CN105994735A - Semen ginkgo tea for refreshing brain and restoring consciousness - Google Patents
Semen ginkgo tea for refreshing brain and restoring consciousness Download PDFInfo
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Abstract
The invention discloses semen ginkgo tea for refreshing the brain and restoring consciousness. The semen ginkgo tea comprises sweet osmanthus, flos chrysanthemi indici, herba verbenae, herba abri, herba menthae, semen cassia, fructus gardeniae, malt extract paste, ginkgetin, tea polyphenol, rebaudioside, vitamins, a thickening agent, cosolvent, a dispersing agent, antioxygen, flavor enhancer and a flavouring agent and is prepared through the steps of medical liquid extraction, clear paste preparation, pelleting, sterilization and the like. The semen ginkgo tea has the effects of refreshing the brain and restoring consciousness, and a prepared drink is good in taste and savoury and mellow in flavor; no preservative or pigment is added, essence is extracted from pure natural plants, a tea making technology with cold water is broken through, a low-temperature extraction technology is utilized, it is guaranteed that active ingredients in plants cannot be damaged, the semen ginkgo tea is absorbed by the body easily after being drunk, and shortcomings of traditional products are overcome due to the fact that the semen ginkgo tea is dissolved and absorbed easily.
Description
[technical field]
The invention belongs to tea processing technique field, be specifically related to a kind of refreshment Folium Ginkgo tea and preparation method thereof.
[background technology]
Ginkgoaceae plant Ginkgo biloba is the endemic tree of China, has another name called maidenhair tree, and the age of tree, up to more than thousand, is ancient
For Permian Period Relict Plant, there is the title of " living fossil " in plant kingdom, be the most ancient in existing seed plant
Relict Plant.Modern science shows, the chemical composition of Folium Ginkgo is sufficiently complex, wherein containing flavone in Folium Ginkgo
The effective ingredient such as class, terpenoid, phenols, healthy trace elements with household and several amino acids.Folium Ginkgo extract contains greatly
The ginkgetin of amount, ginkgetin is highly resistant to and prevents the electromagnetic radiation such as computer, mobile phone to make human body
The infringement become, particularly obvious to the protective effect of brain cell, also have vessel softening, remove rubbish in blood,
Drop three fat, remove the effects such as free radical.In active substance, the content of flavone decides the medical value of Folium Ginkgo,
Go for more flavone, it is critical only that the extracting method of Folium Ginkgo；During traditional extraction, solvent exists
It is easily accessible cell under conditions of heating, but solable matter is higher at the condition dissolubility of heat, is successively dissolved
And the highest permeability occurs, and to cause that extraction ratio is low, active component is low, and technique is loaded down with trivial details, the production cycle is long.
Tea polyphenols is the general name of Polyphenols of Tea, is a kind of pure natural complex, and its content accounts for Folium Camelliae sinensis and does
The 10%-25% (Forint phenol method) of material total amount.Tea polyphenols is by catechin (flavanol compound), anthocyan
(leucoanthocyanidin and anthocyanidin), anthoxanthins (flavone and flavonols), phenolic acid and the big material group of depside four
Becoming, wherein catechin is mostly important, and activity is the highest, accounts for the 70%-80% of tea polyphenols total amount.Tea polyphenols
It is a kind of high-efficient pure natural antioxidant, it is possible to remove human free radical, enhancing human body immunity power, has anti-swollen
The multiple medical health care functions such as tumor, radioprotective, antiviral, defying age, lowering blood-fat and reducing weight, also have suppression tremulous pulse
The effects such as atherosis, removing halitosis, enhancing vascular resistance ability.The oxidation resistance ratio of tea polyphenols
Strong 3-9 times of VE, Butylated hydroxyanisole (BHA) and dibenzylatiooluene (BHT), the most extensively should
The every field such as oxidation resistanct fresh-keeping, medicine, health product, cosmetics and the article of everyday use for varieties of food items.Carry
Taking is that tea polyphenols produces and the first step of preparation, improves the extraction ratio of tea polyphenols the most at low cost, and protects
Hold the biological activity of tea polyphenols, be the bottleneck problem in producing.It is usually in commercial production after first Folium Camelliae sinensis being pulverized
Sieve, then extract with water or high concentration ethanol aqueous solution under the high temperature conditions.Used high-temp extracting method is deposited
Problem have: (1) energy consumption is high；(2) Product Activity low (tea polyphenols is oxidizable)；(3) extract is miscellaneous
Matter content is high (high temperature easily leaches impurity)；(4) subsequent purification is often, and tea polyphenols loss amount is big；(5)
Easy gelatinizing during tea-leaf power high-temp extracting, is difficult to filter；(6) high to equipment requirements.Therefore tea polyphenols is carried
The improvement of access method is significant with innovation.
Stevioside has excellent physiological property and stability, is widely used in as a kind of new food additive
The industries such as food, beverage, wine brewing, medicine, daily-use chemical industry, not only extraction process reaches its maturity, and extraction ratio is also
Day by day improve.The method extracting stevioside at present from Stevia leaves mainly has organic solvent extraction and water
Extraction method, wherein organic solvent extraction solvent consumption is big, cost is high, practicality is not good enough.Hot water extraction is
Application comparison extracting method widely at present, in industry, the general technology flow process of stevioside's water extraction is as follows: sweet
Ye Juye → water logging (8-10h) → coarse filtration → removing impurity by means of precipitation → fine straining → purification → decolouring → desalination → concentrate drying,
Wherein water logging extraction and purification are the committed step of this technique, and it is 80 DEG C that extracting process widely is compared in use
Hot water extracted many times, the method for purification now more uses resin absorption to separate, and the main active charcoal of method of decolouring takes off
Normal complexion resin decolorization two kinds.The shortcoming of this technique is that extraction time is long, and thermal energy consumption is high, and High Temperature High Pressure is to equipment
Processing safety requires height, and in purification and decolorization, seriality is poor, and resin and reagent dosage are big simultaneously, tree
Fat utilization rate is low, and operation is time-consuming long.
