CN103520036B - Hair-loss-preventing shampoo - Google Patents

Hair-loss-preventing shampoo Download PDF

Info

Publication number
CN103520036B
CN103520036B CN201310475889.4A CN201310475889A CN103520036B CN 103520036 B CN103520036 B CN 103520036B CN 201310475889 A CN201310475889 A CN 201310475889A CN 103520036 B CN103520036 B CN 103520036B
Authority
CN
China
Prior art keywords
hair
chinese medicine
parts
loss
weight portion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201310475889.4A
Other languages
Chinese (zh)
Other versions
CN103520036A (en
Inventor
刘友佳
陈勇
车丽
张鹏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUNAN JINHAO CAMELLIA OIL CO Ltd
Original Assignee
HUNAN JINHAO CAMELLIA OIL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HUNAN JINHAO CAMELLIA OIL CO Ltd filed Critical HUNAN JINHAO CAMELLIA OIL CO Ltd
Priority to CN201310475889.4A priority Critical patent/CN103520036B/en
Publication of CN103520036A publication Critical patent/CN103520036A/en
Application granted granted Critical
Publication of CN103520036B publication Critical patent/CN103520036B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Cosmetics (AREA)

Abstract

Disclosed hair-loss-preventing shampoo relates to the technical field of edible grease processing, and is prepared from the following raw materials in parts by weight: 15-18 parts of 70% AESA, 8-10 parts of 70% SLA, 5-8 part sof 35% CAB, 1-2 parts of 95% CMEA, 2-3 parts of 6501, 5-5.7 parts of 2% guar gum, 0.5-1.5 parts of a pearlescing agent, 1-1.5 parts of an antibacterial itch-relieving agent, 0.05-0.1 part of kathon, 0.5-1 part of camellia essence, 20-26 parts of traditional Chinese medicine extract, 15-18 parts of 60% tea saponin solution, the balance water, and the total amount of the above components is 100 parts. The hair-loss-preventing shampoo has the characteristics of being relatively strong in foaming capacity and decontamination capacity, capable of moistening and tonifying hair, capable of preventing hair loss, and the like; and the hair-loss-preventing shampoo is applicable to hair washing of male and female adults, and is applicable to treat and prevent hair loss.

