CN103613978B - A kind of detergent for ink undamaged to equipment and preparation method thereof - Google Patents
A kind of detergent for ink undamaged to equipment and preparation method thereof Download PDFInfo
- Publication number
- CN103613978B CN103613978B CN201310514978.5A CN201310514978A CN103613978B CN 103613978 B CN103613978 B CN 103613978B CN 201310514978 A CN201310514978 A CN 201310514978A CN 103613978 B CN103613978 B CN 103613978B
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- CN
- China
- Prior art keywords
- sodium
- castor oil
- auxiliary agent
- ink
- undamaged
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000003599 detergent Substances 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 7
- MUBZPKHOEPUJKR-UHFFFAOYSA-N oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000002253 acid Substances 0.000 claims abstract description 14
- 239000004359 castor oil Substances 0.000 claims abstract description 13
- 235000019438 castor oil Nutrition 0.000 claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- XMGQYMWWDOXHJM-UHFFFAOYSA-N (+-)-(RS)-limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims abstract description 7
- VKYKSIONXSXAKP-UHFFFAOYSA-N Hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229960004011 Methenamine Drugs 0.000 claims abstract description 7
- 210000001834 NPE Anatomy 0.000 claims abstract description 7
- KIEOKOFEPABQKJ-UHFFFAOYSA-N Sodium dichromate Chemical compound [Na+].[Na+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KIEOKOFEPABQKJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 7
- XMVONEAAOPAGAO-UHFFFAOYSA-N Sodium tungstate Chemical compound [Na+].[Na+].[O-][W]([O-])(=O)=O XMVONEAAOPAGAO-UHFFFAOYSA-N 0.000 claims abstract description 7
- LSNNMFCWUKXFEE-UHFFFAOYSA-L Sulphite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 claims abstract description 7
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Tris Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940087305 limonene Drugs 0.000 claims abstract description 7
- 229930007650 limonene Natural products 0.000 claims abstract description 7
- 235000001510 limonene Nutrition 0.000 claims abstract description 7
- 235000006408 oxalic acid Nutrition 0.000 claims abstract description 7
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims abstract description 7
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 150000007949 saponins Chemical class 0.000 claims abstract description 7
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 7
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- 241001122767 Theaceae Species 0.000 claims description 9
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000001808 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 6
- 229910000077 silane Inorganic materials 0.000 claims description 6
- SLCVBVWXLSEKPL-UHFFFAOYSA-N 2,2-dimethylpropane-1,3-diol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 229940117969 NEOPENTYL GLYCOL Drugs 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N Para-tert-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 230000003078 antioxidant Effects 0.000 claims description 3
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 3
- 235000013824 polyphenols Nutrition 0.000 claims description 3
- VBICKXHEKHSIBG-UHFFFAOYSA-N rac-1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 3
- 235000013616 tea Nutrition 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000007639 printing Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 230000003000 nontoxic Effects 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 231100000486 side effect Toxicity 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 240000007524 Camellia sinensis var. sinensis Species 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 description 6
- 239000002904 solvent Substances 0.000 description 5
- 239000003502 gasoline Substances 0.000 description 4
- 239000003350 kerosene Substances 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 206010022114 Injury Diseases 0.000 description 1
- 210000003491 Skin Anatomy 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002522 swelling Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Abstract
The invention discloses a kind of detergent for ink undamaged to equipment, it is characterized in that, be prepared by the raw materials in: NPE 57, sodium sulfonate 23, triethanolamine 12, oxalic acid 23, limonene 34, tea saponin 12, sodium tungstate 12, hexamethylenamine 23, sodium dichromate 12, sodium lauryl sulfate 12, sodium tripolyphosphate 12, castor oil acid 23, auxiliary agent 45, water 100 110；The present invention adds auxiliary agent, improves the processing performance of abluent, reduces its toxic and side effects and the pollution to environment；Cleansing power of the present invention is strong, and nontoxic, non-volatile, harmless, to printing equipment not damaged, corrosion-free, cost of manufacture is low, safety and environmental protection, and application prospect is extensive.
Description
Technical field
The present invention relates to print cleaning technique field, particularly a kind of detergent for ink undamaged to equipment and preparation method thereof.
Background technology
In printing industry, the most commonly used element purge having ink for printing machinery forme, rubber roll, blanket etc. is to be carried out with organic solvents such as gasoline, kerosene, acetone, ethanol；Such abluent also exists inflammable, explosive, polluting environment, harm bedding sack is healthy, and to cleaning parts, as: glue rod, blanket surface burn into swelling action, to parts damages, greatly shorten service life, simultaneously to the workman's skin of hand burn into injury using solvent, this solvent clean weak effect, gasoline, coal are the products of Petroleum refining, and present ballooning oil prices so can cause the waste of non-renewable resources petroleum-based energy.At present, the widely used abluent in market, is not to be exactly in alkalescence in acidity, can have a strong impact on the original this normal complexion fineness in acid abluent, and the abluent in alkalescence can permeate cleaning objects, causes object to corrode, even comes off.
Novel printing ink cleaning agent is compared with gasoline and kerosene, and cleaning performance is good, and security performance is high, and the contamination hazard to human body and environment is little.Novel printing ink cleaning agent is typically to be made up of solvent, surfactant, auxiliary agent, water.The most conventional solvent is still from non-renewable solvent naphtha, such as kerosene, and abnormal smells from the patient is big, and degradability is poor, and environment still suffers from certain threat.
Summary of the invention
It is an object of the invention to provide a kind of detergent for ink undamaged to equipment and preparation method thereof.
In order to realize the purpose of the present invention, the present invention is implemented by below scheme:
A kind of detergent for ink undamaged to equipment, is prepared by the raw materials in: NPE 5-7, sodium sulfonate 2-3, triethanolamine 1-2, oxalic acid 2-3, limonene 3-4, tea saponin 1-2, sodium tungstate 1-2, hexamethylenamine 2-3, sodium dichromate 1-2, sodium lauryl sulfate 1-2, sodium tripolyphosphate 1-2, castor oil acid 2-3, auxiliary agent 4-5, water 100-110；
Described auxiliary agent is prepared by the raw materials in: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, tea polyphenols 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 1035
1-2, ethanol 15-18；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
Detergent for ink undamaged to equipment of the present invention, is made up of step in detail below:
(1) at room temperature adding in mixing kettle by triethanolamine, oxalic acid, limonene, tea saponin, sodium tungstate, hexamethylenamine, sodium dichromate, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) NPE, sodium sulfonate, sodium lauryl sulfate, sodium tripolyphosphate, castor oil acid are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-5 minute with the speed of 1300-1500 rev/min；
(3) finally auxiliary agent and remaining residual components are added in mixing kettle, stir, natural cooling.
The excellent effect of the present invention is: the present invention adds auxiliary agent, improves the processing performance of abluent, reduces its toxic and side effects and the pollution to environment；Cleansing power of the present invention is strong, and nontoxic, non-volatile, harmless, to printing equipment not damaged, corrosion-free, cost of manufacture is low, safety and environmental protection, and application prospect is extensive.
Detailed description of the invention
Below by instantiation, the present invention is described in detail.
A kind of detergent for ink undamaged to equipment, is made up of the raw material of following weight portion (kilogram): NPE 5, sodium sulfonate 2, triethanolamine 1, oxalic acid 2, limonene 3, tea saponin 1, sodium tungstate 1, hexamethylenamine 2, sodium dichromate 1, sodium lauryl sulfate 1, sodium tripolyphosphate 1, castor oil acid 2, auxiliary agent 4, water 100；
Described auxiliary agent is made up of the raw material of following weight portion (kilogram): Silane coupling reagent KH-570 3, castor oil acid 2, tea polyphenols 2, glyceryl monostearate 4, neopentyl glycol 2, p-tert-butyl benzoic acid 4, antioxidant 1035
1, ethanol 15；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
Detergent for ink undamaged to equipment of the present invention, is made up of step in detail below:
(1) at room temperature adding in mixing kettle by triethanolamine, oxalic acid, limonene, tea saponin, sodium tungstate, hexamethylenamine, sodium dichromate, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) NPE, sodium sulfonate, sodium lauryl sulfate, sodium tripolyphosphate, castor oil acid are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-5 minute with the speed of 1300-1500 rev/min；
(3) finally auxiliary agent and remaining residual components are added in mixing kettle, stir, natural cooling.
Being applied to by ink on the stainless steel metal thin slice of certain mass, dry under naturalness, be placed in by steel disc in the beaker filling abluent, after soaking 5 minutes, more at the uniform velocity vibrate 5 minutes at 25 DEG C, obtaining clean dirt rate is 92.6%, and cleansing power is good.With this abluent with compared with gasoline, kerosene, rubber cloth increases the service life 2 years, and ink roller can increase the service life 2 years.
Claims (2)
1. a detergent for ink undamaged to equipment, it is characterized in that, be prepared by the raw materials in: NPE 5-7, sodium sulfonate 2-3, triethanolamine 1-2, oxalic acid 2-3, limonene 3-4, tea saponin 1-2, sodium tungstate 1-2, hexamethylenamine 2-3, sodium dichromate 1-2, sodium lauryl sulfate 1-2, sodium tripolyphosphate 1-2, castor oil acid 2-3, auxiliary agent 4-5, water 100-110；
Described auxiliary agent is prepared by the raw materials in: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, tea polyphenols 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 1035 1-2, ethanol 15-18；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
Detergent for ink undamaged to equipment the most according to claim 1, it is characterised in that be made up of step in detail below:
(1) at room temperature adding in mixing kettle by triethanolamine, oxalic acid, limonene, tea saponin, sodium tungstate, hexamethylenamine, sodium dichromate, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) NPE, sodium sulfonate, sodium lauryl sulfate, sodium tripolyphosphate, castor oil acid are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, with 1300-1500 rev/min
Speed stir 4-5 minute；
(3) finally auxiliary agent is added in mixing kettle, stir, natural cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310514978.5A CN103613978B (en) | 2013-10-28 | A kind of detergent for ink undamaged to equipment and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310514978.5A CN103613978B (en) | 2013-10-28 | A kind of detergent for ink undamaged to equipment and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103613978A CN103613978A (en) | 2014-03-05 |
| CN103613978B true CN103613978B (en) | 2016-11-30 |
Family
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101089168A (en) * | 2007-06-19 | 2007-12-19 | 吕连新 | Multifunctional cleaning agent |
| CN101597547A (en) * | 2009-05-21 | 2009-12-09 | 陈安友 | A kind of phosphate-free environment-friendly cleaning agent |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
| CN101684212A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Efficient detergent for print ink |
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101089168A (en) * | 2007-06-19 | 2007-12-19 | 吕连新 | Multifunctional cleaning agent |
| CN101684212A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Efficient detergent for print ink |
| CN101597547A (en) * | 2009-05-21 | 2009-12-09 | 陈安友 | A kind of phosphate-free environment-friendly cleaning agent |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Xiao Xiaomei Inventor before: Song Yuchun |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20161008 Address after: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Applicant after: Xiao Xiaomei Address before: 233000 No. 404 South Daqing Road, hi tech Zone, Anhui, Bengbu Applicant before: Anhui Topusen Battery Co., Ltd. |
|
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Tang Jun Inventor before: Xiao Xiaomei |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20170627 Address after: 523960, No. 235, West Ring Road, Houjie village, Houjie Town, Guangdong, Dongguan Patentee after: Dongguan Vatican Industry Co., Ltd. Address before: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Patentee before: Xiao Xiaomei |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161130 Termination date: 20201028 |