Working is liked to feel sleepy and is the most all annoying the working people of the overwhelming majority, causes the reason felt sleepy to have very
Many, main cause be evening sleep quality bad, also have in part because seasonal factor, such as spring sleepiness, it is
A kind of temporarily physiological phenomenon that natural climate, temperature go up and produces.People when cold winter and the early spring,
Being affected by low temperature, sweat gland of skin shrinks, and to reduce distributing of internal heat, keeps thermostasis.Enter the spring
In season, temperature raises, and skin pore is unfolded, and amount of blood supply increases, and the oxygen supplying brain reduces accordingly, brain work
Being affected, biological clock is the most accurate.Warm spring sun-light, magnetic field intensity increases, and body is the most right
These are reacted, the symptom of performance work exactly easily feel sleepy, tired.Spring, often from noon to afternoon,
" family of office " is the drowsiest, and " spring sleepiness " takes place frequently.In recent years, many white collars encounter identical being stranded
Disturb, then try every means and exchange experience, the invasion of opposing " spring sleepiness "." eat up lunch not all rightly the most tired
" having a meal after 12 noon half returns to office, eyes face toward computer screen, frankly, wholeheartedly only
The white collar that sleepy is felt is not within minority.For for a long time these people of office work, cervical vertebra is in flexing for a long time
Position or some special body position, and busy life allow they have no time motion, the space of closing often some
Symptom perplexs them, and when spring sleepiness occurs when, whole people becomes dispirited.Feel sleepy and do not only result in work
Inefficiency, and cause work being liked make a mistake.
It is presently used for the medicine refreshed oneself and beverage has a lot, wherein, although one can be reached by medicine effect of refreshing oneself
Fixed effect of refreshing oneself, but the mouthfeel of medicine is not good enough.By contrast, in beverage, tea good in taste, obtain wide
The favor of big consumer.Tea is a kind of famous health beverage, has an effect refreshed oneself, but the refreshing oneself of most tea
Acting on inconspicuous, the mouthfeel of some tea is not good enough, it is difficult to obtain the favor of consumer.
[summary of the invention]
The technical problem to be solved in the present invention is to provide a kind of refreshment Folium Ginkgo tea, to solve to make in prior art
Standby ginkgetin extraction ratio and active component are low, and technique is loaded down with trivial details, and the production cycle is long；The tea polyphenols activity of preparation is low
(tea polyphenols is oxidizable) and extract impurity content are high (high temperature easily leaches impurity)；Stevioside's purification and decolouring
During seriality poor, resin and reagent dosage are big, and resin utilization rate is low, the time-consuming problem such as long of operation.Institute
State that refreshment Folium Ginkgo tea extract through medicinal liquid, prepared by clear paste, prepared by pelletize, the step such as sterilizing.This
Bright Folium Ginkgo tea have the effects such as refreshment, make that beverage mouthfeel is good, taste is aromatic；The refreshment of the present invention
Folium Ginkgo tea are without any preservative and pigment, and pure natural plant refines elite, breach cold water and make tea technology,
Utilize low-temperature extraction technology, it is ensured that the active component in plant is not destroyed, and is easily absorbed by the body after drinking,
It is readily soluble and is easily solved the short slab of traditional product by absorption；The refreshment Folium Ginkgo tea frozen water of the present invention, cold water,
Brewed in hot water even can, unique flavor, facilitate all ages drunk by people.
In order to solve above technical problem, the present invention by the following technical solutions:
A kind of refreshment Folium Ginkgo tea, in units of weight portion, including following raw material: Flos Osmanthi Fragrantis 150-450 part,
Flos Chrysanthemi Indici 150-450 part, Herba Verbenae 150-450 part, Herba Abri 80-200 part, Herba Menthae 80-200 part, certainly
Pine torch 60-100 part, Fructus Gardeniae 60-100 part, malt extract stick with paste 30-60 part, ginkgetin 1-3 part, tea polyphenols
1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent 0.8-2 part, point
Powder 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5 part；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: Flos Osmanthi Fragrantis, Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae, Fructus Gardeniae are respectively dried rear powder
Broken, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, add the 2000-7500 abundant moistening of part water laggard
Row extracts, and the condition of extraction is: ultrasonic power is 120-180W, and Extracting temperature is 40-70 DEG C, during extraction
Between be 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, Folium Stevlae Rebaudianae after puckery
Glycoside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, at rotating speed be
Stirring 1-3min under 200-500r/min, be uniformly mixed liquid, concentrates the filtrate to temperature when being 64-66 DEG C
Relative density is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 is spray-dried to water content≤6% at temperature 200-220 DEG C, after pulverizing
Cross the sieve of 200-400 mesh, prepare powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water uses pelletize mechanism after being sufficiently mixed
Becoming granule, finally prepared described granule is 134-136 DEG C in temperature, pressure is 210-230KPa,
Time is sterilizing under 20-40s, obtains refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) water of 38-62 DEG C is used to extract the Ginkgo Leaf that step 1 prepares, solid-to-liquid ratio in extraction
For 1:12-14 (W/V), extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction,
Prepare mixing lixiviating solution；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 5.5-6
The water of 45-55 DEG C of times volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extraction 2-3 time, continuation
Carrying out repeatedly crystallization treatment with anhydrous ethyl acetate, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), system
Obtain crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, and extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, be the ethanol water of 40%-60% with mass fraction
Mix for 1:16-20 in mass ratio, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, mistake
Filter, merging filtrate, concentrate, prepare tea polyphenols crude extract；
(b) by step a prepare tea polyphenols crude extract join in KCl solution, pH regulator to 6.8-7.2,
Under centrifugal rotational speed is 4000-4500r/min, removes impurity, uses 0.45 μm filter membrane to be 34-36 DEG C in temperature
Under the solution after centrifugal is filtered, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) crossing 40-80 mesh sieve after being pulverized by Stevia leaves, be dipped in water immersion 1-1.2.h, solid-to-liquid ratio is
1:20-25 (W/V), is 100-120W at ultrasonic power, and Extracting temperature is 40-60 DEG C, extraction time
For extracting under 20-30min, prepare Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl of filtrate percentage by weight 0.8%-1%
(SO4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2,
At temperature 44-48 DEG C, stand 3.2-3.5h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 10%-25%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, condition
For: resolving agent is the ethanol solution of 55%-65%, and its consumption is 1-3 times of macroporous adsorbent resin volume, water
Washing district is deionized water, and absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, and adsorption zone is flowed
Speed 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity
6-8BV/h, switching time is 700-750s, and temperature is 40-50 DEG C, and pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, carry out at temperature is 200-220 DEG C
It is spray-dried, prepares stevioside.