Description

A kind of Hair-loss-preventingshampoo shampoo
Technical field
The present invention relates to daily-use chemical industry technical field, particularly a kind of Hair-loss-preventingshampoo shampoo.
Technical background
With the quickening pace of modern life, and being on the rise of environmental pollution, the alopecia of modern is more and more serious.Alopecia not only affects attractive in appearance, also affects living environment, even affects the mental status of people.At present, shampoo is on the market a feast for the eyes, has various effect, although there is this shampoo also to have effect of Anti-hair loss, great majority are all with the addition of more chemical substance, thus very easily sensitization.Also some Anti-hair loss hair washing products utilizing effective components of Chinese medicinal to prepare had been there is in recent years, as Chinese patent (number of patent application 201110387707.9) " for anti-loss shampoo and preparation method thereof ", it is be prepared from by following raw materials in parts by weight number ratio: Fructus Ligustri Lucidi 10-20 part, Rhizoma Zingiberis Recens 15-25 part, Rhizoma Gastrodiae 20-30 part, Radix Astragali 10-25 part, Radix Salviae Miltiorrhizae 10-30 part, Radix Angelicae Sinensis 15-35 part, Radix Rehmanniae 30-45 part, Radix Polygoni Multiflori 30-50 part, Semen Sesami Nigrum 20-40 part, essence 10-20 part, pure water 800-1000 part; This invention thoroughly can remove the dirty thing of the sebum deposition in pore, suppresses alopecia, promotes hair regeneration, cultivates and improves germinal cell activity and hair follicle environment, activate hair follicle, consolidate the consolidation of root of hair; Impel root of hair swell, greatly meet the object that user is anti-loss.And for example Chinese patent (number of patent application 201210142407.9) " has compound Chinese medicine extract of Anti-hair loss effect and preparation method thereof and application ", and this compound Chinese medicine extract is prepared by 40 ~ 65 mass parts Radix Polygoni Multiflori, 35 ~ 45 mass parts Herba Ecliptaes and 10 ~ 30 mass parts Radixs Astragali; This invention uses ZLUPD High Pressure Difference continuous low-temperature high efficiency extraction device to extract; Rationally, the compound Chinese medicine extract obtained has enrich and benefit essence and blood, black one of the main divisions of the male role in traditional opera sends out, effect of inhibiting bacteria and diminishing inflammation, can effectively improve skin of head microcirculating state, promotes the metabolism cycle of hair, adds the vitality of hair in the raw medicinal material collocation of this invention.Preparation method of the present invention overcomes length consuming time in Chinese medicine extracting method, effective component extracting is unstable, extraction efficiency is not high shortcoming; And utilize micro-filtration membrane isolation technics to filter extracting solution, can effectively remove macromole impurity, more retain effective ingredient.This preparation method can greatly reduce the consumption of Extraction solvent, and time-saving energy-saving reduces costs, and realizes continuous prodution.
Technology contents
The object of the present invention is to provide a kind of foaming power and detergency comparatively strong, there is the effects such as moist, maintenance hair quality, shampoo that can be anti-loss.
For realizing its object, the technical solution used in the present invention is a kind of Hair-loss-preventingshampoo shampoo of invention, is be prepared from by following raw material by weight:
Its preparation process is: 60% tea saponin solution of above-mentioned weight portion and pure water are mixed, be heated to 70-90 DEG C, keeps 4-6min, then adds the 70%AESA of above-mentioned weight portion, stirs; After 70%AESA dissolves, then add 35%CAB, the 70%SLA, 6501 of above-mentioned weight portion, maintain the temperature at 60-80 DEG C, be stirred to and dissolve completely; Then be cooled to 53-58 DEG C, then add after the Chinese medicine extraction liquid of above-mentioned weight portion, 2% guar gum, 95%CMEA mix homogeneously, continue to stir; In time being cooled to 48-52 DEG C, the pearlescent flake of above-mentioned weight portion, anti-bacterial, anti-itching agent, Kazon, Flos Camelliae Japonicae essence being added and stirs evenly, then regulate pH value to 6.0-6.5 with 20% citric acid; Continue to stir, be cooled to 35-45 DEG C;
