CN103536793A - Composition with functions of clearing away heat and toxic materials and removing fire as well as preparation method thereof - Google Patents
Composition with functions of clearing away heat and toxic materials and removing fire as well as preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of foods, and discloses a composition with functions of clearing away heat and toxic materials and removing fire as well as a preparation method thereof. The composition with functions of clearing away heat and toxic materials and removing fire disclosed by the invention is prepared from the following medical and edible medicinal raw materials: honeysuckle, Mentha haplocalyx, liquorice, lophatherum gracile and Momordica grosvenori. The composition is simple in formula, and has remarkable effects of clearing heat and dispelling wind, removing pattogenic heat from the blood and toxic material from the body, nourishing yin to lessen fire, relieving summer heat and quenching thirst and relieving sore-throat and dispelling the effects of alcohol. The preparation method of the composition with functions of clearing away heat and toxic materials and removing fire disclosed by the invention comprises the following steps: respectively extracting effective components of honeysuckle, Mentha haplocalyx, liquorice, lophatherum gracile and Momordica grosvenori by adopting different methods to obtain a liquorice, lophatherum gracile and Momordica grosvenori mixed extract liquid, a honeysuckle extract liquid and a Mentha haplocalyx extract liquid; finally mixing the extract liquids in a certain proportion to prepare the composition. The effective components of the raw materials are remained to the maximum extent. The composition prepared by the method has the remarkable effects of clearing away heat and toxic materials and removing fire, and the preparation method is simple to operate and applicable to industrialized production.
Description
Technical field
The invention belongs to food technology field, relate to specifically a kind of dispel composition and method of making the same of fire action of heat-clearing and toxic substances removing that has.
Background technology
" getting angry " is Chinese medicine specific term.If there is symptoms such as pharyngodynia with dryness, two furious red, nasal cavity baking the affected part after applying some drugs, xerostomia glossodynia and angular chilitis, epistaxis, toothache, the traditional Chinese medical science is just thought " getting angry ".Get angry be divided into diseases caused by exogenous pathogenic factor burning hot and in the heat of lighting a fire.Diseases caused by exogenous pathogenic factor are be intimately directly subject to the invasion and attack of nature " burning hot heresy " and cause " getting angry " symptom.Heatstroke is exactly the burning hot diseases of a kind of typical diseases caused by exogenous pathogenic factor, is all conventionally slow-witted overlong time under excess Temperature, hydropenia, sultry environment, and then body temperature also can raise.The heat of inside lighting a fire be exist in body can promote vital functions and invisible " fire ", due to imbalance of YIN and YANG, lost normal hiding function, and caused " getting angry " symptom.Get angry and have the deeper meaning, the symptom of some broad sense of namely getting angry, such as symptoms such as stomach-fire can have a stomach-ache, large dry stool, halitosis, lung-fire can have the symptoms such as spitting of blood, cough, yellow sputum, liver-fire has some agitations, insomnia, women and has distending pain of the breast, and heart-fire will palpitation and insomnia, vexed.
The material elements that causes " getting angry " is a lot, and anxious state of mind is excessive, heatstroke, suffer from cold, catch cold, have a liking for the pungent product such as tobacco and wine and surfeit Herba Alii fistulosi, Rhizoma Zingiberis Recens, Bulbus Allii, Fructus Capsici, the product that voracious Carnis caprae seu ovis, Carnis Canitis etc. are rich and poisoning, lack sleep etc. and all can " get angry ".Along with the raising of people's living standard, work and rhythm of life are accelerated, and it is large that people's pressure becomes, often stay up late, and dietary structure imbalance in addition, gluttonous pungent, rich food, the factor of lighting a fire in making is more much bigger than in the past.So the enthusiasm condition of lighting a fire is in general burning hot more than diseases caused by exogenous pathogenic factor.
A lot of people think that getting angry is indisposition, have some heat-clearing and toxic substances removing dispel fiery medicine or food self regulation just passable once.In fact the lighter situation of getting angry, be to note striking a proper balance between work and rest by taking the heat-clearing and toxic substances removing fiery health food of dispelling simultaneously, eats less pungent fried food and carry out own adjusting.Along with socioeconomic development and the higher pursuit to health, the concern that there is specific function, the plain health food that supplements the nutrients is more and more subject to broad masses of the people.At present the conventional heat-clearing and toxic substances removing fiery health food of dispelling is a lot, the fiery DeGrain but mostly fill a prescription complexity or heat-clearing and toxic substances removing are dispelled, and therefore, research and development compatibility is simple, the significant heat-clearing and toxic substances removing of effect is dispelled fiery health food is to regulating the symptom of getting angry significant.
Summary of the invention
In view of this, the object of the present invention is to provide that a kind of compatibility is simple, effect has the dispel composition and method of making the same of fire action of heat-clearing and toxic substances removing significantly.
For realizing object of the present invention, the present invention adopts following technical scheme:
There is the dispel compositions of fire action of heat-clearing and toxic substances removing, by the raw material of following weight portion, made: Flos Lonicerae 400-500 part, Herba Menthae 5-15 part, Radix Glycyrrhizae 20-60 part, Herba Lophatheri 10-30 part, Fructus Momordicae 5-15 part.
Preferably, described in there is the dispel compositions of fire action of heat-clearing and toxic substances removing, by following weight portion raw material, made: 460 parts of Flos Loniceraes, 10 parts of Herba Menthaes, 40 parts, Radix Glycyrrhizae, 20 parts, 10 portions Fructus Momordicaes of Herba Lophatheri.
