinal fertilizer is safe, environment-friendly and suitable for industrial production.

Description

A kind of composite fertilizer with pesticide and preparation method thereof
Technical field
The present invention relates to a kind of composite fertilizer with pesticide and preparation method thereof.
Background technology
In agriculture production, agricultural chemicals and fertilizer are guaranteeing on crop yield, to play requisite effect.The biology of agricultural chemicals energy kill pests, fungi and other growth that harms the crops; Fertilizer can provide plant necessary nutrition, and improves the soil property of soil.Along with scientific and technological development, not only had to kill and pressed down diseases and pests of agronomic crop but also can become main research direction for farm crop provide the functional composite fertilizer with pesticide of nutrition.
At present, composite fertilizer with pesticide is that fertilizer is major ingredient, adopts coating method that agricultural chemicals is wrapped in to fertiliser granulates appearance.The major ingredient adopting is generally nitrogen, phosphorus, potassium macroelement fertilizer, ignored the use of trace element fertilizer, and for farm crop, no matter macroelement or trace element are of equal importance, when trace element is not enough, not only affect the output of farm crop, and lower the quality of farm crop, even farm crop also there will be pathology.Therefore, peasant when using medicine fertilizer, need add trace element fertilizer to farm crop according to the needs of farm crop, and manual stirring is time-consuming, and, easily cause secondary pollution; And farm crop are few to micro-demand, during mixing, be difficult for stirring, easily cause farmland micro-fertile local excessive or not enough, affect output.
CN101906001A discloses " the fertile preparation method of a kind of medicine fertilizer and application thereof, particle formulation medicine fertilizer and powder-type medicine ", and the method is by solvent, Avrmectin, Volaton and/or Chlorpyrifos 94, tensio-active agent mixed dissolution, is mixed with mother liquor; By mother liquor mix with macroelement fertilizer, trace element fertilizer, sorbent material, carrier, granulation, obtain particle formulation medicine fertile.This preparation method's technique is simple, and condition is easily controlled, and is suitable for suitability for industrialized production.Its shortcoming is: adopt the method for mixing granulation, the slow release effect of agricultural chemicals is undesirable, and in granulation process, needs to dry, and easily causes a large amount of farm chemical ingredients to vapor away, and affects the fertile insecticidal effect of medicine, to environment, affects direct labor healthy.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of composite fertilizer with pesticide and preparation method thereof, and fertilizer nutritive ingredient is abundant, in production process without hyperthermia drying, can effectively guarantee farm chemical ingredients, safety and environmental protection, is applicable to suitability for industrialized production.
Technical solution of the present invention is:
A composite fertilizer with pesticide, percentage composition meter is comprised of following composition by weight:
Nitrogen-phosphorus-potassium compound fertilizer 30%~40%;
Provado 22%~30%;
Difenoconazole 0.1%~1%;
Bacillus thuringiensis 0.1%~0.5%;
Coating agent 5%~8%;
Boron magnesium slag 24%~36%.
Described coating agent is that mean particle size is 100 order~150 object gypsum.
Meter by weight, in described nitrogen-phosphorus-potassium compound fertilizer, nitrogenous fertilizer is that 15 parts~22 parts, phosphate fertilizer are 10 parts~12 parts of 5 parts~8 parts, potash fertilizer.
In described boron magnesium slag, the quality percentage composition of boron trioxide is 3.0%~3.2%, magnesian quality percentage composition is 22%~24%, the quality percentage composition of calcium oxide is 4.0%~4.2%, the quality percentage composition of silicon-dioxide is 9.2%~9.5%, the quality percentage composition of ferric oxide is 1.8%~2.1%, the quality percentage composition of sulphur is 0.2%~0.3%, and the quality percentage composition of cupric oxide is 0.3%~0.5%, and the quality percentage composition of molybdenum is 0.3%~0.4%.
A preparation method for composite fertilizer with pesticide, its concrete steps are:
Boron magnesium slag powders is broken to 80 order~100 orders and obtains boron magnesium slag particle, percentage composition meter by weight, after 0.1%~0.5% Bacillus thuringiensis is joined and is mixed in 24%~36% boron magnesium slag particle, mix with 30%~40% nitrogen-phosphorus-potassium compound fertilizer particle, obtain boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, 22%~30% Provado and 0.1%~1% difenoconazole are added to the water and are stirred, evenly be sprayed at the surface of boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, and carry out coating with 5%~8% coating agent, sieve, make composite fertilizer with pesticide particle.