Described Chinese medicine extraction liquid is prepared from by following raw material of Chinese medicine by weight:
Radix Sophorae Flavescentis 3-6 Radix Salviae Miltiorrhizae 2-5 Radix Polygoni Multiflori Preparata 6-12 Herba Agrimoniae 4-8
Pseudobulbus Bletillae (Rhizoma Bletillae) 2-5 Radix Astragali 3-6 Herba Ecliptae 4-8 Fructus Viticis 6-10.
The first preparation method of described Chinese medicine extraction liquid is: after the raw material of Chinese medicine washed with de-ionized water of above-mentioned weight portion is clean, moisture is dried to lower than 5% at 100-110 DEG C, then pulverize, cross 10-30 mesh sieve, again according to the part by weight of solid-liquid ratio 1:4-6, adding volumetric concentration is the ethanol of 50%, stirs; Then, soak 45-50 hour at normal temperatures and pressures, filter; Again filtrate is adopted the method for concentrating under reduced pressure, be concentrated into without alcohol, obtain required Chinese medicine extraction liquid.
The second preparation method of described Chinese medicine extraction liquid is: after being cleaned up by the raw material of Chinese medicine water of above-mentioned weight portion, add clear water according to the part by weight of solid-liquid ratio 1:1-3, boils and extracts 0.5-1.5 hour, filters, obtains an extracting solution; Add clear water according to the part by weight of solid-liquid ratio 1:1-2 again, boil and extract 0.5-1 hour, filter, obtain secondary raffinate; Merge extracted twice liquid, adopt the method for vacuum concentration, be concentrated into the half of merge extractive liquid, original volume, obtain required Chinese medicine extraction liquid.
The first preparation method of described 60% tea saponin solution is: get respectively by weight net content be 95% tea saponin 6.3 parts, volumetric concentration be 90% ethanol 10 parts, be placed in container mix homogeneously, be heated with stirring to 60-70 DEG C, until completely dissolved, be cooled to room temperature, obtain 60% required tea saponin solution.
The second preparation method of described 60% tea saponin solution is: the cake of camellia oleifera seeds raw material getting constant weight, is dried to moisture lower than 5%, then pulverizes at 100-110 DEG C, crosses 30-50 mesh sieve; Remove contained Residual oil again; According to the part by weight of solid-liquid ratio 1:4-6, being soaked in volumetric concentration is in the ethanol of 90%, stirs, again by its temperature increase to 60-70 DEG C, start ultrasonic cell disruptor extract 1-3 hour, filter, so repeat extraction three times, merging three filtrates is merging filtrate; Measure the content of tea saponin in merging filtrate again, and adopt the mode of adding aquiferous ethanol or being concentrated by merging filtrate, in adjustment merging filtrate, the content of tea saponin reaches 60%, obtains 60% tea saponin solution.
Hair-loss-preventingshampoo shampoo of the present invention, the main raw material(s) adopted comprises:
A, 70%AESA(be namely: content is the alkylpolyoxyethylene ammonium sulfate of 70%): foaming abundancy is fine and smooth, strong detergency, and biological degradability is good; There is good anti-performance of hard water; Degreasing power is moderate; For shampoo, having good cardability and skin comfort, is the surfactant that the present invention is main;
B, 70%SLA(be namely: content is the sodium laurate of 70%): have fabulous foaming capacity and low degreasing power, zest is low, is surfactant of the present invention;
C, 35%CAB(be namely: content is the cellulose acetate butyrate of 35%): have excellent moisture-resisting, ultraviolet resistance, the performance such as cold-resistant, pliable and tough, transparent are neutral surface active agent of the present invention and foaming agent;
D, 95%CMEA(be namely: the coconut monoethanolamide that content is greater than 95%): there are excellent thickening property and foam stability, are mainly used in thickening in the present invention and bubble;
E, 6501(be namely: cocoanut oil diethan olamide): there is good foaming, steady bubble, function such as infiltration decontamination, anti-hard water etc., use as surfactant compound in the present invention;