The present invention also provides a kind of dispel preparation method of compositions of fire action of heat-clearing and toxic substances removing that has, and comprising:
Step 1: get 400-500 weight portion Flos Lonicerae and add flooding, filter and collect Flos Lonicerae extractive solution, filtering residue is standby;
Step 2: get 5-15 weight portion Herba Menthae and add water ultrasonic extraction, filter and collect Herba Menthae extracting solution, filtering residue is standby;
Step 3: 20-60 weight portion Radix Glycyrrhizae, 10-30 weight portion Herba Lophatheri, 5-15 weight portion Fructus Momordicae are mixed, decoct with water, filter and collect Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, filtering residue is standby; Wherein the weight ratio of Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae is 4:2:1;
Step 4: the filtering residue producing in above-mentioned three steps is mixed, decoct with water, filter and collect filtering residue extracting solution;
Step 5: after the extracting solution remove impurity of respectively above-mentioned four steps being collected by Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio that filtering residue extracting solution is 46:1:7:40 is mixed and be get final product.
Preferably, described in step 1, adding flooding is to add the water of 30 times of weight in 80 ℃ of lixiviate 30min.
Preferably, described in step 2, adding water ultrasonic extraction is the water ultrasonic extraction 30min that adds 20 times of weight.
Preferably, described in step 3, decoct with water as adding the decocting of 20 times of weight to boil 20min.
Preferably, described in step 4, decoct with water as adding the decocting of 30 times of weight to boil 20min.
The compositions that the present invention also provides described preparation method to prepare.
The present invention also provides the health food that comprises described compositions, and it is tea beverage and contains slab sugar.
The present invention also provides a kind of dispel preparation method of tea beverage of fire action of heat-clearing and toxic substances removing that has.
The dispel preparation method of tea beverage of fire action of heat-clearing and toxic substances removing, the sucrose solution mixing preparation that is 6 by Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Flos Lonicerae extractive solution, Herba Menthae extracting solution, filtering residue extracting solution and sugariness, fill, sterilizing and get final product; Wherein, described Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio of filtering residue extracting solution and sucrose solution is 46:1:7:40:400.
Of the present invention have heat-clearing and toxic substances removing and dispel that to select the medical material of Flos Lonicerae, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae five tastes medicine-food two-purpose be that raw material is made for the compositions of fire action, formula is simple, clearing away heat to dispel wind, removing pathogenic heat from blood and toxic substance from the body, nourishing YIN to lower pathogenic fire, relieve summer heat quench one's thirst, the sore-throat relieving effect of relieving the effect of alcohol is remarkable.Of the present invention have the dispel preparation method of fire action of heat-clearing and toxic substances removing and adopt distinct methods to extract respectively the effective ingredient in Flos Lonicerae, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae, obtain Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Flos Lonicerae extractive solution, Herba Menthae extracting solution, then mix and make according to a certain percentage, the effective ingredient that has farthest retained each raw material, the compositions heat-clearing and toxic substances removing the preparing fiery effect of dispelling is remarkable, simultaneously simple to operate, be suitable for suitability for industrialized production.
The specific embodiment
The embodiment of the invention discloses a kind of dispel composition and method of making the same of fire action of heat-clearing and toxic substances removing that has.Those skilled in the art can use for reference content herein, suitably improve technological parameter and realize.Special needs to be pointed out is, all similar replacements and change apparent to those skilled in the artly, they are all deemed to be included in the present invention.Method of the present invention is described by preferred embodiment, and related personnel obviously can change method as herein described or suitably change and combination within not departing from content of the present invention, spirit and scope, realizes and apply the technology of the present invention.
For realizing object of the present invention, the present invention adopts following technical scheme:
There is the dispel compositions of fire action of heat-clearing and toxic substances removing, by the raw material of following weight portion, made: Flos Lonicerae 400-500 part, Herba Menthae 5-15 part, Radix Glycyrrhizae 20-60 part, Herba Lophatheri 10-30 part, Fructus Momordicae 5-15 part.
The mechanism that compositions of the present invention causes getting angry for the invasion and attack of " burning hot heresy " is selected the Chinese crude drug of the five tastes medicine-food two-purposes such as Flos Lonicerae, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae.
Wherein, Flos Lonicerae has another name called Radix Ophiopogonis, is the perennial half evergreen xylophyta of Caprifoliaceae, and Flos Lonicerae is Caprifoliaceae woodbine Radix Ophiopogonis and congener dry flower or the first flower of opening of band.Flos Lonicerae is cold in nature, and sweet in the mouth enters lung, the heart, stomach warp, has the effect of heat-clearing and toxic substances removing, antiinflammatory, tonify deficiency treatment wind, cures mainly disease under distension, epidemic febrile disease heating, the diseases such as pyretic toxicity carbuncle and ulcer and tumor.
Herba Menthae, popular name is " lunar caustic grass ", for labiate " Herba Menthae " belongs to other dry herbs together, cool in nature, acrid in the mouth, enter lung meridian, Liver Channel, the effect with dispelling wind and heat pathogens, the clear sharp head, sore-throat relieving rash, soothing the liver circulation of qi promoting, cures mainly dispelling wind, dispels the heat, wards off dirty, removing toxic substances, affection due to external wind and heat, headache, laryngopharynx swelling and pain, dyspepsia flatulence, aphtha, toothache, skin ulcer scabies, urticaria, epidemic febrile disease be from the beginning of, rubella pruritus, stagnation of QI due to depression of the liver, hypochondriac pain uncomfortable in chest.
Radix Glycyrrhizae, another name Herba Hedyotis cantonensis root, Radix Glycyrrhizae, Radix Glycyrrhizae are dicotyledon pulse family Radix Glycyrrhizae (Glycyrrhiza uralensis Fisch.), the root and rhizome of Glycyrrhiza inflata Bat. (G.inflata Bat.) or Glycyrrhiza glabra L. (G.glabra L.), be a kind of tonification Chinese herbal medicine, have removing toxic substances, eliminate the phlegm, pain relieving, spasmolytic be so that the pharmacological action such as anticancer.In the traditional Chinese medical science, Radix Glycyrrhizae invigorating the spleen and replenishing QI, grows and to cough lung moistening, and emergency removing toxic substances is in harmonious proportion hundred medicines.Clinical practice divides " raw using " and " processed with honey " not." raw with " Radix Glycyrrhizae has another name called Radix Glycyrrhizae, SHENGCAO, and Radix Glycyrrhizae, for crude drug is removed impurity, is cleaned, runs through section and give birth to being used as medicine; " processed with honey " has another name called Radix Glycyrrhizae Preparata, Radix Glycyrrhizae Preparata, Radix Glycyrrhizae, Radix Glycyrrhizae (processed with honey), and the Radix Glycyrrhizae tabellae of making a living is mixed thoroughly with Mel, then fries to tack-free taking-up airing, is then used as medicine.Radix Glycyrrhizae of the present invention is Radix Glycyrrhizae, sweet in the mouth, property are put down, GUIXIN, lung, spleen, stomach warp, there is invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain, coordinating the actions of various ingredients in a prescription, strong for the anxious pain of weakness of the spleen and stomach, fatigue and weakness, shortness of breath and palpitation, cough with copious phlegm, gastral cavity abdomen, extremity contraction, carbuncle sore tumefacting virus, cushion toxicity.
Herba Lophatheri, has another name called Rhizoma lophantheri, Gallus jabouillei rice, Herba Lophatheri, Folium Bambosae, is the dry stem and leaf of grass family herbaceos perennial Herba Lophatheri.Herba Lophatheri is cold in nature, sweet in the mouth, GUIXIN, kidney channel, have sweetly lightly ooze profit, cold in naturely fall clearly, kind fire of leading the heart and small intestinal is descending and the effects such as inducing diuresis for treating stranguria syndrome, be mainly used in the heart disease heat, cough with dyspnea, haematemesis, pyretic toxicity wind, only quench one's thirst, press borax poison, expectorant, fanatical unhappiness, apoplectic aphasia in silence, bitterly wind syndrome of head, spasmolytic throb with fear, pestilence be confused vexed, pregnant woman's head revolve fall down to the ground, children's shies the diseases such as carbuncle sky hangs, sore throat, dysphoria with smothery sensation.
Fructus Momordicae, claims again LAHANGUO, tamarindus indica L., tea hill, red comospore, is the fruit of Cucurbitaceae liana Fructus Momordicae.Fructus Momordicae is cool in nature, and sweet in the mouth is returned lung, large intestine channel, has the effect of clearing heat and moistening lung, cough-relieving, sore-throat relieving, laxation relieving constipation, is mainly used in lung-fire cough caused by dryness, pharyngalgia aphonia, the diseases such as dryness of the intestine constipation.
The sweet cold of Flos Lonicerae property fragrance in compositions of the present invention, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil, can dispelling wind-heat, also kind removing summer-heat blood poison; Herba Menthae dispelling wind and heat pathogens, soothing the liver circulation of qi promoting; Herba Lophatheri is cold in nature to fall clearly, and the fire that can lead the heart and small intestinal is descending; Fructus Momordicae can dispel lung-fire and stomach-fire, clearing heat and moistening lung, cough-relieving, relieving constipation; Radix Glycyrrhizae invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, simultaneously coordinating the actions of various ingredients in a prescription.The all medicines of Flos Lonicerae, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae are also used, reach clearing away heat to dispel wind, removing pathogenic heat from blood and toxic substance from the body, nourishing YIN to lower pathogenic fire, relieve summer heat quench one's thirst, effect that sore-throat relieving relieves the effect of alcohol, medical material used is all nontoxic simultaneously, long-term taking dependency is little, and cheap, be applicable to ordinary consumer and use.
Flos Lonicerae described in the present invention, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae are well known to a person skilled in the art, can by commercial sources buy from a medical store obtain or by disclosed method cultivation in prior art, gathering obtains, its specification meets country or industry standard.
As preferably, compositions of the present invention, is made by following weight portion raw material: 460 parts of Flos Loniceraes, 10 parts of Herba Menthaes, 40 parts, Radix Glycyrrhizae, 20 parts, 10 portions Fructus Momordicaes of Herba Lophatheri.
The present invention also provides the preparation method of described compositions.
The dispel preparation method of compositions of fire action of heat-clearing and toxic substances removing, comprises
Step 1: get 400-500 weight portion Flos Lonicerae and add flooding, filter and collect Flos Lonicerae extractive solution, filtering residue is standby;
Step 2: get 5-15 weight portion Herba Menthae and add water ultrasonic extraction, filter and collect Herba Menthae extracting solution, filtering residue is standby;
Step 3: 20-60 weight portion Radix Glycyrrhizae, 10-30 weight portion Herba Lophatheri, 5-15 weight portion Fructus Momordicae are mixed, decoct with water, filter and collect Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, filtering residue is standby; Wherein the weight ratio of Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae is 4:2:1;
Step 4: the filtering residue producing in above-mentioned three steps is mixed, decoct with water, filter and collect filtering residue extracting solution;
Step 5: after the extracting solution remove impurity of respectively above-mentioned four steps being collected by Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio that filtering residue extracting solution is 46:1:7:40 is mixed and be get final product.
Raw material variety, rank and extraction pre-treatment may affect the content of effective ingredient in compositions, therefore of the present invention have a dispel preparation method of compositions of fire action of heat-clearing and toxic substances removing, raw materials selected and pretreated step before being also included in each raw extract of preparation.Each material choice is smokeless, burnt, sour, sour and other abnormal flavour all, and without chemical pollutant and heavy metal, the medical material of non agricultural chemical residuum amount.Each pretreatment of raw material is removed the impurity of medical material the inside for selection, with warm water cleaning, shreds.
Wherein, because Flos Lonicerae is in storage process, polyphenols can be oxidized and easily cause quality fission, and therefore preferably four seasons Flos Lonicerae kind is introduced a fine variety in Shandong.This kind has output annual April to October, can guarantee fund's Flos Lonicerae raw materials enjoy stable sources, and avoid Flos Lonicerae to store rotten.For the rank of Flos Lonicerae, be preferably low and middle-grade ranks.Because the tender degree of high level Flos Lonicerae well, soluble component content is higher, easily occur " ripe soup taste ", and price is also higher in the course of processing.Can adopt in certain embodiments and be equipped with a small amount of high-quality Flos Lonicerae, wherein high-quality Flos Lonicerae and low and middle-grade Flos Lonicerae weight ratio are 1:6.
It is key prepared by compositions that material effective component extracts, and by controlling extraction conditions, can reduce leaching process loss of effective components, makes effective ingredient stripping to greatest extent in raw material.The principal element that affects raw material extraction efficiency has extracting mode, extracts the selection of solvent, extracts solid-liquid ratio (ratio that extracts solvent and raw material) and extracts temperature and time etc.
Of the present invention have heat-clearing and toxic substances removing and dispel the preparation method of compositions of fire action according to the character of each raw material, selects different extracting modes.Wherein, preferably Flos Lonicerae adds flooding; Herba Menthae adds water ultrasonic extraction; Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae decoct with water.
Extracting solid-liquid ratio is the key factor that affects extraction efficiency, and it has larger impact to the extraction ratio of raw material, turbidity.When solid-liquid ratio is low, active substance leaching rate is high, and the shared volume of turbidity little ，Dan unit leachate is excessive, has increased equipment investment, operation inconvenience etc.; When solid-liquid ratio is high, leaching rate is low, and raw material availability is low, has increased cost of material and utilization rate.Extract temperature and time and can affect extraction efficiency equally.
Wherein, of the present invention have the heat-clearing and toxic substances removing Flos Lonicerae of dispelling described in the preparation method step 1 of compositions of fire action and add flooding and be preferably Flos Lonicerae and add the water of 30 times of weight in 80 ℃ of lixiviate 30min.Described in step 2, Herba Menthae adds water ultrasonic extraction and is preferably the water ultrasonic extraction 30min that Herba Menthae adds 20 times of weight.Described in step 3, decoct with water and be preferably Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae mixture and add the decocting of 20 times of weight to boil 20min.
In leaching process, once extract and active substance can not be extracted completely, therefore of the present invention have the dispel preparation method step 4 of compositions of fire action of heat-clearing and toxic substances removing the filtering residue producing in above-mentioned three steps mixed, decoct with water, to improve each raw material availability, there is the dispel content of each effective ingredient in the compositions of fire action of heat-clearing and toxic substances removing described in raising.Wherein, described in step 4, decoct with water as adding the decocting of 30 times of weight to boil 20min.
Owing to may influencing each other between the raw material of Chinese medicine in compositions, may be potentiation, attenuation, antagonism, oppose each other and yet also complement each other, sometimes also may produce chemical reaction.Therefore the proportioning of each raw material extracting solution has material impact to the effect of compositions.In order to reach clearing away heat to dispel wind, removing pathogenic heat from blood and toxic substance from the body, nourishing YIN to lower pathogenic fire, relieve summer heat quench one's thirst, effect that sore-throat relieving relieves the effect of alcohol, of the present invention have heat-clearing and toxic substances removing and dispel the preparation method step 5 of compositions of fire action preferably by Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio that filtering residue extracting solution is 46:1:7:40 is mixed.
The compositions that the present invention also provides above-mentioned preparation method to prepare.
The present invention also provides has the dispel health food of compositions of fire action of heat-clearing and toxic substances removing described in comprising.Those skilled in the art can basis demand compositions of the present invention is added and prepares the adjuvant that different dosage form is required various routines, as disintegrating agent, lubricant, emulsifying agent, binding agent etc., with conventional formulation method, through the acceptable adjuvant that adds that conventional machining is direct or indirect, make common dosage forms as tea-drinking, tablet, granule, capsule, powder, pill, oral liquid and syrup etc.
Preferably, the health food of compositions of the present invention is tea beverage and containing slab sugar, is easy to take, and with strong points, effect is obvious.
The present invention also provides a kind of dispel preparation method of tea beverage of fire action of heat-clearing and toxic substances removing that has.
The dispel preparation method of tea beverage of fire action of heat-clearing and toxic substances removing, the sucrose solution mixing preparation that is 6 by Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Flos Lonicerae extractive solution, Herba Menthae extracting solution, filtering residue extracting solution and sugariness, fill, sterilizing and get final product; Wherein, described Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio of filtering residue extracting solution and sucrose solution is 46:1:7:40:400.
Radix Glycyrrhizae in the preparation method of tea beverage of the present invention, Herba Lophatheri, Fructus Momordicae mixed extract, Flos Lonicerae extractive solution, Herba Menthae extracting solution, filtering residue extracting solution have the heat-clearing and toxic substances removing method described in the preparation method of compositions of fire action of dispelling and prepare according to above-mentioned.
Be described Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract for by 20-60 weight portion Radix Glycyrrhizae, 10-30 weight portion Herba Lophatheri, 5-15 weight portion Fructus Momordicae by weight for 4:2:1 mixes, decoct with water, filter collection filtrate and get final product.Preferably, described in, decoct with water as adding the decocting of Radix Glycyrrhizae, Herba Lophatheri and 20 times of weight of Fructus Momordicae mixture to boil 20min.
Described Flos Lonicerae extractive solution adds flooding for getting 400-500 weight portion Flos Lonicerae, filters and collects filtrate and get final product.Preferably, described in, adding flooding is to add the water of 30 times of weight in 80 ℃ of lixiviate 30min.
Described Herba Menthae extracting solution adds water ultrasonic extraction for getting 5-15 weight portion Herba Menthae, filters and collects filtrate and get final product.Preferably, described in, adding water ultrasonic extraction is the water ultrasonic extraction 30min that adds 20 times of weight.
Described filtering residue extracting solution is to get said extracted Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixture, extract Flos Lonicerae and extract the filtering residue mixing producing in Herba Menthae three steps, decocts with water, and filters and collects filtrate and get final product.Preferably, described in, decoct with water as adding the decocting of 30 times of weight of filtering residue to boil 20min.
Allotment is according to product demand, by raw material extracting solution dilute with water, the physical and chemical index of each raw material extracting solution and taste style are adjusted guaranteeing that product has on the basis of effect of clearing away heat to dispel wind, removing pathogenic heat from blood and toxic substance from the body, nourishing YIN to lower pathogenic fire, made its indices meet national Specification value.The factor that affects product physical and chemical index and taste style comprises raw material extracting solution ratio, raw material extracting solution order of addition and temperature.
Wherein, the ratio of allotment is preferably described Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: filtering residue extracting solution: the weight ratio of sucrose solution is 46:1:7:40:400.
Allotment is sequentially preferably that first to add sugariness be 6 sucrose solution, then adds Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Herba Menthae extracting solution and filtering residue extracting solution, finally adds Flos Lonicerae extractive solution.Preferred, before adding Flos Lonicerae extractive solution, make solution temperature be cooled to below 40 ℃.
Sucrose solution of the present invention is to get appropriate white sugar in suitable quantity of water, after heating for dissolving, boil to sugariness be 6.The sugariness of wherein said sucrose solution is to using sucrose as standard, and 1% the aqueous sucrose solution sugariness in the time of 20 ℃ of take is 1.0.
Of the present invention have heat-clearing and toxic substances removing and dispel before each raw material extracting solution of preparation method of compositions of fire action and filtering residue extracting solution mix and also comprise the step to each raw material extracting solution and the remove impurity of filtering residue extracting solution, to remove insoluble visible impurity and the macromolecular complex thing in extracting solution.Macromolecular complex thing is when solution temperature declines, and polymerization can occur.Abbreviation reaction, forms macromolecular complex thing, and along with degree of association constantly increases, complex diameter also constantly increases, and causes extracting solution muddy.Described remove impurity is preferably to filter collects filtrate, standing rear centrifugal.Wherein, filtration can be removed the insoluble visible impurity in extracting solution, and the centrifugal macromolecular complex thing of removing in extracting solution.Described filtration, by general filtered through gauze, is the filtered through gauze through 28*28 specification in some specific embodiments.The described standing cooling standing 12h that is preferably.Described centrifugal preferred rotating speed is 10000-15000r/min, and centrifuging temperature is controlled at 25-30 ℃, and treating capacity is 250L/h.
The preparation method of tea beverage of the present invention is carried out fill by deployed solution after allotment.Preferably, adopt warm fill in 70～80 ℃.During fill, filling liquid volume should strictly be controlled, and prevents that in sterilization process, liquid volume expands, and causes jar distortion or leaks tank phenomenon.
After fill, need to carry out sterilizing, with improve nutritional labeling in beverage can digestibility and availability improve beverage quality, destroy wherein unwanted harmful components simultaneously, extend shelf life.Preferably, described sterilizing is instantaneous ultrahigh-temperature sterilization, thereby is conducive to the color of described tea beverage and the maintenance of quality.More preferably, described instantaneous ultrahigh-temperature sterilization is under 135 ℃～150 ℃ ultra-high temperature conditions, sterilizing 2s～8s.
Water be of the present invention have heat-clearing and toxic substances removing dispel fire action compositions and described in there is the important component part that heat-clearing and toxic substances removing is dispelled in the tea beverage preparation process of fire action, directly have influence on quality and the mouthfeel of compositions and beverage, therefore need to be that tap water is suitably processed to general water source, with have described in improving heat-clearing and toxic substances removing dispel fire action compositions and described in there is dispel quality and the mouthfeel of tea beverage of fire action of heat-clearing and toxic substances removing.
Preferably, described in, be treated to tap water through filtering after-tack desalination, afterwards disinfection.
Wherein, described filtration object is except anhydrating middle fine suspension and colloidal substance.When tap water sees through filter medium, in surface or hole that some float in water and colloidal substance are trapped within filter medium.
In certain embodiments, described filtration is preferably and adopts single current pressure filter to filter.During operation, tap water enters filter from water inlet pipe, through inlet damper uniform water distribution, passes through filtering layer from top to bottom; Remove the clear water of float and colloidal substance after filter tip (water cap) is collected, by outlet pipe, drawn.
In filter process, when filtration resistance reaches certain value, by pressure transducer, control appliance is out of service, carries out backwash.Backwash mode need to adopt pure water pressure flush, after filtering layer is cleaned, stops backwash, just washes, and after the wash water matter is qualified by online detection, enters next periodic duty.Generally control with the loss of flood peak filter cycle, adopts 98kPa during three-layer filter.Filtrate adopts 18-20L/(s.m
2).With filtering layer expansion rate, reaching 40%-50% is advisable.Washing time 5-7min.
Water after filtration need to soften desalination, to reduce the dissolubility impurity in water.Wherein, softening is the Ca reducing in water
2+and Mg
2+the processing of content, desalination is to reduce whole cationes and all processing of the content of aniones.In certain embodiments, described softening desalination is preferably the reverse osmosis membrane separation technology that adopts.Preferred, described permeable membrane is complete fragrant high-crosslinking-degree polyamide composite film.
The sterilization that carries out disinfection of water after softening processing, to kill the microorganism in water.In certain embodiments, described disinfection is preferably ultraviolet-sterilization.More preferably 250～260nm length ultraviolet line irradiates.
In order further to understand the present invention, below in conjunction with embodiment, the present invention is described in detail.
Embodiment 1: have heat-clearing and toxic substances removing the dispel compositions of fire action and the processing that tea beverage is prepared water
Tap water filters through single current pressure filter, utilizes afterwards complete fragrant high-crosslinking-degree polyamide composite film to carry out the softening desalination of reverse osmosis, then through 250～260nm length ultraviolet line irradiation-sterilize, reaches water quality requirement.
Concrete operations are as follows:
Operation single current pressure filter, tap water enters filter from water inlet pipe, through inlet damper uniform water distribution, passes through filtering layer from top to bottom.Clear water, after filter tip (water cap) is collected, is drawn by outlet pipe.When the filtration resistance of filter reaches certain value, need be out of service, carry out backwash.Backwash mode can adopt as required water to rinse or auxiliary air rinses, auxiliary surface is rinsed.While adopting auxiliary air to rinse, generally first the water in water subfill in filter is put to filtering layer edge, then from bottom, sent into compressed air rinsing filtering layer, then rinse with gas, water simultaneously, last alone water rinses.After filtering layer is cleaned, stop backwash, just wash, after the wash water matter is qualified, enter next periodic duty.Generally control with the loss of flood peak filter cycle, adopts 98kPa during three-layer filter.Filtrate adopts 18-20L/(s.m2).With filtering layer expansion rate, reaching 40%-50% is advisable.Washing time 5-7min.
Water conservancy after single current pressure filter filters is carried out reverse osmosis with complete fragrant high-crosslinking-degree polyamide composite film, water turbidity≤2 degree during infiltration, and water temperature is 5-35 ℃, SDI≤5, Fe≤0.1mg/L, pH4-11, chlorine residue≤0.1mg/L.
Water standard after processing is as shown in table 1.
Water standard after table 1 is processed
| Project | Index |
| Turbidity | ＜1 |
| Colourity | ＜5 |
| Total dissolved solid | ＜500 |
| Total hardness is (with CaCO 3Meter)/(mg/L) | ＜100 |
| Ferrum (in Fe) (mg/L) | ＜0.1 |
| Total alkalinity is (with CaCO 3Meter)/(mg/L) | ＜50 |
| Free chlorine/(mg/L) | ＜0.1 |
| Pathogenic bacterium | Must not detect |
Embodiment 2: have the dispel preparation of compositions of fire action of heat-clearing and toxic substances removing
1, material choice
Select all smokeless, burnt, sour, sour and other abnormal flavour, and without chemical pollutant and heavy metal, the Flos Lonicerae of non agricultural chemical residuum amount, Herba Menthae, Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae, choose the removal of impurity, warm water cleaning, chopping.Wherein, Flos Lonicerae is four seasons Flos Loniceraes, and rank is that high-quality Flos Lonicerae and low and middle-grade Flos Lonicerae weight ratio are 1:6.
2, extracting solution preparation
1), get 460kg selection, cleaned Flos Lonicerae adds the water of 30 times of weight in 80 ℃ of lixiviate 30min, filters and collects Flos Lonicerae extractive solution, filtering residue is standby;
2), get the water ultrasonic extraction 30min that 10kg selection, cleaned Herba Menthae add 20 times of weight, filter and collect Herba Menthae extracting solution, filtering residue is standby;
3), selection, cleaned 40kg Radix Glycyrrhizae, 20kg Herba Lophatheri, 10kg Fructus Momordicae are mixed, add the decocting of 20 times of weight to boil 20min, filter and collect Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, filtering residue is standby, and wherein the weight ratio of Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae is 4:2:1;
4), the filtering residue that produces in above-mentioned three steps is mixed, add the decocting of 30 times of weight to boil 20min, filter and collect filtering residue extracting solution;
5), get respectively the filtered through gauze of the extracting solution employing 28*28 specification of above-mentioned four steps collections, the cooling standing 12h of filtrate, 10000-15000r/min, centrifuging temperature is controlled at 25-30 ℃, treating capacity is 250L/h, then by Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio that filtering residue extracting solution is 46:1:7:40 is mixed and be get final product.
Embodiment 3: have the dispel effect experiment of compositions of fire action of heat-clearing and toxic substances removing
Choose there is large dry stool, the sub-health population of the symptom such as halitosis, cough, yellow sputum, dry pharynx pharyngalgia, agitation or insomnia, be divided at random experimental group and matched group, experimental group is established 6 repetitions, matched group is established 3 repetitions, every group of 100 people;
Experimental technique: what experimental group was taken the embodiment of the present invention 2 preparation has a dispel compositions of fire action of heat-clearing and toxic substances removing, and 310mL, takes one month continuously for each person every day; Matched group is taken the Liquor Flos Lonicerae Distillata, and 310mL, takes one month continuously for each person every day;
Judge index:
Effective: in high spirits, have rosy cheeks, the transference cures such as large dry stool, halitosis, cough, yellow sputum, dry pharynx pharyngalgia, agitation or insomnia;
Effective: spirit is improved, the remissions such as large dry stool, halitosis, cough, yellow sputum, dry pharynx pharyngalgia, agitation or insomnia;
Invalid: cardinal symptom does not alleviate, spirit is poor.
Statistical result is in Table 2.
