CN103613180A - Polymer gel breaker and preparation method thereof - Google Patents
Polymer gel breaker and preparation method thereof Download PDFInfo
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- CN103613180A CN103613180A CN201310627796.9A CN201310627796A CN103613180A CN 103613180 A CN103613180 A CN 103613180A CN 201310627796 A CN201310627796 A CN 201310627796A CN 103613180 A CN103613180 A CN 103613180A
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- gel breaker
- polymkeric substance
- persulphate
- water
- preparation
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Abstract
The invention discloses a polymer gel breaker and a preparation method thereof. The preparation method comprises the following steps: mixing 1.175% of persulfate with 1-5% of propylene glycol, further mixing the obtained mixture with 1-2% of hydrogen peroxide, 2-3% of citric acid and water, and finally split charging, packaging, inspecting and subsequently storing in warehouses. As polymer gel breakage is sufficiently solved in a chemical mode, the polymer gel breaker is rapid and durable in effect.
Description
Technical field
The present invention relates to field of chemicals, relate in particular to a kind of polymkeric substance gel breaker and preparation method thereof.
Background technology
Solving in the market the muddy major part of water body is to use the mode of chemical flocculation, can only play temporary transient control action kou to granular physics muddiness like this, cannot tackle the problem at its root.
Summary of the invention
Technical problem to be solved by this invention is, a kind of water body muddiness that solves from source is provided, and uses chemical mode to cause that muddy organic matter decomposes utilization, polymkeric substance gel breaker of purifying water body and preparation method thereof,
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: a kind of polymkeric substance gel breaker, and percentage ratio meter by weight, its formula comprises following component and content:
Described persulphate is persulphate ammonium or Potassium Persulphate.
Also comprise that weight percent is 2-3% citric acid.
Preferably, percentage ratio meter by weight, its formula comprises following component and content:
The preparation method of above-mentioned polymkeric substance gel breaker, comprises the steps:
(1) persulphate is mixed with to the aqueous solution, with mixed with propylene glycol;
(2) add again remaining other components and water, mix;
(3) packing packing, warehouse-in is up to the standards.
The invention has the beneficial effects as follows: the present invention solves the broken glue of polymkeric substance from source, use chemical mode to solve the broken glue of polymkeric substance, its effect is lasting again fast, for water body aboundresources serious China of eutrophication again, has wide market outlook.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail:
Polymkeric substance gel breaker of the present invention, percentage ratio meter by weight, its formula comprises following component and content:
Described persulphate is persulphate ammonium or Potassium Persulphate.
Also comprise that weight percent is 2-3% citric acid.
Preferably, percentage ratio meter by weight, its formula comprises following component and content:
The preparation method of above-mentioned polymkeric substance gel breaker, comprises the steps:
(1) persulphate is mixed with to the aqueous solution, with mixed with propylene glycol;
(2) add again remaining other components and water, mix;
(3) packing packing, warehouse-in is up to the standards.
Hydrogen peroxide of the present invention is for the fast decoupled granular greasy filth dregs that flocculates; Propylene glycol is mainly as the carrier of ammonium persulphate, can absorbed portion compound as the corrosion base of ammonium persulphate, also can adsorb, the granular dregs of the part of flocculating simultaneously; Persulphate causes muddy organism more than needed for solving, raising water transparency.
Specific embodiments of the invention given below can further be understood the present invention, but they are not limitation of the invention.In addition, unless stated otherwise, the per-cent adopting in the present invention is all weight percentage.
Embodiment 1
By following step, prepare polymkeric substance gel breaker of the present invention:
(1) by 5 kilograms of ammonium persulphates (content 35% of ammonium persulphate) and 5 kilograms of mixed with propylene glycol;
(2) again this mixture is mixed with 5 kilograms of aqueous hydrogen peroxide solutions (content 35% of hydrogen peroxide), 85 kg of water;
(3) packing packing, warehouse-in is up to the standards.
Embodiment 2
By following step, prepare polymkeric substance gel breaker of the present invention:
(1) by 5 kilograms of ammonium persulphates (content 35% of ammonium persulphate, lower same) and 5 kilograms of mixed with propylene glycol;
(2) again this mixture is mixed with 3 kilograms of aqueous hydrogen peroxide solutions (content 35% of hydrogen peroxide), 3 kilograms of citric acids, 84 kg of water;
(3) packing packing, warehouse-in is up to the standards.
Embodiment 3
By following step, prepare polymkeric substance gel breaker of the present invention:
(1) by 4.3 kilograms of Potassium Persulphates (content 35% of Potassium Persulphate) and 1 kilogram of mixed with propylene glycol;
(2) again this mixture is mixed with 4 kilograms of aqueous hydrogen peroxide solutions (content 35% of hydrogen peroxide), 2 kilograms of citric acids, 88.7 kg of water;
(3) packing packing, warehouse-in is up to the standards.
Embodiment 4
By following step, prepare polymkeric substance gel breaker of the present invention:
(1) by 3 kilograms of ammonium persulphates (content 35% of ammonium persulphate) and 5 kilograms of mixed with propylene glycol;
(2) again this mixture is mixed with 3 kilograms of aqueous hydrogen peroxide solutions (content 35% of hydrogen peroxide), 3 kilograms of citric acids, 86 kg of water;
(3) packing packing, warehouse-in is up to the standards.