Further, during described vitamin includes vitamin A, vitamin C, vitamin D and vitamin E
One or more.
Further, one during described thickening agent includes xanthan gum, guar gum, locust bean gum and locust bean gum or
Multiple.
Further, described cosolvent is polyvinylpyrrolidone.
Further, described dispersant includes following component: potassium carboxymethylcellulose, agar, modified starch,
One or more in polyacrylic acid potassium and potassium alginate.
Further, described antioxidant includes food grade antioxidant 9701, food grade antioxidant BHT, food
One in level antioxidant different VC potassium, food grade antioxidant BHA and food grade antioxidant MSK-NE150
Or it is multiple.
Further, one or more during described tasty agents includes inosinic acid potassium and guanyl potassium.
Further, described flavouring agent is methyl cyclopentenyl ketone.
Pharmacological action of the present invention is as follows:
Flos Osmanthi Fragrantis is that people's China ten great tradition loved by all views and admires one of famous flower.Additionally, Flos Osmanthi Fragrantis has the highest food
By value, it is common health food in autumn, is widely used as food seasoning by our people since ancient times.Flos Osmanthi Fragrantis
Or a kind of crude drug, acrid in the mouth warm in nature, have stomach invigorating, reduce phlegm, promote the production of body fluid, dissipate expectorant, the effect of suppressing the hyperactive liver, energy
Control abundant expectoration cough, hemorrhoidal hamorrhage dysentery, toothache halitosis, inappetence, amenorrhea stomachache.Further, Flos Osmanthi Fragrantis fragrance fragrance
Strongly fragrant grace, contains multiple bioactive ingredients simultaneously, has refreshment, inspires enthusiasm, tenderization skin, prolongs
The effects such as slow aging.
Chrysanthemum has more than 30 to plant, China originate in 17 kinds, mainly have: Herba Dendranthematis indici, Flos Chrysanthemi, Mao Huaju, Flos Chrysanthemi,
Little Chrysanthemum, pale reddish brown Herba Dendranthematis indici, Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) etc..For herbaceos perennial.Happiness is nice and cool, more cold-resistant, grows thermophilic
18-21 DEG C, underground rhizome is drought-enduring, avoids most long-pending flood, and happiness high-land, soil layer be deep, rich in humus, loose
Loam fertile, well-drained.Subacidity to alkalescence soil all can grow.And with pH6.2-6.7
Good.For short-day plant, nourish and grow under the long-day of 14.5 hours every days, 12 hours every days with
On dark be suitable to flower bud development with the temperature at night of 10 DEG C.Flos Chrysanthemi contains stachydrine, wood grass glycoside, cosmos
The compositions such as glycoside, gland fat purine, choline, glycoside, be especially enriched in volatile oil, and oil predominantly chrysanthanone,
The materials such as Borneolum Syntheticum, Borneolum Syntheticum caproate.Efficacy effect aspect, property is sweet, be slightly cold, have scattered wind heat, suppressing the hyperactive liver improving eyesight,
Disappear and cough effect of pain relieving, be used for treating the disease effects such as headache dizziness, conjunctival congestion and swelling pain, anemopyretic cold, cough and show
Write, also there is effect of refreshment.
Herba Verbenae have refresh oneself, mild emotion, eliminate exert one's utmost effort, the effect such as facilitating digestion, can control lump in the abdomen,
The diseases such as amenorrhea dysmenorrhea, malaria, sore throat, carbuncle, edema, pyretic stranguria.
Herba Abri contains abrine Semen Abri Precatorii Fructus Gleditsia, flavonoid, aminoacid, saccharide, and Semen Abri Precatorii soap alcohol is sweet
Grass time alkali, major function is heat-clearing and toxic substances removing, refreshment, the most also effect of diuretic damp eliminating.It addition, chicken
GUCAO has special efficacy to hepatitis, and often food can improve liver function.
Herba Menthae mainly containing the volatile oil component such as nettle lotus brain, menthone, have excited brain, blood circulation promoting,
Diaphoresis, with the effect of indometacin, anti-itch detoxification and dispelling wind and heat pathogens.
Semen Cassiae is a kind of Chinese medicinal herbs, study of semen cassia, is also Semen Cassiae, to go back gb 1, bullshit bean, vacation green
Bean, Horse hoof, Herba Senecionis Scandentis, leguminous herbaceous plant's Semen Cassiae or the mature seed of little Semen Cassiae, bitter in the mouth, Gan Erxing
Frightened, there is the functions such as clearing away liver-fire, wind-damp dispelling, tonifying kidney and improving eyesight.In addition to medicinal ingredient, Semen Cassiae is possibly together with multiple
Vitamin and abundant aminoacid, fat, carbohydrate etc., its health care is increasingly subject to people in recent years
Attention.