Table 2 is taken effect
As can be seen from Table 2, the obvious effective rate of each group of experimental group is all higher than 65%, and matched group obvious effective rate is all lower than 55%.Result shows, the present invention have heat-clearing and toxic substances removing dispel the compositions of fire action there is obvious clearing away heat to dispel wind, removing pathogenic heat from blood and toxic substance from the body, nourishing YIN to lower pathogenic fire, relieve summer heat quench one's thirst, the effect of sore-throat relieving, successful is better than matched group.
Embodiment 4: have the dispel preparation of tea beverage of fire action of heat-clearing and toxic substances removing
1), get 460kg selection, cleaned Flos Lonicerae adds the water of 30 times of weight in 80 ℃ of lixiviate 30min, filters and collects Flos Lonicerae extractive solution, filtering residue is standby;
2), get the water ultrasonic extraction 30min that 10kg chooses, cleaned Herba Menthae adds 20 times of weight., filtering and collect Herba Menthae extracting solution, filtering residue is standby;
3), selection, cleaned 40kg Radix Glycyrrhizae, 20kg Herba Lophatheri, 10kg Fructus Momordicae are mixed, add the decocting of 20 times of weight to boil 20min, filter and collect Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, filtering residue is standby, and wherein the weight ratio of Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae is 4:2:1;
4), the filtering residue that produces in above-mentioned three steps is mixed, add the decocting of 30 times of weight to boil 20min, filter and collect filtering residue extracting solution;
5) get, respectively extracting solution that above-mentioned four steps collect and adopt the filtered through gauze of 28*28 specification, the cooling standing 12h of filtrate, the centrifugal 10min of 3000r/min, collects respectively the extracting solution after centrifugal;
6), get appropriate white sugar in suitable quantity of water, after boiling after heating for dissolving and being 6 to sugariness, add Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Herba Menthae extracting solution and filtering residue extracting solution after centrifugal, when solution temperature is cooled to below 40 ℃, adding the Flos Lonicerae extractive solution after centrifugal to allocate, the ratio of allotment is Flos Lonicerae extractive solution, Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: filtering residue extracting solution: the weight ratio of sucrose solution is 46:1:7:40:400.
7), deployed solution is 70～80 ℃ of lower temperature fills, under 135 ℃～150 ℃ ultra-high temperature conditions, sterilizing 2s～8s.
Embodiment 5: have heat-clearing and toxic substances removing the dispel every physical and chemical index of tea beverage of fire action and the detection of microbiological indicator
That gets described in embodiment 4 prepared by preparation method has a dispel tea beverage of fire action of heat-clearing and toxic substances removing, by national standard, detects more every physical and chemical index and microbiological indicator, the results are shown in Table 3 and 4.
The testing result of table 3 physical and chemical index
| Project | Index | Assay |
| Soluble solid (20 ℃ of compound microcapsules), | ≥1.0% | 5.6 |
| Chlorogenic acid/mg/L | ≥5 | 6.695 |
| Total arsenic (in As)/mg/kg | ≤0.2 | 0.032 |
| Plumbous (in Pb)/mg/Kg | ≤0.3 | 0.072 |
| Copper (in Cu), mg/Kg | ≤5.0 | 0.25 |
| Sulfur dioxide residual quantity, mg/Kg | ≤10 | 3.74 |
| Gamma Hexaochlorocyclohexane, mg/Kg | ≤0.02 | Do not detect |
| Clofenotane, mg/Kg | ≤0.02 | Do not detect |
Table 4 microorganism is limited the quantity of
| Project | Index | Assay |
| Total plate count/(CFU/mL) | ≤100 | ＜1 |
| Coliform/(MPN/mL) | ≤0.06 | ＜0.03 |
| Mold count/(CFU/mL) | ≤10 | ＜1 |
| Yeast counts/(CFU/mL) | ≤10 | ＜1 |
| Salmonella | 0/25mL | Do not detect |
| Shigella | 0/25mL | Do not detect |
| Staphylococcus aureus | 0/25mL | Do not detect |
[0118] the dispel every physical and chemical index of tea beverage and the microbiological indicator of fire action of heat-clearing and toxic substances removing that have of being prepared according to the method for the invention as seen by table 3 and table 4 result all meets national standard requirement.
Embodiment 6: have the dispel evaluation of tea beverage taste index of fire action of heat-clearing and toxic substances removing
The dispel taste of tea beverage of fire action of heat-clearing and toxic substances removing that has prepared by preparation method described in embodiment 4 is evaluated.Evaluation index comprises 1) color and luster, mainly by Polyphenol oxide, the decisions such as xanthin; 2) fragrance, is mainly determined by all kinds of aromatics; 3) flavour, comprises bright refreshing taste, bitter taste, delay sense, sweet taste etc.The results are shown in Table 2.
Respectively in Chengdu, Zhengzhou, Shenyang, Suzhou and each random investigation 100 people of city, 5, Kunming, respectively embodiment 4 preparation had to heat-clearing and toxic substances removing color and luster, fragrance and the flavour of tea beverage of a fire action evaluation of marking of dispelling: extremely enjoying a lot is 5 minutes, like is 4 minutes, be generally 3 minutes, not liking is 2 minutes, and very not liking is 1 minute.Statistical result is described in 95% people likes or extremely likes, to have the dispel color pool of tea beverage of fire action of heat-clearing and toxic substances removing; Described in liking or extremely like, 97% people there is the dispel fragrance of tea beverage of fire action of heat-clearing and toxic substances removing; Described in liking or extremely like, 98% people there is the dispel flavour of tea beverage of fire action of heat-clearing and toxic substances removing.
In addition, in 100 people in Chengdu, 98% has the dispel whole local flavor of tea beverage of fire action of heat-clearing and toxic substances removing described in liking or extremely liking; In 100 people in Zhengzhou, 95% has the dispel whole local flavor of tea beverage of fire action of heat-clearing and toxic substances removing described in liking or extremely liking; In 100 people in Shenyang, 93% has the dispel whole local flavor of tea beverage of fire action of heat-clearing and toxic substances removing described in liking or extremely liking; In 100 people in Suzhou, 96% has the dispel whole local flavor of tea beverage of fire action of heat-clearing and toxic substances removing described in liking or extremely liking; In 100 people in Kunming, 97% has the dispel whole local flavor of tea beverage of fire action of heat-clearing and toxic substances removing described in liking or extremely liking.As can be seen here, of the present invention have heat-clearing and toxic substances removing and dispel that west area, middle part, northern territory, eastern region and southern areas have all obtained good evaluation at home for the tea beverage of fire action.
The explanation of above embodiment is just for helping to understand method of the present invention and core concept thereof.It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, can also carry out some improvement and modification to the present invention, these improvement and modification also fall in the protection domain of the claims in the present invention.
Claims (10)
1. there is the dispel compositions of fire action of heat-clearing and toxic substances removing, it is characterized in that, by the raw material of following weight portion, made: Flos Lonicerae 400-500 part, Herba Menthae 5-15 part, Radix Glycyrrhizae 20-60 part, Herba Lophatheri 10-30 part, Fructus Momordicae 5-15 part.
2. compositions according to claim 1, is characterized in that, by following weight portion raw material, is made: 460 parts of Flos Loniceraes, 10 parts of Herba Menthaes, 40 parts, Radix Glycyrrhizae, 20 parts, 10 portions Fructus Momordicaes of Herba Lophatheri.
3. there is the dispel preparation method of compositions of fire action of heat-clearing and toxic substances removing, it is characterized in that, comprise
Step 1: get 400-500 weight portion Flos Lonicerae and add flooding, filter and collect Flos Lonicerae extractive solution, filtering residue is standby;
Step 2: get 5-15 weight portion Herba Menthae and add water ultrasonic extraction, filter and collect Herba Menthae extracting solution, filtering residue is standby;
Step 3: 20-60 weight portion Radix Glycyrrhizae, 10-30 weight portion Herba Lophatheri, 5-15 weight portion Fructus Momordicae are mixed, decoct with water, filter and collect Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, filtering residue is standby; Wherein the weight ratio of Radix Glycyrrhizae, Herba Lophatheri and Fructus Momordicae is 4:2:1;
Step 4: the filtering residue producing in above-mentioned three steps is mixed, decoct with water, filter and collect filtering residue extracting solution;
Step 5: after the extracting solution remove impurity of respectively above-mentioned four steps being collected by Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio that filtering residue extracting solution is 46:1:7:40 is mixed and be get final product.
4. preparation method according to claim 3, is characterized in that, adding flooding described in step 1 is to add the water of 30 times of weight in 80 ℃ of lixiviate 30min.
5. preparation method according to claim 3, is characterized in that, adding water ultrasonic extraction described in step 2 is the water ultrasonic extraction 30min that adds 20 times of weight.
6. preparation method according to claim 3, is characterized in that, decocts with water as adding the decocting of 20 times of weight to boil 20min described in step 3.
7. preparation method according to claim 3, is characterized in that, decocts with water as adding the decocting of 30 times of weight to boil 20min described in step 4.
8. the compositions that described in claim 3-7 any one prepared by preparation method.
9. the health food that comprises the compositions described in claim 1,2 or 7, it is tea beverage and containing slab sugar.
10. one kind has the dispel preparation method of tea beverage of fire action of heat-clearing and toxic substances removing, it is characterized in that, the sucrose solution mixing preparation that is 6 by Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract, Flos Lonicerae extractive solution, Herba Menthae extracting solution, filtering residue extracting solution and sugariness, fill, sterilizing and get final product; Wherein, described Flos Lonicerae extractive solution: Herba Menthae extracting solution: Radix Glycyrrhizae, Herba Lophatheri, Fructus Momordicae mixed extract: the weight ratio of filtering residue extracting solution and sucrose solution is 46:1:7:40:400.
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| CN104324264A (en) * | 2014-11-04 | 2015-02-04 | 西双版纳版纳药业有限责任公司 | Herbal preparation for relieving summer heat, clearing heat and removing toxicity and preparation method thereof |
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| CN106890274A (en) * | 2015-12-17 | 2017-06-27 | 上海寿叶生物科技有限公司 | Tea for moistening lung and treating cough |
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| CN113662067A (en) * | 2021-08-27 | 2021-11-19 | 百色学院 | Preparation method of medicinal and edible fermented herbal tea suitable for drinking after sports and product thereof |
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| CN103907728A (en) * | 2014-03-26 | 2014-07-09 | 赵云 | Tea capable of eliminating heat and purging fire and preparation method of tea |
| CN104146247A (en) * | 2014-07-29 | 2014-11-19 | 桂林实力科技有限公司 | Preparation method of momordica grosvenori syrup |
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| CN106890274A (en) * | 2015-12-17 | 2017-06-27 | 上海寿叶生物科技有限公司 | Tea for moistening lung and treating cough |
| CN105995363A (en) * | 2016-06-29 | 2016-10-12 | 王啸天 | Honeysuckle flower and peppermint water flavored beverage and preparation method thereof |
| CN107279852A (en) * | 2017-07-07 | 2017-10-24 | 贵州省黎平县筑绿康农业发展贸易有限公司 | A kind of hand rubbing capsicum manufacture craft |
| CN113662067A (en) * | 2021-08-27 | 2021-11-19 | 百色学院 | Preparation method of medicinal and edible fermented herbal tea suitable for drinking after sports and product thereof |
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