The polymkeric substance gel breaker that embodiment 3 is made, samples processing for the smelly sewage of water body, the effect obtaining in Table 1 with table 2, wherein the polymkeric substance gel breaker of embodiment 4 is for the water body of pH3.0-7.0.
Table 1
Water purification agent of the present invention, can be widely used in the oily(waste)water waste oil mud of the industries such as chemical industry, oil field, iron and steel etc.
This product has good chemical stability, facile hydrolysis not, to containing polymeric colloid water by broken glue effect preferably.By changing profit surface tension, make the oil-water mixture of " water-in-oil " or " oil-in-water " form reach the object that profit breaks glue, there is good intermiscibility with other various water treatment agents, in order to form multiple water treatment formula.Render to town domestic sewage, trade effluent, in aquaculture wastewater, can make heavy metal substance and contamination precipitation in water body, can make the larger molecular organics in sewage resolve into small organic molecule simultaneously, and be convenient to flocculate, and in flocculation process, nitrogen in a large amount of adsorbed water bodies, phosphorus nutrition thing and other suspended matter, and become the flocculation group that stability is strong, make water body become transparent limpid, allow hydrobiont and plant in water, can be at healthy growth under sufficient photosynthesis, effectively reduce the rich nutritive material in water simultaneously, to controlling or eliminate Blue-green Algae Fast Growth, there is remarkable effect, and then improve water ecological setting, recover the original eubiosis of water body.
Above-described embodiment is only for illustrating technological thought of the present invention and feature, its object is to make those skilled in the art can understand content of the present invention and implement according to this, can not only with the present embodiment, limit the scope of the claims of the present invention, be equal variation or the modification that all disclosed spirit is done, still drop in the scope of the claims of the present invention.
Claims (4)
1. a polymkeric substance gel breaker, is characterized in that, percentage ratio meter by weight, and its formula comprises following component and content:
Described persulphate is persulphate ammonium or Potassium Persulphate.
2. polymkeric substance gel breaker according to claim 1, is characterized in that, also comprises that weight percent is 2-3% citric acid.
3. polymkeric substance gel breaker according to claim 2, is characterized in that, percentage ratio meter by weight, and its formula comprises following component and content:
4. a preparation method for the polymkeric substance gel breaker as described in claim 1-3 any one, is characterized in that, comprises the steps:
(1) persulphate is mixed with to the aqueous solution, with mixed with propylene glycol;
(2) add again remaining other components and water, mix;
(3) packing packing, warehouse-in is up to the standards.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310627796.9A CN103613180A (en) | 2013-11-28 | 2013-11-28 | Polymer gel breaker and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310627796.9A CN103613180A (en) | 2013-11-28 | 2013-11-28 | Polymer gel breaker and preparation method thereof |
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| CN103613180A true CN103613180A (en) | 2014-03-05 |
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| CN201310627796.9A Pending CN103613180A (en) | 2013-11-28 | 2013-11-28 | Polymer gel breaker and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107188381A (en) * | 2017-05-12 | 2017-09-22 | 浙江奇彩环境科技股份有限公司 | A kind of greasy filth separation medicament and preparation method thereof |
| CN109231355A (en) * | 2018-10-26 | 2019-01-18 | 知合环境（北京）有限责任公司 | A kind of polymer-containing oil sludge purifying treatment method and cleaning agent used |
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| US20050178553A1 (en) * | 2004-02-13 | 2005-08-18 | Harris Phillip C. | Two stage subterranean zone fracturing fluids and methods |
| CN102417814A (en) * | 2011-11-16 | 2012-04-18 | 北京国海能源技术研究院 | Seawater-based fracturing fluid and preparation method thereof |
| CN102618249A (en) * | 2012-03-05 | 2012-08-01 | 中国海洋石油总公司 | Seawater base fracturing fluid and preparation method thereof |
| CN103173200A (en) * | 2012-12-24 | 2013-06-26 | 北京仁创科技集团有限公司 | Water-base fracturing fluid and method for preparing same |
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2013
- 2013-11-28 CN CN201310627796.9A patent/CN103613180A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050178553A1 (en) * | 2004-02-13 | 2005-08-18 | Harris Phillip C. | Two stage subterranean zone fracturing fluids and methods |
| CN102417814A (en) * | 2011-11-16 | 2012-04-18 | 北京国海能源技术研究院 | Seawater-based fracturing fluid and preparation method thereof |
| CN102618249A (en) * | 2012-03-05 | 2012-08-01 | 中国海洋石油总公司 | Seawater base fracturing fluid and preparation method thereof |
| CN103173200A (en) * | 2012-12-24 | 2013-06-26 | 北京仁创科技集团有限公司 | Water-base fracturing fluid and method for preparing same |
Non-Patent Citations (1)
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| 李平安等: "《食品添加剂原理与安全使用》", 30 September 2011, article "载体溶剂", pages: 301 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107188381A (en) * | 2017-05-12 | 2017-09-22 | 浙江奇彩环境科技股份有限公司 | A kind of greasy filth separation medicament and preparation method thereof |
| CN109231355A (en) * | 2018-10-26 | 2019-01-18 | 知合环境（北京）有限责任公司 | A kind of polymer-containing oil sludge purifying treatment method and cleaning agent used |
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Application publication date: 20140305 |