F, 2% guar gum (that is: content is the guar gum of 2%): there is good stabilizing agent, low irritant and thickening agent, excellent antistatic behaviour and opsonic action can be presented after being adsorbed in hair, improve the wet comb of hair;
G, pearlescent flake: in shampoo system, form pearly-lustre, give product pearl effect;
H, anti-bacterial, anti-itching agent (can adopt content be 50% hd-303 Gan Baolu or Triclosan or KF88 KF-88 etc.): multiple fungus can be suppressed, especially have unique effect to the fungus-oval scurf sporeformer producing human body scurf, reason is not hydrolyzed and causes stimulation to scalp;
I, Kazon: the sterilization antiseptic being a kind of broad-spectrum, can effectively algae, antibacterial and fungus, uses in the present invention as antiseptic;
J, 20% citric acid (that is: content is the citric acid of 20%): cutin can be accelerated and upgrade, contribute to melanic in skin peeling off, the receipts of pore are thin, the dissolving of blackhead; Also there is sterilization, antisepsis; Consumption is less in the present invention, is mainly used in the pH value adjusting shampoo;
K, Flos Camelliae Japonicae essence: give this product distinct unique fragrance;
L, tea saponin (60% tea saponin solution refers to that tea saponin content is the solution of 60%): the natural nonionic surfactant being a kind of function admirable, it has foaming, emulsifying, dispersion, the performance such as gentle, and has the pharmacological action of the aspects such as impervious, antiinflammatory, analgesia; Be commonly used to manufacture various types of emulsifying agent, detergent, foam, antiseptic, insecticide and other medicaments;
Chinese medicine included by its Chinese medicine extraction liquid has:
M, Radix Sophorae Flavescentis (Sophora flavescens var.flavescens), cold in nature, there is effect of heat clearing and damp drying, parasite killing, antibacterial, antiinflammatory, can Bergamot Mint Extract, dredge and restrain pore, promoting growth and the reparation of damaged blood vessels neurocyte, recover subcutaneous capillary cell viability;
N, Radix Salviae Miltiorrhizae (Salvia miltiorrhiza Bge.), energy promoting blood flow to regulate menstruation, stasis-dispelling and pain-killing, removing heat from blood eliminating carbuncle, the relieving restlessness that clears away heart-fire, nourishing blood to tranquillize the mind;
O, Radix Polygoni Multiflori Preparata (polygoni multiflori), have enrich and benefit essence and blood, nourishing the liver is calmed the nerves, bone and muscle strengthening, effects such as crow palpus of reinforcing the kidney;
P, Herba Agrimoniae (Agrimonia pilosa Ledeb.), have stronger removing heat from blood, antibacterial action;
Q, the Pseudobulbus Bletillae (Rhizoma Bletillae) (Bletilla striata (Thunb.ex A.Murray) Rchb.f.), have anti-bacillus, fungus, astringing to arrest bleeding, detumescence and promoting granulation, promotes epithelial cell reparation, and participate in reparation and the metabolic process of damaged tissues and cell directly;
R, Herba Ecliptae (Herba Ecliptae Eclipta prostrala L.), have nourishing the liver and kidney, effect such as crow palpus teeth consolidating, cooling blood for hemostasis etc., have inhibitory action to staphylococcus aureus;
S, the Radix Astragali (Leguminosae), have invigorating QI to consolidate the body surface resistance, diuresis poison holding, evacuation of pus, effect of expelling pus and promoting granulation;
T, Fructus Viticis (Vitex trifolia L.var.simplicifolia Cham. or Vitextrifolia L.), energy dispelling wind and heat pathogens, the clear sharp head, can promote scalp hair growth promoting.
The traditional Chinese medical science is thought, kidney governing bones store essential substances, its Hua Biao, and human hair growth, the process come off, show the process of kidney qi prosperity and decline, and kidney qi prosperity person then hair is pitch-black, and gloss is dense, and people's then prematured white hair of deficiency of kidney-QI, tarnish even comes off.Therefore, all early whitening of hair or come off, majority all with suffer from a deficiency of the kidney, the kidney store essential substances that do not nourish blood is relevant.The present invention adopts above-mentioned eight kinds of drug matchings, interior energy