Meter by weight, in described nitrogen-phosphorus-potassium compound fertilizer, nitrogenous fertilizer is that 15 parts~22 parts, phosphate fertilizer are 10 parts~12 parts of 5 parts~8 parts, potash fertilizer.
Described coating agent is that mean particle size is 100 order~150 object gypsum.
In described boron magnesium slag, the quality percentage composition of boron trioxide is 3.0%~3.2%, magnesian quality percentage composition is 22%~24%, the quality percentage composition of calcium oxide is 4.0%~4.2%, the quality percentage composition of silicon-dioxide is 9.2%~9.5%, the quality percentage composition of ferric oxide is 1.8%~2.1%, the quality percentage composition of sulphur is 0.2%~0.3%, and the quality percentage composition of cupric oxide is 0.3%~0.5%, and the quality percentage composition of molybdenum is 0.3%~0.4%.
The effective content of described Bacillus thuringiensis is 8000IU/ milligram~16000IU/ milligram.
Beneficial effect of the present invention:
1, in boron magnesium slag, contain the required trace element of abundant plant-growth, for fertile production of medicine, turn waste into wealth, reduced the be rivals in a contest pollution of environment of slagheap, boron magnesium slag being mixed to the medicine fertilizer making with nitrogen-phosphorus-potassium compound fertilizer and agricultural chemicals can provide plant-growth required nutrient, single-dose application can reach requirement, alleviated peasant's labour intensity, saving of work and time, has avoided Multiple Pesticides and fertilizer to puddle the secondary pollution causing.
2, Provado and difenoconazole compound use, control wheat aphid and smut are had a significant effect, add Tribactur all to there is specific strong cytotoxicity to above and below ground insects such as the arthropodss such as lepidopteran, Coleoptera, Diptera, Hymenoptera, Homoptera and Plant nematode, acarians, thereby make more wide spectrum of insecticidal effect, the dual function with desinsection and sterilization, and safe and harmless to nontarget organism people and animals etc.
3, boron magnesium slag is acid, with soil neutralization, can play the effect of Porous soil, boron magnesium slag has space vesicular structure, and specific surface area is large, Bacillus thuringiensis and Provado and difenoconazole are had to absorption and slow releasing function, and the long action time to farm crop, is more easily absorbed by plants nutrient, fertilizer efficiency is more lasting, and boron magnesium slag also has adsorption to oxygen and moisture content, thereby there is water conservation effect.
4, technique is simple, in production process without hyperthermia drying, can effectively guarantee farm chemical ingredients, safety and environmental protection, is applicable to suitability for industrialized production.
Embodiment
Embodiment 1
By following weight, take raw material: the mean particle size that the Bacillus thuringiensis of 15 kilograms of nitrogenous fertilizer particles (main component is urea), 5 kilograms of phosphate fertilizer particles (main component is diammonium phosphate), 10 kilograms of potassium fertilizer particles (main component is potassium sulfate), 30 kilograms of Provados, 0.1 kilogram of difenoconazole, 8000IU/ milligram is 0.1 kilogram, 8 kilograms is the boron magnesium slag (form and content as table 1) of 150 object gypsum and 31.8 kilograms;
Table 1
Figure 2013106821002100002DEST_PATH_IMAGE001
During production, boron magnesium slag powders is broken to 100 orders and obtains boron magnesium slag particle, after the Bacillus thuringiensis of 0.1 kilogram is joined and is mixed in 31.8 kilograms of boron magnesium slag particles, with 15 kilograms of nitrogenous fertilizer particles, the nitrogen-phosphorus-potassium compound fertilizer of 5 kilograms of phosphate fertilizer particles and 10 kilograms of potassium fertilizer particles mixes, obtain boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, 30 kilograms of Provados and 0.1 kilogram of difenoconazole are added to the water and are stirred, evenly be sprayed at the surface of boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, then by mean particle size, be that 150 object gypsum carry out coating, the consumption of gypsum is 8 kilograms, sieve, make composite fertilizer with pesticide particle.
During sowing wheat, use the composite fertilizer with pesticide particle of the embodiment of the present invention 1, amount of application is 30 kgs/acre (without topdressing), broadcasts latter 20 days, compares with using common NPK fertilizers, and the prevention effect of wheat aphid is 93.23%; And the prevention effect of smut is 89.2%, during harvesting wheat, than using common NPK fertilizers (topdressing 3 times) farmland volume increase 18.6%.
Embodiment 2
By following weight, take raw material: the mean particle size that the Bacillus thuringiensis of 20 kilograms of nitrogenous fertilizer particles (main component is urea), 8 kilograms of phosphate fertilizer particles (main component is diammonium phosphate), 12 kilograms of potassium fertilizer particles (main component is potassium sulfate), 22 kilograms of Provados, 1 kilogram of difenoconazole, 16000IU/ milligram is 0.5 kilogram, 7 kilograms is the boron magnesium slag (form and content as table 2) of 100 object gypsum and 29.5 kilograms;
Table 2
Figure 478604DEST_PATH_IMAGE002
During production, boron magnesium slag powders is broken to 80 orders and obtains boron magnesium slag particle, after the Bacillus thuringiensis of 0.5 kilogram is joined and is mixed in 29.5 kilograms of boron magnesium slag particles, with 20 kilograms of nitrogenous fertilizer particles, the nitrogen-phosphorus-potassium compound fertilizer of 8 kilograms of phosphate fertilizer particles and 12 kilograms of potassium fertilizer particles is mixed to get boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, 22 kilograms of Provados and 1 kilogram of difenoconazole are added to the water and are stirred, evenly be sprayed at the surface of boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, then by mean particle size, be that 100 object gypsum carry out coating, the consumption of gypsum is 7 kilograms, sieve, make composite fertilizer with pesticide particle.
During sowing wheat, use the composite fertilizer with pesticide particle of the embodiment of the present invention 2, amount of application is 30 kgs/acre (without topdressing), broadcasts latter 20 days, compares with using common NPK fertilizers, and the prevention effect of wheat aphid is 92.12%; And the prevention effect of smut is 87.6%, during harvesting wheat, than using common NPK fertilizers (topdressing 3 times) farmland volume increase 19%.
Embodiment 3
By following weight, take raw material: 22 kilograms of nitrogenous fertilizer particles (main component is urea), the mean particle size of 0.4 kilogram, 5.9 kilograms of Bacillus thuringiensiss of phosphate fertilizer particle (main component is diammonium phosphate), 10 kilograms of potassium fertilizer particles (main component is potassium sulfate), 29 kilograms of Provados, 0.8 kilogram of difenoconazole, 10000IU/ milligram of 7 kilograms are the boron magnesium slag (form and content as table 3) of 100 object gypsum and 24.9 kilograms;
Table 3
During production, boron magnesium slag powders is broken to 100 orders and obtains boron magnesium slag particle, after the Bacillus thuringiensis of 0.4 kilogram is joined and is mixed in 24.9 kilograms of boron magnesium slag particles, with 22 kilograms of nitrogenous fertilizer particles, the nitrogen-phosphorus-potassium compound fertilizer of 7 kilograms of phosphate fertilizer particles and 10 kilograms of potassium fertilizer particles is mixed to get boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, 29 kilograms of Provados and 0.8 kilogram of difenoconazole are added to the water and are stirred, evenly be sprayed at the surface of boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, then by mean particle size, be that 100 object gypsum carry out coating, the consumption of gypsum is 5.9 kilograms, sieve, make composite fertilizer with pesticide particle.
During sowing wheat, use the composite fertilizer with pesticide particle of the embodiment of the present invention 3, amount of application is 30 kgs/acre (without topdressing), broadcasts latter 20 days, compares with using common NPK fertilizers, and the prevention effect of wheat aphid is 90.71%; And the prevention effect of smut is 88.1%, during harvesting wheat, than using common NPK fertilizers (topdressing 3 times) farmland volume increase 18%.

Claims (10)

1. a composite fertilizer with pesticide, is characterized in that: percentage composition meter is comprised of following composition by weight:
Nitrogen-phosphorus-potassium compound fertilizer 30%~40%;
Provado 22%~30%;
Difenoconazole 0.1%~1%;
Bacillus thuringiensis 0.1%~0.5%;
Coating agent 5%~8%;
Boron magnesium slag 24%~36%.
2. composite fertilizer with pesticide according to claim 1, is characterized in that: described coating agent is that mean particle size is 100 order~150 object gypsum.
3. composite fertilizer with pesticide according to claim 1, is characterized in that: meter by weight, in described nitrogen-phosphorus-potassium compound fertilizer, nitrogenous fertilizer is that 15 parts~22 parts, phosphate fertilizer are 10 parts~12 parts of 5 parts~8 parts, potash fertilizer.
4. composite fertilizer with pesticide according to claim 1, it is characterized in that: in described boron magnesium slag, the quality percentage composition of boron trioxide is 3.0%~3.2%, magnesian quality percentage composition is 22%~24%, the quality percentage composition of calcium oxide is 4.0%~4.2%, the quality percentage composition of silicon-dioxide is 9.2%~9.5%, the quality percentage composition of ferric oxide is 1.8%~2.1%, the quality percentage composition of sulphur is 0.2%~0.3%, the quality percentage composition of cupric oxide is 0.3%~0.5%, and the quality percentage composition of molybdenum is 0.3%~0.4%.
5. composite fertilizer with pesticide according to claim 1, is characterized in that: the effective content of described Bacillus thuringiensis is 8000IU/ milligram~16000IU/ milligram.
6. a preparation method for composite fertilizer with pesticide, is characterized in that: concrete steps are as follows:
Boron magnesium slag powders is broken to 80 order~100 orders and obtains boron magnesium slag particle, percentage composition meter by weight, after 0.1%~0.5% Bacillus thuringiensis is joined and is mixed in 24%~36% boron magnesium slag particle, mix with 30%~40% nitrogen-phosphorus-potassium compound fertilizer particle, obtain boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, 22%~30% Provado and 0.1%~1% difenoconazole are added to the water and are stirred, evenly be sprayed at the surface of boron magnesium slag and nitrogen-phosphorus-potassium compound fertilizer composite grain, and carry out coating with 5%~8% coating agent, sieve, make composite fertilizer with pesticide particle.
7. the preparation method of composite fertilizer with pesticide according to claim 6, is characterized in that: meter by weight, in described nitrogen-phosphorus-potassium compound fertilizer, nitrogenous fertilizer is that 15 parts~22 parts, phosphate fertilizer are 10 parts~12 parts of 5 parts~8 parts, potash fertilizer.
8. the preparation method of composite fertilizer with pesticide according to claim 6, is characterized in that: described coating agent is that mean particle size is 100 order~150 object gypsum.
9. the preparation method of composite fertilizer with pesticide according to claim 6, it is characterized in that: in described boron magnesium slag, the quality percentage composition of boron trioxide is 3.0%~3.2%, magnesian quality percentage composition is 22%~24%, the quality percentage composition of calcium oxide is 4.0%~4.2%, the quality percentage composition of silicon-dioxide is 9.2%~9.5%, the quality percentage composition of ferric oxide is 1.8%~2.1%, the quality percentage composition of sulphur is 0.2%~0.3%, the quality percentage composition of cupric oxide is 0.3%~0.5%, and the quality percentage composition of molybdenum is 0.3%~0.4%.
10. the preparation method of composite fertilizer with pesticide according to claim 6, is characterized in that: the effective content of described Bacillus thuringiensis is 8000IU/ milligram~16000IU/ milligram.
CN201310682100.2A 2013-12-16 2013-12-16 Composite medicinal fertilizer and preparation method thereof Pending CN103708976A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040007034A (en) * 2002-07-16 2004-01-24 권종근 Germicidal Fertillizing Aqua-solution Comprising Colloidal Silver and Minor Species
CN102334500A (en) * 2011-10-31 2012-02-01 联保作物科技有限公司 Insect-killing and disease-preventing suspension seed coating formulation
CN102617229A (en) * 2012-03-22 2012-08-01 锦州硕丰农药集团有限公司 Application of stassfurtite waste residues and boric sludge in pesticide granule
CN102910981A (en) * 2012-10-16 2013-02-06 南通派斯第农药化工股份有限公司 8,000 UI/mg bacillus thuringiensis SC and preparation method thereof
CN103288557A (en) * 2013-05-29 2013-09-11 张仕耀 Mixture of secondary element fertilizer and pesticide
CN103319278A (en) * 2013-05-23 2013-09-25 锦州硕丰农药集团有限公司 Multifunctional pesticide fertilizer and production method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040007034A (en) * 2002-07-16 2004-01-24 권종근 Germicidal Fertillizing Aqua-solution Comprising Colloidal Silver and Minor Species
CN102334500A (en) * 2011-10-31 2012-02-01 联保作物科技有限公司 Insect-killing and disease-preventing suspension seed coating formulation
CN102617229A (en) * 2012-03-22 2012-08-01 锦州硕丰农药集团有限公司 Application of stassfurtite waste residues and boric sludge in pesticide granule
CN102910981A (en) * 2012-10-16 2013-02-06 南通派斯第农药化工股份有限公司 8,000 UI/mg bacillus thuringiensis SC and preparation method thereof
CN103319278A (en) * 2013-05-23 2013-09-25 锦州硕丰农药集团有限公司 Multifunctional pesticide fertilizer and production method thereof
CN103288557A (en) * 2013-05-29 2013-09-11 张仕耀 Mixture of secondary element fertilizer and pesticide

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Application publication date: 20140409