Fructus Gardeniae derives from the dry mature fruit of Maguireothamnus speciosus Fructus Gardeniae.Be applicable to affection due to external wind and heat type by table people it
The diseases such as flu, influenza, pneumonia, the conjunctival congestion headache caused by liver and gall excess-fire superinverse, hypochondriac pain bitter taste, otalgia tinnitus
And dampness-heat in the liver and gallbladder bet caused by stranguria with turbid discharge, cyst, the inferior disease of band, additionally, can be additionally used in calentura coma,
Refreshment, apoplectic hemiplegia, infective fever, acute, chronic hepatitis, pneumonia, upper respiratory tract infection and cerebral thrombosis,
The diseases such as cerebral hemorrhage.
Ginkgetin be from the leaf of " living fossil " ginkgo extract, be highly resistant to and prevent computer,
The infringement that human body is caused by the electromagnetic radiation such as mobile phone, the particularly protective effect to brain cell are obvious, also have
There is rubbish in vessel softening, removing blood, drop the effect such as three fat, removing free radical.
Tea polyphenols is extracting directly from a tender leaf of sieve tea and spring bud, has the strongest Scavenger of ROS and freedom
The effects such as base, control oxidase, elimination halitosis, protection vision.
Stevioside extracts from natural Stevia leaves, is a kind of to have high sugariness, crude sweet low in calories
Taste agent.It is eaten for a long time and people will not be made to get fat, and have certain regulation blood glucose function stevioside to have no side effect,
Non-carcinogenesis, noresidue, safe and reliable, the most edible can the disease such as prophylaxis of hypertension, heart disease, dental caries,
It is particularly well-suited to diabetics, phenyl ketonuria patient and the health care of obese people.Stevioside is current
The world it has been found that and through China's Ministry of Public Health, Ministry of Light Industry approval use the natural low grade fever closest to sucrose taste
Value sweeting agent, is that have Development volue and the healthy natural sucrose praised highly outside cane suger and beet sugar that continue replaces
Product, are described as " third place in the world sucrose ".
The method have the advantages that
(1) xanthan gum in the present invention, guar gum, locust bean gum, locust bean gum, can play thickening, hang
Floating effect, improves mouthfeel, makes mouthfeel smooth, improves the quality of refreshment Folium Ginkgo tea；
(2) present invention uses inosinic acid potassium, guanyl potassium, and delicate flavour can be made to increase several times, makes refreshment silver
Fructus Pruni tea has strong natural flavor；
(3) present invention uses cosolvent, the dissolving of the most each composition, makes solution mix homogeneously；
(4) present invention uses dispersant, and system can be made uniform, and suspendability increases, and does not precipitates, makes whole
System physico-chemical property is the same；
(5) present invention uses antioxidant, it is to avoid the materials such as tea polyphenols are during preparing refreshment Folium Ginkgo tea
Lose activity；
(6) present invention uses flavouring agent to cover abnormal flavour in refreshment Folium Ginkgo tea, improve refreshment Folium Ginkgo tea
Palatability；
(7) present invention extracts ginkgetin rate and active component is high, and technique is simple, with short production cycle；
(8) tea polyphenols activity and the extract impurity content that prepared by the present invention are high；
(9) in stevioside's purification of the present invention and decolorization, seriality is good, and resin and reagent dosage are little, tree
Fat utilization rate is high, operates the shortest；
(10) Folium Ginkgo tea of the present invention have the effects such as refreshment, make that beverage mouthfeel is good, taste is aromatic；
(11) compared with the Folium Ginkgo tea of traditional handicraft, the problems such as de-bitter detoxification are fully achieved, safely and effectively
The benefit of Semen Ginkgo is performed to ultimate attainment；
(12) the refreshment Folium Ginkgo tea of the present invention refine without any preservative and pigment, pure natural plant
Elite, breaches cold water and makes tea technology, utilize low-temperature extraction technology, it is ensured that the active component in plant is not subject to
Destroying, be easily absorbed by the body after drinking, it is readily soluble and is easily solved the short slab of traditional product by absorption；
(13) the refreshment Folium Ginkgo tea frozen water of the present invention, cold water, brewed in hot water even can, unique flavor, side
Just the drinking of each age level.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following instance, these examples belong to the present invention's
Protection domain, but it is not intended to protection scope of the present invention.