strenghthening bone, nourishing the liver and kidney, and blood circulation promoting and blood stasis dispelling, promotes cell division and hair growth, prevent alopecia; External enwergy Pesticidal and sterilizing, reduces outside stimulus.Meanwhile, be equipped with the natural surfactant tea saponin extracted from cake of camellia oleifera seeds, and other stimulate little composition.Thus, made Hair-loss-preventingshampoo shampoo, foaming power and detergency are comparatively strong, and wash and feel submissive, cleaning effect is outstanding, are unlikely again simultaneously and take away scalp excess moisture, therefore can moisten hair on the contrary; Its Chinese medicine ingredients can nourish root of hair, maintenance hair quality, and promotes hair growth, prevents alopecia.
Table 1 is Major health index and sense organ, the physical and chemical index of Hair-loss-preventingshampoo shampoo of the present invention below, and its quality meets the requirement of QB/T1974-2004 shampoo (cream) completely.
The sanitary index of table 1 Hair-loss-preventingshampoo shampoo and sense organ, physical and chemical index
Hair-loss-preventingshampoo shampoo of the present invention, through acute skin irritation test, result proves nonirritant; Acute ocular irritation test (30s) rinses, and result is subexcite; Skin allergy test result is for having no skin allergic reaction; Skin phototoxicity result of the test is for having no skin phototoxicity.
Hair-loss-preventingshampoo shampoo of the present invention, test through external Anti-hair loss:
Choose 60 volunteers and participate in test, volunteer's age, between 20-40 year, belongs to seborrheic alopecia, alopecia areata and physiologic alopecia etc., may not affect the other diseases of this observed result, do not use similar anti-product-stripping mechanism in 1 month, and observation etc. can have been coordinated voluntarily on request.In addition, consider seasonal factor, test and Selection is carried out at winter-spring season.Volunteer is divided into test group (30 people) and matched group (30 people) at random, and the volunteer of test group, uses Hair-loss-preventingshampoo shampoo of the present invention; The volunteer of matched group, uses commercially available shampoo as reference.3 combing hairs of every natural gift morning, noon and afternoon, the hair that collection comes off also records radical, gets its integer after obtaining meansigma methods.After the test of 56 days, statistical data, it the results are shown in table 2 below.
Table 2 Anti-hair loss statistical effect
From table 2 above, test through external Anti-hair loss, Hair-loss-preventingshampoo shampoo of the present invention improves significantly the effect of alopecia.Thus, prove that Hair-loss-preventingshampoo shampoo of the present invention possesses certain effect to Anti-hair loss.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplified, but protection scope of the present invention is not limited thereto.
Embodiment one
The Hair-loss-preventingshampoo shampoo of the present embodiment is prepared from by following raw material by weight:
Its preparation process is:
(i), Chinese medicine extraction liquid preparation:
1., Chinese medicine is got the raw materials ready:
Pressing row weight portion, to get raw material of Chinese medicine for subsequent use:
Radix Sophorae Flavescentis 3 Radix Salviae Miltiorrhizae 2 Radix Polygoni Multiflori Preparata 6 Herba Agrimoniae 4
The Pseudobulbus Bletillae (Rhizoma Bletillae) 2 Radix Astragali 3 Herba Ecliptae 4 Fructus Viticis 6;
2., Chinese medicine extraction:
After above-mentioned raw material of Chinese medicine washed with de-ionized water for subsequent use is clean, at 105 DEG C, be dried to moisture lower than 5%, then pulverized, 20 mesh sieves, then add according to the part by weight of solid-liquid ratio 1:5 the ethanol that volumetric concentration is 50%, stir; Then, soak 48 hours at normal temperatures and pressures, filter; Again filtrate is adopted the method for concentrating under reduced pressure, be concentrated into without alcohol, obtain Chinese medicine extraction liquid; Get 20 parts according to above-mentioned weight portion again, be required Chinese medicine extraction liquid, for subsequent use;
(ii), 60% tea saponin solution preparation:
Get the cake of camellia oleifera seeds raw material of constant weight, at 105 DEG C, be dried to point content lower than 5%, then pulverize, cross 40 mesh sieves; Adopt soxhlet extraction methods (that is: apparatus,Soxhlet's again; Also can adopt other method) remove contained by Residual oil; Then, according to the part by weight of solid-liquid ratio 1:5, being soaked in volumetric concentration is in the ethanol of 90%, stirs; Thereafter, by temperature increase to 60-70 DEG C, start ultrasonic cell disruptor and extract 2 hours, filter, so repeat extraction three times, merging three filtrates is merging filtrate; " vanillin-concentrated sulphuric acid development process " (other method also can be adopted to measure) is adopted to measure the content of tea saponin in merging filtrate again; When the content of tea saponin in merging filtrate is more than 60%, adds aquiferous ethanol (volumetric concentration is the ethanol of 30-90%), the content of tea saponin in merging filtrate is adjusted to 60%; When tea saponin in merging filtrate content lower than 60% time, concentrated merging filtrate, adjusts to 60% by the content of tea saponin in merging filtrate; Get 15 parts according to above-mentioned weight portion, be 60% required tea saponin solution, for subsequent use;
(iii), synthesize:
The pure water of above-mentioned 60% tea saponin solution for subsequent use and above-mentioned weight portion is mixed, is heated to 80 DEG C, after keeping 5min, add the 70%AESA of above-mentioned weight portion, stir; After 70%AESA dissolves, then add 35%CAB, the 70%SLA, 6501 of above-mentioned weight portion, maintain the temperature at 70 DEG C, be stirred to after dissolving completely; Then be cooled to 55 DEG C, then add after the Chinese medicine extraction liquid of above-mentioned weight portion, 2% guar gum, 95%CMEA mix homogeneously, continue to stir; In time being cooled to 50 DEG C, the pearlescent flake of above-mentioned weight portion, 50% anti-bacterial, anti-itching agent, Kazon, Flos Camelliae Japonicae essence being added and stirs evenly, then regulate pH value to 6.2 with 20% citric acid; Continue to stir, be cooled to 40 DEG C, i.e. the Hair-loss-preventingshampoo shampoo of cost implementation.Subsequently, through after the assay was approved leave standstill, fill, packaging, warehouse-in.
Embodiment two
The Hair-loss-preventingshampoo shampoo of the present embodiment is prepared from by following raw material by weight:
Its preparation process is:
(i), Chinese medicine extraction liquid preparation:
1., Chinese medicine is got the raw materials ready:
Pressing row weight portion, to get raw material of Chinese medicine for subsequent use:
Radix Sophorae Flavescentis 4 Radix Salviae Miltiorrhizae 3 Radix Polygoni Multiflori Preparata 8 Herba Agrimoniae 5
The Pseudobulbus Bletillae (Rhizoma Bletillae) 3 Radix Astragali 4 Herba Ecliptae 5 Fructus Viticis 7;
Other step is identical with embodiment one.
Embodiment three
The Hair-loss-preventingshampoo shampoo of the present embodiment is prepared from by following raw material by weight:
Its preparation process is:
(i), Chinese medicine extraction liquid preparation:
1., Chinese medicine is got the raw materials ready:
Pressing row weight portion, to get raw material of Chinese medicine for subsequent use:
Radix Sophorae Flavescentis 5 Radix Salviae Miltiorrhizae 4 Radix Polygoni Multiflori Preparata 10 Herba Agrimoniae 6
The Pseudobulbus Bletillae (Rhizoma Bletillae) 4 Radix Astragali 5 Herba Ecliptae 6 Fructus Viticis 8;
Other step is identical with embodiment one.
Embodiment four
The Hair-loss-preventingshampoo shampoo of the present embodiment is prepared from by following raw material by weight:
Its preparation process is:
(i), Chinese medicine extraction liquid preparation:
1., Chinese medicine is got the raw materials ready:
Pressing row weight portion, to get raw material of Chinese medicine for subsequent use:
Radix Sophorae Flavescentis 6 Radix Salviae Miltiorrhizae 5 Radix Polygoni Multiflori Preparata 12 Herba Agrimoniae 8
The Pseudobulbus Bletillae (Rhizoma Bletillae) 5 Radix Astragali 6 Herba Ecliptae 8 Fructus Viticis 10;
Other step is identical with embodiment one.
Hair-loss-preventingshampoo shampoo of the present invention, is suitable for the hair washing of men and women's Adult Groups and uses, both can be used for hair growth, and also can be used for pre-Anti-hair loss.

