CN103599733A - Vibration feeding device applied in deposition fluidized bed - Google Patents
Vibration feeding device applied in deposition fluidized bed Download PDFInfo
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- CN103599733A CN103599733A CN201310383263.0A CN201310383263A CN103599733A CN 103599733 A CN103599733 A CN 103599733A CN 201310383263 A CN201310383263 A CN 201310383263A CN 103599733 A CN103599733 A CN 103599733A
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- feed arrangement
- feeding cylinder
- bed
- fluidized bed
- oscillatory type
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- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
The invention relates to a vibration feeding device applied in a deposition fluidized bed. The vibration feeding device comprises a feeding barrel and an actuating part. The feeding barrel stores bed layer particles for the deposition fluidized bed. The actuating part can touch the feeding barrel periodically so that the feeding barrel generates vibration under touch, thus achieving discharge of the bed layer particles. The novel vibration feeding device applied in the deposition fluidized bed can effectively solve disadvantages of gas-carrying type feeding devices in the prior art, and can achieve a stable and controllable feeding amount. When the vibration feeding device is applied in the deposition fluidized bed, a stable-state deposition reaction process can be achieved.
Description
Technical field
The present invention relates to a kind of vibrating feed device being applied in deposition fluidized bed.
Background technology
Isotropic pyrolytic carbon (Isotropic pyrolytic carbon) material is a kind of high performance carbon material that utilizes chemical gaseous phase depositing process (chemical vapor deposition is CVD one by one) to prepare, because its knot ditch is fine and close, crystallite dimension is little, therefore except possessing the high temperature resistant of general carbonaceous material, lubricated, wear-resistant, outside the general character advantages such as good biocompatibility, also there is intensity high, airtight, the good holding point of processability, do not need any impregnating post processing just can directly be used as high-performance mechanical black box, its intensity, wear-resisting, sealing property, biocompatibility, processability etc. are all better than conventional carbon material greatly.
In the deposition fluidized bed system adopting in prior art, in deposition process, by the particle collection device of gas-phase deposition reactor bottom and the particle adder on reactor top, realize the replacing of bed particle, by particle adder and particle, collecting device can be to adding in fluid bed or emitting bed particle
Particle adder of the prior art shown in Fig. 1 has air inlet, enters particle weight by regulating the air-flow (argon gas, hydrogen or nitrogen etc.) of particle adder to regulate, and particle enters reaction zone by gas outlet under airflow function.Thisly by carrier band gas mobile, carry the mode that the micro-material of bottom carries out reaction zone, in actual production, material footpath and proportion variation due to the micro-material of bottom, when air-flow is carried, its inlet amount can not be accurately controlled in easy appearance, thereby cannot realize the stable control to whole deposition fluidized bed system production process.
Summary of the invention
In order to overcome above-mentioned deficiency, the object of the present invention is to provide a kind of vibrating feed device being applied in deposition fluidized bed, realize for the equal effective inlet amount of precise control of different bed particles.
Technical scheme of the present invention is:
Be applied to the oscillatory type feed arrangement in deposition fluidized bed, comprise feeding cylinder, actuated components; Feeding cylinder storage is for the bed particle of deposition fluidized bed; It is characterized in that:
Actuated components can periodically be touched feeding cylinder, and feeding cylinder produces vibration under touching, realizes the discharge of bed particle.
Advantage of the present invention and beneficial effect are:
The present invention has designed for the new-type vibrating feed device in deposition fluidized bed, can effectively solve the shortcoming of gas portable type feed arrangement in prior art, realize stablizing of inlet amount controlled, be applied to can control the deposition reaction process that realizes stable state in deposition fluidized bed.
Accompanying drawing explanation
Fig. 1 is particle adder schematic diagram in prior art.
Fig. 2 is for adopting the fluidized system figure of vibrating feed device of the present invention
Fig. 3 is feed arrangement front view
Fig. 4 is feed arrangement top view
Fig. 5 is charging orifice plate
1-feed arrangement fixed mount, 2-feeding cylinder hold-down screw, 3-feeding cylinder support spring,
4-charging orifice plate, 5-feeding cylinder, 6-particle, 7-drive motors,
8-eccentric rotary parts
The specific embodiment
System in the present invention utilizes chemical vapor deposition method to prepare isotropic pyrolytic carbon material.Fig. 2 is system diagram, is mainly divided into reaction unit, feed arrangement, drawing mechanism, sensing and control device, thermatron five parts.In reaction unit, high frequency induction power supply heats precipitation equipment by induction coil, with photoelectric pyrometer, temperature control system, measures and regulation and control depositing temperature.Precipitation equipment is graphite conical fluidized bed precipitation equipment.Dilution and carrier band gas are hydrogen, argon gas or nitrogen etc., and the flow of gas is measured and controlled by flowmeter and needle-valve.The tail gas that reaction produces is processed by exhaust treatment system.As shown in Figure 1.The reaction zone of precipitation equipment is provided with back taper opening, realizes bed particle fluidization.Hydrocarbon gas and carrier gas pass into from gas access and blow diameter is that bed particle forms fluidization in reactor.In deposition process, by the drawing mechanism of precipitation equipment bottom and the feed arrangement on top, realize the stable replacing of bed particle, can be continuous by feed arrangement and drawing mechanism to adding in fluid bed or emitting bed particle.
The reaction zone of precipitation equipment is provided with back taper opening, realizes bed particle fluidization.Hydrocarbon gas and carrier gas pass into from gas access and blow diameter is that the bed particle of 0.2mm-0.5mm forms fluidization in reactor.In deposition process, by the drawing mechanism of precipitation equipment bottom and the feed arrangement on top, realize the stable replacing of bed particle, can be continuous by feed arrangement and drawing mechanism to adding in fluid bed or emitting bed particle.
As shown in Figure 3-Figure 5, feed arrangement has feeding cylinder, eccentric rotary parts and the drive motors that holds bed particle, motor drives eccentric rotary parts to rotate, property performance period touching feeding cylinder, and make the displacement of feeding cylinder generating period lateral vibration, and feeding cylinder bottom is back taper, and feeding cylinder is connected by screw in feed arrangement fixed mount, in its underpart, adopt spring to support, can make it carry out vibration displacement, below, feeding cylinder inside is provided with charging orifice plate, on charging orifice plate, there are one or more charging holes, the 1-5 of the general optional bed particle diameter of charging hole diameter doubly, under normal circumstances, the bed particle holding in feeding cylinder is each other due to friction and Extrusion effect, can not pass through smoothly charging hole, when eccentric rotary parts are periodically touched feeding cylinder, the bed particle holding in feeding cylinder is under vibration force effect, friction and Extrusion effect weakens each other, the bed particle of some can pass through charging hole smoothly, after the rotation of eccentric rotary parts is passed through, because vibration force effect disappears, the bed particle holding in feeding cylinder can recover inactive state again under friction and Extrusion effect, cannot pass through charging hole.By selecting charging hole quantity, diameter dimension and controlling motor rotary speed, can achieve effective control feed particles amount.In addition, motor can adopt forward and reverse rotation mode work, reduces rotating mechanism and takes up room and increase work efficiency.
Feed particles amount is controlled motor direction of rotation and the rotational speed regulation of feed arrangement by sensing and control device, the charging frequency of feed arrangement is regulated to the technological parameters such as real-time maintenance bed area, fluidized state stable.The above-mentioned cycle actuating mechanism of realizing based on motor, also can adopt other conventional similar periodicity actuating mechanism, as electric and magnetic oscillation, and air pressure or hydraulic vibration.
By above feed arrangement, realized the accurate and effective of bed pellet feed amount and controlled.
Claims (7)
1. be applied to the oscillatory type feed arrangement in deposition fluidized bed, comprise feeding cylinder, actuated components; Feeding cylinder storage is for the bed particle of deposition fluidized bed; It is characterized in that:
Actuated components can periodically be touched feeding cylinder, and feeding cylinder produces vibration under touching, realizes the discharge of bed particle.
2. oscillatory type feed arrangement as claimed in claim 1, is characterized in that: feeding cylinder bottom is back taper, and the charging orifice plate of its internal placement is provided with one or more charging holes.
3. oscillatory type feed arrangement as claimed in claim 2, is characterized in that: charging hole diameter is elected 1-5 times of bed particle diameter as.
4. oscillatory type feed arrangement as claimed in claim 2, is characterized in that: by selecting quantity and the size of charging hole, single particle discharge rate is regulated.
5. oscillatory type feed arrangement as claimed in claim 2, is characterized in that: regulate the action cycle of actuated components, realize the pellet feed amount of adjusting in its unit interval.
6. oscillatory type feed arrangement as claimed in claim 2, is characterized in that: actuated components adopts one of motor driving, Electromagnetic Drive, air pressure driving or hydraulic driving mode.
7. oscillatory type feed arrangement as claimed in claim 6, is characterized in that: when adopting motor to drive, by controlling motor direction of rotation and the rotational speed regulation of feed arrangement, the charging frequency of feed arrangement is regulated.
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CN201310383263.0A CN103599733B (en) | 2013-08-29 | 2013-08-29 | A kind of vibrating feed device be applied in deposition fluidized bed |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105568254A (en) * | 2016-02-24 | 2016-05-11 | 清华大学 | Gas inlet equipment for chemical vapor deposition reactor of fluidized bed |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN201997308U (en) * | 2010-11-23 | 2011-10-05 | 天津市科迈化工有限公司 | Novel rubber accelerator granulation equipment |
CN202955949U (en) * | 2012-12-14 | 2013-05-29 | 铜陵鑫克精细化工有限责任公司 | Fluidized bed with screening device |
CN203620590U (en) * | 2013-08-29 | 2014-06-04 | 北京思达医用装置有限公司 | Vibration feeding device applied to deposition fluidized bed |
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2013
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN201997308U (en) * | 2010-11-23 | 2011-10-05 | 天津市科迈化工有限公司 | Novel rubber accelerator granulation equipment |
CN202955949U (en) * | 2012-12-14 | 2013-05-29 | 铜陵鑫克精细化工有限责任公司 | Fluidized bed with screening device |
CN203620590U (en) * | 2013-08-29 | 2014-06-04 | 北京思达医用装置有限公司 | Vibration feeding device applied to deposition fluidized bed |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105568254A (en) * | 2016-02-24 | 2016-05-11 | 清华大学 | Gas inlet equipment for chemical vapor deposition reactor of fluidized bed |
CN105568254B (en) * | 2016-02-24 | 2018-10-30 | 清华大学 | A kind of gas inlet device for fluidized-bed chemical vapor deposition reactor |
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CN103599733B (en) | 2016-01-20 |
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