CN103613984B - A kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof - Google Patents
A kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof Download PDFInfo
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- CN103613984B CN103613984B CN201310579649.9A CN201310579649A CN103613984B CN 103613984 B CN103613984 B CN 103613984B CN 201310579649 A CN201310579649 A CN 201310579649A CN 103613984 B CN103613984 B CN 103613984B
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- cleaning
- acid
- cleaning agent
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- auxiliary agent
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 20
- 238000004140 cleaning Methods 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 18
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 12
- PMZURENOXWZQFD-UHFFFAOYSA-L sodium sulphate Substances [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 7
- AOKRXIIIYJGNNU-UHFFFAOYSA-N 3-methylcyclopentan-1-one Chemical compound CC1CCC(=O)C1 AOKRXIIIYJGNNU-UHFFFAOYSA-N 0.000 claims abstract description 6
- OTLNPYWUJOZPPA-UHFFFAOYSA-N 4-nitrobenzoic acid Chemical compound OC(=O)C1=CC=C([N+]([O-])=O)C=C1 OTLNPYWUJOZPPA-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001293 FEMA 3089 Substances 0.000 claims abstract description 6
- 229920000877 Melamine resin Polymers 0.000 claims abstract description 6
- 229910021538 borax Inorganic materials 0.000 claims abstract description 6
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims abstract description 6
- 229910000397 disodium phosphate Inorganic materials 0.000 claims abstract description 6
- 235000019800 disodium phosphate Nutrition 0.000 claims abstract description 6
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 6
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 6
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 6
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 7
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004359 castor oil Substances 0.000 claims description 6
- 235000019438 castor oil Nutrition 0.000 claims description 6
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000008878 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 6
- 229910000077 silane Inorganic materials 0.000 claims description 6
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 230000003078 antioxidant effect Effects 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 3
- 235000013824 polyphenols Nutrition 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 208000033999 Device damage Diseases 0.000 abstract description 2
- 239000012530 fluid Substances 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 description 8
- 239000002904 solvent Substances 0.000 description 5
- 239000003502 gasoline Substances 0.000 description 4
- 239000003350 kerosene Substances 0.000 description 4
- 238000007639 printing Methods 0.000 description 4
- 230000006378 damage Effects 0.000 description 3
- VGTPCRGMBIAPIM-UHFFFAOYSA-M sodium thiocyanate Chemical compound [Na+].[S-]C#N VGTPCRGMBIAPIM-UHFFFAOYSA-M 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- OUHCZCFQVONTOC-UHFFFAOYSA-N [3-acetyloxy-2,2-bis(acetyloxymethyl)propyl] acetate Chemical compound CC(=O)OCC(COC(C)=O)(COC(C)=O)COC(C)=O OUHCZCFQVONTOC-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000010695 polyglycol Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of cleaning agent for cleaning of graphic arts equipment ink, it is characterized in that, made by the raw material of following weight portion: turpentine oil 6-8,3-methyl-cyclopentanone 10-12, sodium hydrogen phosphate 3-4, borax 2-3, paranitrobenzoic acid 3-4, sodium sulfocyanate 2-3, aniline 1-2, melamine 3-4, sodium sulphate 2-3, citric acid 3-4, PAG 10-12, auxiliary agent 4-5, water 100-110; The present invention adds auxiliary agent, has improved the processing performance of cleaning agent, reduces its toxic and side effect and the pollution to environment; Cleaning fluid of the present invention can reduce oil consumption, reduces cost, reduce device damage, improves surface smoothness, strengthens cleannes, nontoxic, volatilize little, harmlessly, and application prospect is extensive.
Description
Technical field
The present invention relates to print cleaning technique field, particularly a kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof.
Background technology
In printing industry, often use now to have the parts of ink to clean for printing machinery forme, rubber roll, blanket etc. be to clean with organic solvents such as gasoline, kerosene, acetone, alcohol; Such cleaning agent exists inflammable, explosive, contaminated environment, harm bedding sack health, and to cleaning part, as: glue rod, blanket surface burn into swelling action, to parts damages, shorten service life widely, simultaneously to using workman's skin of hand burn into injury of solvent, this solvent clean weak effect, gasoline, coal are the products of Petroleum refining, and ballooning oil prices, can cause the waste of non-renewable resources petroleum-based energy so now. At present, the widely used cleaning agent in market, is not that to be acidity be exactly to be alkalescence, is acid cleaning agent and can has a strong impact on original true qualities and fineness, is alkaline cleaning agent and can permeates cleaning objects, causes object corrosion, even comes off.
Novel printing ink cleaning agent is compared with kerosene with gasoline, and cleaning performance is good, and security performance is high, and little to the contamination hazard of human body and environment. Novel printing ink cleaning agent is normally made up of solvent, surfactant, auxiliary agent, water. At present conventional solvent is still from non-renewable solvent naphtha, and such as kerosene, smell is large, and degradability is poor, and environment is still existed to certain threat.
Summary of the invention
The object of this invention is to provide a kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
For a cleaning agent for cleaning of graphic arts equipment ink, made by the raw material of following weight portion: turpentine oil 6-8,3-methyl-cyclopentanone 10-12, sodium hydrogen phosphate 3-4, borax 2-3, paranitrobenzoic acid 3-4, sodium sulfocyanate 2-3, aniline 1-2, melamine 3-4, sodium sulphate 2-3, citric acid 3-4, PAG 10-12, auxiliary agent 4-5, water 100-110;
Described auxiliary agent is made up of the raw material of following weight portion: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, Tea Polyphenols 2-3, glycerin monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 10351-2, ethanol 15-18; Preparation method mixes Silane coupling reagent KH-570, castor oil acid, ethanol, is heated to 60-70 DEG C, stirs after 20-30 minute, then adds other residual components, is warming up to 80-85 DEG C, stirs 30-40 minutes, to obtain final product.
Cleaning agent for cleaning of graphic arts equipment ink of the present invention, made by following concrete steps:
(1) at room temperature turpentine oil, 3-methyl-cyclopentanone, sodium hydrogen phosphate, borax, paranitrobenzoic acid 3, sodium sulfocyanate, aniline, melamine are added in mixing kettle, after the water of half amount is heated to 65-75 DEG C, add in mixing kettle, be stirred to completely and dissolve;
(2) sodium sulphate, citric acid, PAG are added in mixing kettle, add the water that is heated to 80-90 DEG C of surplus, stir 4-5 minute with the speed of 1300-1500 rev/min;
(3) finally auxiliary agent and all the other residual components are added in mixing kettle, stir, naturally cooling.
Excellent effect of the present invention is: the present invention adds auxiliary agent, has improved the processing performance of cleaning agent, reduces its toxic and side effect and the pollution to environment; Cleaning fluid of the present invention can reduce oil consumption, reduces cost, reduce device damage, improves surface smoothness, strengthens cleannes, nontoxic, volatilize little, harmlessly, and application prospect is extensive.
Detailed description of the invention
Below by instantiation, the present invention is described in detail.
For a cleaning agent for cleaning of graphic arts equipment ink, by following weight portion (kilogram) raw material make: turpentine oil 6,3-methyl-cyclopentanone 10, sodium hydrogen phosphate 3, borax 2, paranitrobenzoic acid 3, sodium sulfocyanate 2, aniline 1, melamine 3, sodium sulphate 2, citric acid 3, PAG 10, auxiliary agent 4, water 100;
Described auxiliary agent by following weight portion (kilogram) raw material make: Silane coupling reagent KH-570 3, castor oil acid 2, Tea Polyphenols 2, glycerin monostearate 4, neopentyl glycol 2, p-tert-butyl benzoic acid 4, antioxidant 10351, ethanol 15; Preparation method mixes Silane coupling reagent KH-570, castor oil acid, ethanol, is heated to 60-70 DEG C, stirs after 20-30 minute, then adds other residual components, is warming up to 80-85 DEG C, stirs 30-40 minutes, to obtain final product.
Cleaning agent for cleaning of graphic arts equipment ink of the present invention, made by following concrete steps:
(1) at room temperature turpentine oil, 3-methyl-cyclopentanone, sodium hydrogen phosphate, borax, paranitrobenzoic acid 3, sodium sulfocyanate, aniline, melamine are added in mixing kettle, after the water of half amount is heated to 65-75 DEG C, add in mixing kettle, be stirred to completely and dissolve;
(2) sodium sulphate, citric acid, PAG are added in mixing kettle, add the water that is heated to 80-90 DEG C of surplus, stir 4-5 minute with the speed of 1300-1500 rev/min;
(3) finally auxiliary agent and all the other residual components are added in mixing kettle, stir, naturally cooling.
Ink is applied on the stainless steel metal thin slice of certain mass, under nature, dries, steel disc is placed in to the beaker that fills cleaning agent, at 25 DEG C, soak after 5 minutes, more at the uniform velocity vibrate 5 minutes, obtaining cleaning soil removal efficiency is 93.1%, and cleansing power is good. With this cleaning agent, with compared with gasoline, kerosene, rubber cloth increases the service life 2 years, and ink roller can increase the service life 2 years.
Claims (1)
1. the cleaning agent for cleaning of graphic arts equipment ink, it is characterized in that, made by the raw material of following weight portion: turpentine oil 6-8,3-methyl-cyclopentanone 10-12, sodium hydrogen phosphate 3-4, borax 2-3, paranitrobenzoic acid 3-4, sodium sulfocyanate 2-3, aniline 1-2, melamine 3-4, sodium sulphate 2-3, citric acid 3-4, PAG 10-12, auxiliary agent 4-5, water 100-110; Described auxiliary agent is made up of the raw material of following weight portion: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, Tea Polyphenols 2-3, glycerin monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 10351-2, ethanol 15-18; Preparation method mixes Silane coupling reagent KH-570, castor oil acid, ethanol, is heated to 60-70 DEG C, stirs after 20-30 minute, then adds other residual components, is warming up to 80-85 DEG C, stirs 30-40 minutes, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310579649.9A CN103613984B (en) | 2013-11-19 | 2013-11-19 | A kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310579649.9A CN103613984B (en) | 2013-11-19 | 2013-11-19 | A kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103613984A CN103613984A (en) | 2014-03-05 |
| CN103613984B true CN103613984B (en) | 2016-05-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310579649.9A Active CN103613984B (en) | 2013-11-19 | 2013-11-19 | A kind of cleaning agent for cleaning of graphic arts equipment ink and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103613984B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101050323A (en) * | 2007-04-24 | 2007-10-10 | 华南理工大学 | Cleaning agent for ink printed on surface of plastic and preparation method |
| CN101089168A (en) * | 2007-06-19 | 2007-12-19 | 吕连新 | Multifunctional cleaning agent |
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN102558941A (en) * | 2010-12-31 | 2012-07-11 | 宋国新 | Printing ink cleaning agent |
-
2013
- 2013-11-19 CN CN201310579649.9A patent/CN103613984B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101050323A (en) * | 2007-04-24 | 2007-10-10 | 华南理工大学 | Cleaning agent for ink printed on surface of plastic and preparation method |
| CN101089168A (en) * | 2007-06-19 | 2007-12-19 | 吕连新 | Multifunctional cleaning agent |
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN102558941A (en) * | 2010-12-31 | 2012-07-11 | 宋国新 | Printing ink cleaning agent |
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| Publication number | Publication date |
|---|---|
| CN103613984A (en) | 2014-03-05 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Cleaning agent for cleaning printing ink of printing equipment and preparation method thereof Effective date of registration: 20170818 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank, Limited by Share Ltd, Fuyang Ying River West Road subbranch Pledgor: ANHUI BENSE PRINTING CO., LTD. Registration number: 2017340000164 |
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Date of cancellation: 20181012 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank, Limited by Share Ltd, Fuyang Ying River West Road subbranch Pledgor: ANHUI BENSE PRINTING CO., LTD. Registration number: 2017340000164 |
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Denomination of invention: Cleaning agent for cleaning printing ink of printing equipment and preparation method thereof Effective date of registration: 20181017 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank, Limited by Share Ltd, Fuyang Ying River West Road subbranch Pledgor: ANHUI BENSE PRINTING CO., LTD. Registration number: 2018330000311 |
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Date of cancellation: 20191203 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank, Limited by Share Ltd, Fuyang Ying River West Road subbranch Pledgor: ANHUI BENSE PRINTING CO., LTD. Registration number: 2018330000311 |
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Denomination of invention: Cleaning agent for cleaning printing ink of printing equipment and preparation method thereof Effective date of registration: 20191205 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank, Limited by Share Ltd, Fuyang Ying River West Road subbranch Pledgor: ANHUI BENSE PRINTING CO., LTD. Registration number: Y2019330000253 |
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Date of cancellation: 20201016 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank Limited by Share Ltd. Fuyang Ying River West Road subbranch Pledgor: ANHUI COLOR PRINTING Co.,Ltd. Registration number: Y2019330000253 |
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Denomination of invention: A cleaning agent for cleaning printing ink and its preparation method Effective date of registration: 20201019 Granted publication date: 20160525 Pledgee: Huizhou Merchants Bank Limited by Share Ltd. Fuyang Ying River West Road subbranch Pledgor: ANHUI COLOR PRINTING Co.,Ltd. Registration number: Y2020980006903 |
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