Claims (3)

1. a Hair-loss-preventingshampoo shampoo, it is characterized in that being prepared from by following raw material by weight:
Its preparation process is: 60% tea saponin solution of above-mentioned weight portion and pure water are mixed, be heated to 70-90 DEG C, keeps 4-6min, then adds the 70%AESA of above-mentioned weight portion, stirs; After 70%AESA dissolves, then add 35%CAB, the 70%SLA, 6501 of above-mentioned weight portion, maintain the temperature at 60-80 DEG C, be stirred to and dissolve completely; Then be cooled to 53-58 DEG C, then add after the Chinese medicine extraction liquid of above-mentioned weight portion, 2% guar gum, 95%CMEA mix homogeneously, continue to stir; In time being cooled to 48-52 DEG C, the pearlescent flake of above-mentioned weight portion, anti-bacterial, anti-itching agent, Kazon, Flos Camelliae Japonicae essence being added and stirs evenly, then use 20% citric acid adjust ph to 6.0-6.5; Continue to stir, be cooled to 35-45 DEG C;
Described Chinese medicine extraction liquid is prepared from by following raw material of Chinese medicine by weight:
The preparation method of described 60% tea saponin solution is: the cake of camellia oleifera seeds raw material getting constant weight, is dried to moisture lower than 5%, then pulverizes at 100-110 DEG C, crosses 30-50 mesh sieve; Remove contained Residual oil again; According to the part by weight of solid-liquid ratio 1:4-6, being soaked in volumetric concentration is in the ethanol of 90%, stirs, again by its temperature increase to 60-70 DEG C, start ultrasonic cell disruptor extract 1-3 hour, filter, so repeat extraction three times, merging three filtrates is merging filtrate; Measure the content of tea saponin in merging filtrate again, and adopt the mode of adding aquiferous ethanol or being concentrated by merging filtrate, in adjustment merging filtrate, the content of tea saponin reaches 60%, obtains 60% tea saponin solution.
2. Hair-loss-preventingshampoo shampoo according to claim 1, it is characterized in that the preparation method of described Chinese medicine extraction liquid is: after the raw material of Chinese medicine washed with de-ionized water of above-mentioned weight portion is clean, moisture is dried to lower than 5% at 100-110 DEG C, then pulverize, cross 10-30 mesh sieve, again according to the part by weight of solid-liquid ratio 1:4-6, adding volumetric concentration is the ethanol of 50%, stirs; Then, soak 45-50 hour at normal temperatures and pressures, filter; Again filtrate is adopted the method for concentrating under reduced pressure, be concentrated into without alcohol, obtain required Chinese medicine extraction liquid.
3. Hair-loss-preventingshampoo shampoo according to claim 1, it is characterized in that the preparation method of described Chinese medicine extraction liquid is: after being cleaned up by the raw material of Chinese medicine water of above-mentioned weight portion, clear water is added according to the part by weight of solid-liquid ratio 1:1-3, boil and extract 0.5-1.5 hour, filter, obtain an extracting solution; Add clear water according to the part by weight of solid-liquid ratio 1:1-2 again, boil and extract 0.5-1 hour, filter, obtain secondary raffinate; Merge extracted twice liquid, adopt the method for vacuum concentration, be concentrated into the half of merge extractive liquid, original volume, obtain required Chinese medicine extraction liquid.
CN201310475889.4A 2013-10-12 2013-10-12 Hair-loss-preventing shampoo Active CN103520036B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310475889.4A CN103520036B (en) 2013-10-12 2013-10-12 Hair-loss-preventing shampoo