In an embodiment, refreshment Folium Ginkgo tea, in units of weight portion, including following raw material: Flos Osmanthi Fragrantis 150-450
Part, Flos Chrysanthemi Indici 150-450 part, Herba Verbenae 150-450 part, Herba Abri 80-200 part, Herba Menthae 80-200 part,
It is many that Semen Cassiae 60-100 part, Fructus Gardeniae 60-100 part, malt extract stick with paste 30-60 part, ginkgetin 1-3 part, tea
Phenol 1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent 0.8-2 part,
Dispersant 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5 part；
Described vitamin includes the one in vitamin A, vitamin C, vitamin D and vitamin E or many
Kind；
Described thickening agent includes one or more in xanthan gum, guar gum, locust bean gum and locust bean gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant includes following component: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium
With one or more of potassium alginate；
Described antioxidant includes that food grade antioxidant 9701, food grade antioxidant BHT, food grade antioxidant are different
One or more in VC potassium, food grade antioxidant BHA and food grade antioxidant MSK-NE150；
Described tasty agents includes one or more in inosinic acid potassium and guanyl potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: Flos Osmanthi Fragrantis, Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae and Fructus Gardeniae are respectively dried rear powder
Broken, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, after adding 2000-7500 part abundant moistening of water water
Extracting, the condition of extraction is: ultrasonic power is 120-180W, and Extracting temperature is 40-70 DEG C, extracts
Time is 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, Folium Stevlae Rebaudianae after puckery
Glycoside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, at rotating speed be
Stirring 1-3min under 200-500r/min, be uniformly mixed liquid, concentrates the filtrate to temperature when being 64-66 DEG C
Relative density is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 is spray-dried to water content≤6% at temperature 200-220 DEG C, after pulverizing
Cross the sieve of 200-400 mesh, prepare powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water uses pelletize mechanism after being sufficiently mixed
Becoming granule, finally prepared described granule is 134-136 DEG C in temperature, pressure is 210-230KPa,
Time is sterilizing under 20-40s, obtains refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) water of 38-62 DEG C is used to extract the Ginkgo Leaf that step 1 prepares, solid-to-liquid ratio in extraction
For 1:12-14 (W/V), extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction,
Prepare mixing lixiviating solution；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 5.5-6
The water of 45-55 DEG C of times volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extraction 2-3 time, continuation
Carrying out repeatedly crystallization treatment with anhydrous ethyl acetate, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), system
Obtain crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, and extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, be the ethanol water of 40%-60% with mass fraction
Mix for 1:16-20 in mass ratio, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, mistake
Filter, merging filtrate, concentrate, prepare tea polyphenols crude extract；
(b) by step a prepare tea polyphenols crude extract join in KCl solution, pH regulator to 6.8-7.2,
Under centrifugal rotational speed is 4000-4500r/min, removes impurity, uses 0.45 μm filter membrane to be 34-36 DEG C in temperature
Under the solution after centrifugal is filtered, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water immersion 1-1.2.h after being pulverized by Stevia leaves, solid-to-liquid ratio is 1:20-25 (W/V),
Being 100-120W at ultrasonic power, Extracting temperature is 40-60 DEG C, and extraction time is to extract under 20-30min,
Prepare Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl of filtrate percentage by weight 0.8%-1%
(SO4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2,
At temperature 44-48 DEG C, stand 3.2-3.5h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 10%-25%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, condition
For: resolving agent is the ethanol solution of 55%-65%, and its consumption is 1-3 times of macroporous adsorbent resin volume, water
Washing district is deionized water, and absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, and adsorption zone is flowed
Speed 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity
6-8BV/h, switching time is 700-750s, and temperature is 40-50 DEG C, and pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, carry out at temperature is 200-220 DEG C
It is spray-dried, prepares stevioside.
Below by more specifically embodiment, the present invention will be described.
Embodiment 1
A kind of refreshment Folium Ginkgo tea, in units of weight portion, including following raw material: Flos Osmanthi Fragrantis 300 parts, Herba Dendranthematis indici
Spend 300 parts, Herba Verbenae 300 parts, Herba Abri 130 parts, Herba Menthae 130 parts, Semen Cassiae 80 parts, Fructus Gardeniae 80
Part, malt extract stick with paste 50 parts, ginkgetin 2 parts, tea polyphenols 2 parts, stevioside 2 parts, vitamin 2 parts,
Thickening agent 1.5 parts, cosolvent 1.5 parts, dispersant 1.5 parts, 1.5 parts of antioxidant, tasty agents 1 part, fragrance
Agent 1 part；
Described vitamin is vitamin A, vitamin C, vitamin D, vitamin E；
Described thickening agent is xanthan gum, guar gum, locust bean gum, locust bean gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: potassium carboxymethylcellulose, agar, modified starch；
Described antioxidant is food grade antioxidant different VC potassium, food grade antioxidant BHA, food grade antioxidant
MSK-NE150；
Described tasty agents is inosinic acid potassium, guanyl potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: by Flos Osmanthi Fragrantis；Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae, Fructus Gardeniae, be respectively dried after
Pulverize, cross 60 mesh sieves, put in ultrasonic extraction equipment, extract after adding 5000 parts of abundant moistenings of water,
The condition extracted is: ultrasonic power is 150W, and Extracting temperature is 100 DEG C, and extraction time is 50min；
S2: step S1 is extracted medical filtration, except add after puckery ginkgetin, tea polyphenols, stevioside,
Vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, be 300r/min at rotating speed
Lower stirring 2min, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 65 DEG C is 1.35
Clear paste；
S3: being spray-dried at 210 DEG C by the clear paste of step S2 to water content is 5%, crosses 300 mesh after pulverizing
Sieve, prepare powder；
S4: stuck with paste with malt extract by the powder of step S3,80 parts of water mix and make granule, finally system
The described granule obtained is 135 DEG C in temperature, and pressure is 220KPa, and the time is sterilizing under 30s, prepares and refreshes oneself
Refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 60 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) using the water of 50 DEG C to extract the Ginkgo Leaf that step 1 prepares, in extraction, solid-to-liquid ratio is
1:13 (W/V), extraction time is 3h, extracts 2 times, filtration, merging filtrate after extraction, prepares mixing leaching
Extract；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 5.8
The water of 50 DEG C of times volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extracting 2 times, continues to use nothing
Water ethyl acetate carries out repeatedly crystallization treatment, and in crystallization process, solid-to-liquid ratio is 1:5.3 (W/V), prepares crystallization
Crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 15MPa, and extraction temperature is 43 DEG C, and extraction time is 36min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 60 mesh sieves, with the ethanol water that mass fraction is 50% in mass ratio after group's sieve tea pulverizing
Mix for 1:18, extract 2 times at temperature is 38 DEG C, each 25min, filter, merging filtrate, concentrate,
Prepare tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator to 7,
Centrifugal rotational speed is removing impurity under 4200r/min, after using 0.45 μm filter membrane to being centrifuged at temperature is 35 DEG C
Solution filter, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water immersion 1.1h after being pulverized by Stevia leaves, solid-to-liquid ratio is 1:22 (W/V),
Ultrasonic power is 110W, and Extracting temperature is 50 DEG C, and extraction time is to extract under 25min, prepares Folium Stevlae Rebaudianae
Medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 150 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl of filtrate percentage by weight 0.9%
(SO4)2Ca (OH) with filtrate percentage by weight 1.2%2, adjusting pH value is 7, temperature 46 DEG C
Under, stand 3.3h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 32%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, and condition is:
Resolve agent be the ethanol solution of 60%, its consumption is 2 times of macroporous adsorbent resin volume, water wash zone for go from
Sub-water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 3%, adsorption zone flow velocity 8BV/h, solves
Inhaling district flow velocity 18BV/h, water wash zone flow velocity 22BV/h, renewing zone flow velocity 7BV/h, switching time is 720s,
Temperature is 45 DEG C, and pressure is 0.7MPa；
(E) stevioside's liquid that step D prepares is concentrated, spray at temperature is 210 DEG C
It is dried, prepares stevioside.
Embodiment 2
A kind of refreshment Folium Ginkgo tea, in units of weight portion, including following raw material: Flos Osmanthi Fragrantis 150 parts, Herba Dendranthematis indici
Spend 150 parts, Herba Verbenae 150 parts, Herba Abri 80 parts, Herba Menthae 80 parts, Semen Cassiae 60 parts, Fructus Gardeniae 60 parts,
Malt extract paste 30 parts, ginkgetin 1 part, tea polyphenols 1 part, stevioside 1 part, vitamin 1 part, increasing
Thick dose 0.8 part, cosolvent 0.8 part, dispersant 0.8 part, 0.8 part of antioxidant, tasty agents 0.5 part, fragrance
Agent 0.5 part；
Described vitamin is vitamin；
Described thickening agent is xanthan gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: modified starch, polyacrylic acid potassium and potassium alginate；
Described antioxidant is food grade antioxidant 9701；
Described tasty agents is inosinic acid potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: by Flos Osmanthi Fragrantis；Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae, Fructus Gardeniae, be respectively dried after
Pulverize, cross 40 mesh sieves, put in ultrasonic extraction equipment, extract after adding 2000 parts of abundant moistenings of water,
The condition extracted is: ultrasonic power is 120W, and Extracting temperature is 40 DEG C, and extraction time is 60min；
S2: step S1 is extracted medical filtration, except add after puckery ginkgetin, tea polyphenols, stevioside,
Vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, be 200r/min at rotating speed
Lower stirring 3min, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 64 DEG C is 1.32
Clear paste；
S3: being spray-dried at 200 DEG C by the clear paste of step S2 to water content is 6%, crosses 200 mesh after pulverizing
Sieve, prepare powder；
S4: stuck with paste with malt extract by the powder of step S3,50 parts of water mix and make granule, finally system
The described granule obtained is 134 DEG C in temperature, and pressure is 210KPa, and the time is sterilizing under 40s, prepares and refreshes oneself
Refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 40 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) using the water of 38 DEG C to extract the Ginkgo Leaf that step 1 prepares, in extraction, solid-to-liquid ratio is
1:12 (W/V), extraction time is 3.5h, extracts 2 times, filtration, merging filtrate after extraction, prepares mixing
Lixiviating solution；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 5.5
The water of 45 DEG C of times volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extracting 2 times, continues to use nothing
Water ethyl acetate carries out repeatedly crystallization treatment, and in crystallization process, solid-to-liquid ratio is 1:5.2 (W/V), prepares crystallization
Crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 12MPa, and extraction temperature is 42 DEG C, and extraction time is 40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40 mesh sieves, with the ethanol water that mass fraction is 40% in mass ratio after group's sieve tea pulverizing
Mix for 1:16, extract 2 times at temperature is 36 DEG C, each 30min, filter, merging filtrate, concentrate,
Prepare tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator to 6.8,
Under centrifugal rotational speed is 4000-/min, removes impurity, uses 0.45 μm filter membrane to centrifugal at temperature is 34 DEG C
After solution filter, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water immersion 1h after being pulverized by Stevia leaves, solid-to-liquid ratio is 1:20 (W/V), super
Acoustic power is 100W, and Extracting temperature is 40 DEG C, and extraction time is to extract under 30min, prepares Folium Stevlae Rebaudianae medicine
Liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl of filtrate percentage by weight 0.8%
(SO4)2Ca (OH) with filtrate percentage by weight 1%2, adjusting pH value is 6.8, temperature 44 DEG C
Under, stand 3.2-3.5h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 10%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, and condition is:
Resolving agent is the ethanol solution of 55%, and its consumption is 1 times of macroporous adsorbent resin volume, and water wash zone is deionization
Water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%, adsorption zone flow velocity 6BV/h, desorbing
District flow velocity 15BV/h, water wash zone flow velocity 20BV/h, renewing zone flow velocity 6BV/h, switching time is 700s, temperature
Degree is 40 DEG C, and pressure is 0.4MPa；
(E) stevioside's liquid that step D prepares is concentrated, spray at temperature is 200 DEG C
It is dried, prepares stevioside.
Embodiment 3
A kind of refreshment Folium Ginkgo tea, in units of weight portion, including following raw material: Flos Osmanthi Fragrantis 450 parts, Herba Dendranthematis indici
Spend 450 parts, Herba Verbenae 450 parts, Herba Abri 200 parts, Herba Menthae 200 parts, Semen Cassiae 100 parts, Fructus Gardeniae
100 parts, malt extract stick with paste 60 parts, ginkgetin 3 parts, tea polyphenols 3 parts, stevioside 3 parts, vitamin 3
Part, thickening agent 2 parts, cosolvent 2 parts, dispersant 2 parts, 2 parts of antioxidant, tasty agents 1.5 parts, fragrance
1.5 part；
Described vitamin is vitamin C；
Described thickening agent is guar gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: potassium carboxymethylcellulose, modified starch, potassium alginate；
Described antioxidant is food grade antioxidant BHT；
Described tasty agents is inosinic acid potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: by Flos Osmanthi Fragrantis；Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae, Fructus Gardeniae are respectively dried rear powder
Broken, cross 60 mesh sieves, put in ultrasonic extraction equipment, extract after adding 7500 parts of abundant moistenings of water,
The condition extracted is: ultrasonic power is 180W, and Extracting temperature is 70 DEG C, and extraction time is 30min；
S2: step S1 is extracted medical filtration, except add after puckery ginkgetin, tea polyphenols, stevioside,
Vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, be 500r/min at rotating speed
Lower stirring 1min, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 66 DEG C is 1.38
Clear paste；
S3: being spray-dried at 220 DEG C by the clear paste of step S2 to water content is 4%, crosses 400 mesh after pulverizing
Sieve, prepare powder；
S4: stuck with paste with malt extract by the powder of step S3,100 parts of water mix and make granule, finally handle
The described granule prepared is 136 DEG C in temperature, and pressure is 230KPa, and the time is sterilizing under 40s, prepares and carries
God's refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) using the water of 62 DEG C to extract the Ginkgo Leaf that step 1 prepares, in extraction, solid-to-liquid ratio is
1:14 (W/V), extraction time is 2.5h, extracts 3 times, filtration, merging filtrate after extraction, prepares mixing
Lixiviating solution；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 6 times
The water of 55 DEG C of volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extracting 3 times, continues with anhydrous
Ethyl acetate carries out repeatedly crystallization treatment, and in crystallization process, solid-to-liquid ratio is 1:5.4 (W/V), prepares crystallization thick
Product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 18MPa, and extraction temperature is 45 DEG C, and extraction time is 32min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 80 mesh sieves, with the ethanol water that mass fraction is 60% in mass ratio after group's sieve tea pulverizing
Mix for 1:20, extract 3 times at temperature is 40 DEG C, each 20min, filter, merging filtrate, concentrate,
Prepare tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator to 7.2,
Under centrifugal rotational speed is 4500r/min, removes impurity, uses 0.45 μm filter membrane to centrifugal at temperature is 36 DEG C
After solution filter, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water immersion 1.2h after being pulverized by Stevia leaves, solid-to-liquid ratio is 1:25 (W/V),
Ultrasonic power is 120W, and Extracting temperature is 60 DEG C, and extraction time is to extract under 20min, prepares Folium Stevlae Rebaudianae
Medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 180 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl (SO of filtrate percentage by weight 1%4)2Ca (OH) with filtrate percentage by weight 1.4%2, adjusting pH value is 7.2, at temperature 48 DEG C, quiet
Put 3.2-3.5h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 25%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, and condition is:
Resolve agent be the ethanol solution of 65%, its consumption is 3 times of macroporous adsorbent resin volume, water wash zone for go from
Sub-water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 4%, adsorption zone flow velocity 10BV/h, solves
Inhaling district flow velocity 20BV/h, water wash zone flow velocity 25BV/h, renewing zone flow velocity 8BV/h, switching time is 750s,
Temperature is 50 DEG C, and pressure is 0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, spray at temperature is 220 DEG C
It is dried, prepares stevioside.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanation, for skill belonging to the present invention
For the those of ordinary skill in art field, without departing from the inventive concept of the premise, it is also possible to make some letters
Single deduction or replace, all should be considered as belonging to the patent protection model that the present invention is determined by the claims submitted to
Enclose.
Claims (8)
1. refreshment Folium Ginkgo tea, it is characterised in that in units of weight portion, including following raw material: osmanthus
Flower 150-450 part, Flos Chrysanthemi Indici 150-450 part, Herba Verbenae 150-450 part, Herba Abri 80-200 part, Herba Menthae
80-200 part, Semen Cassiae 60-100 part, Fructus Gardeniae 60-100 part, malt extract stick with paste 30-60 part, ginkgetin 1-3
Part, tea polyphenols 1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent
0.8-2 part, dispersant 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5
Part；
The preparation method of described refreshment Folium Ginkgo tea, comprises the following steps:
S1: Flos Osmanthi Fragrantis, Flos Chrysanthemi Indici, Herba Verbenae, Herba Abri, Herba Menthae, Semen Cassiae, Fructus Gardeniae are respectively dried rear powder
Broken, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, add the 2000-7500 abundant moistening of part water laggard
Row extracts medicinal liquid, and the condition of extraction is: ultrasonic power is 120-180W, and Extracting temperature is 40-70 DEG C, carries
The time of taking is 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, Folium Stevlae Rebaudianae after puckery
Glycoside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent, at rotating speed be
Stirring 1-3min under 200-500r/min, be uniformly mixed liquid, concentrates the filtrate to temperature when being 64-66 DEG C
Relative density is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 is spray-dried to water content≤6% at temperature 200-220 DEG C, after pulverizing
Cross the sieve of 200-400 mesh, prepare powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water uses pelletize mechanism after being sufficiently mixed
Becoming granule, finally prepared described granule is 134-136 DEG C in temperature, pressure is 210-230KPa,
Time is sterilizing under 20-40s, obtains refreshment Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) carry out pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) water of 38-62 DEG C is used to extract the Ginkgo Leaf that step 1 prepares, solid-to-liquid ratio in extraction
For 1:12-14 (W/V), extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction,
Prepare mixing lixiviating solution；
(3) mixing lixiviating solution concentrate drying step 2 prepared, prepares extraction cream, is used in extraction cream 5.5-6
The water of 45-55 DEG C of times volume dissolves, and uses anhydrous ethyl acetate solvent to carry out extraction 2-3 time, continuation
Carrying out repeatedly crystallization treatment with anhydrous ethyl acetate, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), system
Obtain crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extraction, the condition of extraction: extraction kettle
Pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, and extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, be the ethanol water of 40%-60% with mass fraction
Mix for 1:16-20 in mass ratio, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, mistake
Filter, merging filtrate, concentrate, prepare tea polyphenols crude extract；
(b) by step a prepare tea polyphenols crude extract join in KCl solution, pH regulator to 6.8-7.2,
Under centrifugal rotational speed is 4000-4500r/min, removes impurity, uses 0.45 μm filter membrane to be 34-36 DEG C in temperature
Under the solution after centrifugal is filtered, prepare filtrate；
C filtrate ether extraction that step b is prepared by (), freezing, prepare tea polyphenols after drying；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water immersion 1-1.2.h after being pulverized by Stevia leaves, solid-to-liquid ratio is 1:20-25 (W/V),
Being 100-120W at ultrasonic power, Extracting temperature is 40-60 DEG C, and extraction time is to extract under 20-30min,
Prepare Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 mesh, prepares Folium Stevlae Rebaudianae filtrate；
(C) the Folium Stevlae Rebaudianae filtrate prepared to step B adds the NaAl of filtrate percentage by weight 0.8%-1%
(SO4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2,
At temperature 44-48 DEG C, stand 3.2-3.5h, prepare the solution after the removal of impurity；
(D) containing sweetleaf during the solution filter after removal of impurity step C prepared is filtered and concentrated to every milliliter
Chrysanthemum glycoside 10%-25%, uses macroporous adsorbent resin ADS-8 separating-purifying to prepare the liquid of stevioside, condition
For: resolving agent is the ethanol solution of 55%-65%, and its consumption is 1-3 times of macroporous adsorbent resin volume, water
Washing district is deionized water, and absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, and adsorption zone is flowed
Speed 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity
6-8BV/h, switching time is 700-750s, and temperature is 40-50 DEG C, and pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, carry out at temperature is 200-220 DEG C
It is spray-dried, prepares stevioside.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described vitamin includes that dimension is raw
One or more in element A, vitamin C, vitamin D and vitamin E.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described thickening agent includes xanthan
One or more in glue, guar gum, locust bean gum and locust bean gum.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described cosolvent is polyethylene
Ketopyrrolidine.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described dispersant includes following
Composition: the one or many in potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium and potassium alginate
Kind.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described antioxidant includes food
Level antioxidant 9701, food grade antioxidant BHT, food grade antioxidant different VC potassium, food grade antioxidant BHA
With one or more in food grade antioxidant MSK-NE150.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described tasty agents includes inosine
One or more in acid potassium and guanyl potassium.
Refreshment Folium Ginkgo tea the most according to claim 1, it is characterised in that described flavouring agent is methyl ring
Amylene alcohol ketone.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107996935A (en) * | 2017-12-06 | 2018-05-08 | 安徽省达亿粮油食品有限公司 | One kind refresh the mind defatted wheat germ bag bubble solid beverage |
| CN109984233A (en) * | 2019-03-27 | 2019-07-09 | 福建省农业科学院农业生态研究所 | One kind refreshes the mind tea and preparation method thereof |
| CN112797758A (en) * | 2021-01-05 | 2021-05-14 | 江西众源药业有限公司 | A raw materials drying equipment for cortex acanthopanacis medicinal liquor production and processing |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101717418A (en) * | 2009-12-10 | 2010-06-02 | 黑龙江省农产品加工工程技术研究中心 | Technology for separating stevioside in one step with simulated moving bed |
| CN103719488A (en) * | 2013-12-25 | 2014-04-16 | 广西博士海意信息科技有限公司 | Eyesight-improving refreshing fruit tea and preparation method thereof |
| CN103734414A (en) * | 2013-12-20 | 2014-04-23 | 晓健科技（大连）有限公司 | Slimming single-formula herbal tea |
| CN104387356A (en) * | 2013-11-15 | 2015-03-04 | 广西莱吉生物工程有限公司 | Method for extracting flavone from folium ginkgo |
| CN104431161A (en) * | 2014-11-19 | 2015-03-25 | 繁昌县丹韵电子商务有限公司 | Tea for improving eyesight, refreshing, protecting against cold and warming stomach and preparation method of tea |
-
2016
- 2016-05-12 CN CN201610317374.5A patent/CN105994735A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101717418A (en) * | 2009-12-10 | 2010-06-02 | 黑龙江省农产品加工工程技术研究中心 | Technology for separating stevioside in one step with simulated moving bed |
| CN104387356A (en) * | 2013-11-15 | 2015-03-04 | 广西莱吉生物工程有限公司 | Method for extracting flavone from folium ginkgo |
| CN103734414A (en) * | 2013-12-20 | 2014-04-23 | 晓健科技（大连）有限公司 | Slimming single-formula herbal tea |
| CN103719488A (en) * | 2013-12-25 | 2014-04-16 | 广西博士海意信息科技有限公司 | Eyesight-improving refreshing fruit tea and preparation method thereof |
| CN104431161A (en) * | 2014-11-19 | 2015-03-25 | 繁昌县丹韵电子商务有限公司 | Tea for improving eyesight, refreshing, protecting against cold and warming stomach and preparation method of tea |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107996935A (en) * | 2017-12-06 | 2018-05-08 | 安徽省达亿粮油食品有限公司 | One kind refresh the mind defatted wheat germ bag bubble solid beverage |
| CN109984233A (en) * | 2019-03-27 | 2019-07-09 | 福建省农业科学院农业生态研究所 | One kind refreshes the mind tea and preparation method thereof |
| CN112797758A (en) * | 2021-01-05 | 2021-05-14 | 江西众源药业有限公司 | A raw materials drying equipment for cortex acanthopanacis medicinal liquor production and processing |
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