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310475889.4A CN103520036B (en) 2013-10-12 2013-10-12 Hair-loss-preventing shampoo

Publications (2)

Publication Number Publication Date
CN103520036A CN103520036A (en) 2014-01-22
CN103520036B true CN103520036B (en) 2015-04-08

Family

ID=49922628

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310475889.4A Active CN103520036B (en) 2013-10-12 2013-10-12 Hair-loss-preventing shampoo

Country Status (1)

Country Link
CN (1) CN103520036B (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103989622B (en) * 2014-06-16 2015-06-17 湖南农业大学 Tea saponin shampoo and production method thereof
CN104800118B (en) * 2015-04-17 2017-08-22 云南健牛生物科技有限公司 A kind of antipruritic translucent shampoo of anticreep and preparation method thereof
CN105997729A (en) * 2016-07-12 2016-10-12 黔南民族师范学院 Hair care emulsion prepared from Duyun tippy tea seed cakes and preparation method thereof
CN106176316A (en) * 2016-08-26 2016-12-07 华侨大学 A kind of tea saponin shampoo
CN106265332A (en) * 2016-09-11 2017-01-04 桂林理工大学 A kind of Chinese medicine shampoo containing Folium Kaki and preparation method thereof
CN106727157B (en) * 2017-01-20 2021-05-04 江苏美爱斯化妆品股份有限公司 Hair loss prevention and hair growth promoting shampoo
CN107184453A (en) * 2017-05-13 2017-09-22 吴杰 A kind of Chinese medicine preparation Hair-loss-preventingshampoo shampoo and preparation method thereof
CN107261095A (en) * 2017-07-20 2017-10-20 祁东县恒仁堂化妆品有限责任公司 A kind of pine needle hair lotion of hair growth
CN108721177A (en) * 2018-09-07 2018-11-02 海南迈嘉热带油茶研究院有限公司 Camellia amino acid shampoo
CN109010231A (en) * 2018-09-29 2018-12-18 韶关市小豆子电子科技有限公司 A kind of Haircare composition and preparation method thereof based on marine organism extract
CN110420141A (en) * 2019-08-16 2019-11-08 中国热带农业科学院海口实验站 A kind of Tea Saponin shampoo and its preparation method and application

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1349792A (en) * 2001-11-06 2002-05-22 广东轻工职业技术学院 Composite shampoo with tea component and its making process
CN100569214C (en) * 2008-11-06 2009-12-16 郴州邦尔泰苏仙油脂有限公司 Tea saponin shampoo and production technology
CN102836097B (en) * 2012-08-21 2014-09-03 伊国群 Liquid shampoo containing tea saponin

Also Published As

Publication number Publication date
CN103520036A (en) 2014-01-22

Similar Documents

Publication Publication Date Title
CN103520036B (en) Hair-loss-preventing shampoo
CN105997836B (en) A kind of ferment shampoo and its preparation method
CN103169631B (en) A kind of submissive glossy shampoo and preparation method containing Chinese medicine composition
KR102533052B1 (en) Korean traditional herbs shampoo composition
CN102133162B (en) Anti-dropping and hair reviving shampoo and preparation method thereof
CN105078850A (en) Liquid shampoo and preparation method thereof
CN106038388A (en) Traditional Chinese medicine hair shampoo and preparation method thereof
CN102038626B (en) Traditional Chinese medicinal hair-restoring and anti-alopecia shampoo and preparation method thereof
US9180087B2 (en) Chinese medicine hair-regrowth preparation and formula and preparation method therefor
CN102018771A (en) Hair anti-dropping medical pilatory
CN108272700A (en) A kind of composition and preparation method thereof with hair-loss preventing and hair-restoring, anti-dandruff and itching-relieving efficacies
CN107468571A (en) Shampoo containing Chinese herbal medicines and preparation method thereof
CN111920736A (en) Anti-hair loss composition
CN102755280B (en) Chinese herbal medicine shampoo and preparation method thereof
CN105168074A (en) Antidandruff and antipruritic traditional Chinese medicine composition and application and preparation method thereof
CN104887602A (en) Jasmine hair and face cleaning liquid
CN106265324A (en) A kind of hair care anti-hair loss composition for dryness seborrheic alopecia and application
CN105560151A (en) Salt for hair care, and preparation method thereof
CN105168041A (en) Anti-dandruff antipruritic shampoo and preparation method thereof
CN106177192B (en) Bi-component compound medicine for treating head oil and dandruff and preparation method thereof
CN115227622A (en) Preparation process of hair loss preventing and nourishing essence
CN104013565B (en) A kind of hair protecting shampoo
CN103637956B (en) Shampoo
CN105250207A (en) Agilawood and ant nest fruit ask liquid with pure natural ingredients, mask and preparation method of mask liquid
CN106214556A (en) Both effectiveness plant shampoo

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant