CN103467135A - Preparation method of copper-black metal glaze - Google Patents

Preparation method of copper-black metal glaze Download PDF

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Publication number
CN103467135A
CN103467135A CN 201210184988 CN201210184988A CN103467135A CN 103467135 A CN103467135 A CN 103467135A CN 201210184988 CN201210184988 CN 201210184988 CN 201210184988 A CN201210184988 A CN 201210184988A CN 103467135 A CN103467135 A CN 103467135A
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China
Prior art keywords
parts
glaze
preparation
oxide
copper
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Pending
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CN 201210184988
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Chinese (zh)
Inventor
张新桥
潘俊明
郭亮
曾日伦
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HUNAN TAIXIN CERAMICS CO Ltd
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HUNAN TAIXIN CERAMICS CO Ltd
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Priority to CN 201210184988 priority Critical patent/CN103467135A/en
Publication of CN103467135A publication Critical patent/CN103467135A/en
Pending legal-status Critical Current

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Abstract

A preparation method of copper-black metal glaze is characterized in that: a glaze material comprises the following sources and components (by mass): 15-25 parts of potassium feldspar powder, 6-15 parts of quartz powder, 10-17 parts of calcite, 1-5 parts of processed talc, 4-10 parts of kaolin, 10-20 parts of zinc oxide, 30-85 parts of medium-temperature frit, 5-10 parts of copper oxide, 0.1-1 part of cobalt oxide, 1-4 parts of ferric oxide and 2-5 parts of a black pigment; after glaze slurry is obtained, glaze firing is carried out in accordance with the temperature of the preparation method; and a glazed product has a bright glazing surface, and also has art effects of copper-black metal color.

Description

A kind of preparation method of copper ferrous metal glaze
Technical field
The present invention relates to a kind of preparation method of copper ferrous metal glaze.
Background technology
Ceramic has become more and more general daily product, along with social progress, more and more higher with people's standard of living, the human consumer is also more and more higher for the esthetic requirement of ceramic product, yet the critical material that plays modification effect for ceramic product is glaze, and existing glaze roughly is divided into according to classification and purposes: 1, lead glaze and leadless glaze; 2, raw glaze and fritted glaze; 3, once-firing or twice firing glaze; 4, tableware, ceramic tile, glaze etc. for snitaryware, traditional ceramic surface is all too much not modify or complex pattern, but along with the aesthetic raising of people, the porcelain that carries out metal-imitation glaze, marble grain texts at ceramic surface is more and more welcome, therefore, stability, diversity, glaze decoration, the pattern decoration for ceramic glaze become the target that each ceramic producer is pursued.
Summary of the invention
The invention provides the preparation method of copper ferrous metal glaze, make the product after burning till there is the glaze light, be the artistic effect of the metal glaze of copper black.
The present invention is achieved in that a kind of preparation method of copper ferrous metal glaze, the source of glaze and consist of (mass parts): adopt the feldspar in powder of 15~25 parts, 6~15 parts of silica powders, 10~17 parts of calcites, 1~5 part of ripe talcum, 4~10 parts of kaolin, 10~20 parts of zinc oxide, warm frit in 30~85 parts, 5~10 parts of cupric oxide, 0.1~1 part of cobalt oxide, 1~4 part of ferric oxide, 2~5 parts of black pigments.
The glaze slip preparation: the compositing formula by above-mentioned glaze takes respectively raw material, and in raw material: the ratio of ballstone: water=1:1.5:0.5~0.6 is pulverized in ball mill, Ball-milling Time is 12~20 hours, when the glaze fineness reached 180 mesh sieves, and gets final product during the concentration of furnishing 45~60 degree Beaume.
After glaze slip imposes on the biscuiting base substrate, the glaze layer thickness is controlled at 0.3~0.6 mm.
The glaze firing technique adopted is: be placed in the oxidizing atmosphere of 1180~1200 ℃, burning till frequency is 22~24HZ, and firing period is 4~5 hours, and soak 20~30 minutes, finally naturally cool to room temperature, obtains product.
The invention has the beneficial effects as follows:
1, glaze light, have again the artistic effect of copper ferrous metal look;
2, raw material sources are extensive, burn till rear hardness of glaze surface high, and wear resistance and good corrosion resistance are good ceramic artistic glazes.
Embodiment
In order to make purpose of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only, in order to explain the present invention, be not intended to limit the present invention.
A kind of preparation method of copper ferrous metal glaze, the source of glaze and consist of (mass parts): adopt the feldspar in powder of 15~25 parts, 6~15 parts of silica powders, 10~17 parts of calcites, 1~5 part of ripe talcum, 4~10 parts of kaolin, 10~20 parts of zinc oxide, warm frit in 30~85 parts, 5~10 parts of cupric oxide, 0.1~1 part of cobalt oxide, 1~4 part of ferric oxide, 2~5 parts of black pigments.
The glaze slip preparation: the compositing formula by above-mentioned glaze takes respectively raw material, and in raw material: the ratio of ballstone: water=1:1.5:0.5~0.6 is pulverized in ball mill, Ball-milling Time is 12~20 hours, when the glaze fineness reached 180 mesh sieves, and gets final product during the concentration of furnishing 45~60 degree Beaume.
After glaze slip imposes on the biscuiting base substrate, the glaze layer thickness is controlled at 0.3~0.6 mm.
The glaze firing technique adopted is: be placed in the oxidizing atmosphere of 1180~1200 ℃, burning till frequency is 22~24HZ, and firing period is 4~5 hours, and soak 20~30 minutes, finally naturally cool to room temperature, obtains product.
These are only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.

Claims (1)

1. the preparation method of a copper ferrous metal glaze, it is characterized in that: the source of glaze and consist of (mass parts): adopt the feldspar in powder of 15~25 parts, 6~15 parts of silica powders, 10~17 parts of calcites, 1~5 part of ripe talcum, 4~10 parts of kaolin, 10~20 parts of zinc oxide, warm frit in 30~85 parts, 5~10 parts of cupric oxide, 0.1~1 part of cobalt oxide, 1~4 part of ferric oxide, 2~5 parts of black pigments.
Glaze slip preparation: the compositing formula by above-mentioned glaze takes respectively raw material, and in raw material: the ratio of ballstone: water=1:1.5:0.5~0.6 is pulverized in ball mill, and Ball-milling Time is 12~20 hours; When the glaze fineness reached 180 mesh sieves, and get final product during the concentration of furnishing 45~60 degree Beaume.
After glaze slip imposes on the biscuiting base substrate, the glaze layer thickness is controlled at 0.3~0.6 mm.
The glaze firing technique adopted is: be placed in the oxidizing atmosphere of 1180~1200 ℃, burning till frequency is 22~24HZ, and firing period is 4~5 hours, and soak 20~30 minutes, finally naturally cool to room temperature, obtains product.
CN 201210184988 2012-06-06 2012-06-06 Preparation method of copper-black metal glaze Pending CN103467135A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201210184988 CN103467135A (en) 2012-06-06 2012-06-06 Preparation method of copper-black metal glaze

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201210184988 CN103467135A (en) 2012-06-06 2012-06-06 Preparation method of copper-black metal glaze

Publications (1)

Publication Number Publication Date
CN103467135A true CN103467135A (en) 2013-12-25

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CN 201210184988 Pending CN103467135A (en) 2012-06-06 2012-06-06 Preparation method of copper-black metal glaze

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CN (1) CN103467135A (en)

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104130030A (en) * 2014-08-11 2014-11-05 湖南省醴陵市楚华陶瓷实业有限公司 Preparation method of bright gold glaze
CN105330158A (en) * 2015-10-30 2016-02-17 广东家美陶瓷有限公司 Glaze of brunet ceramic and preparation method of glaze
CN106186700A (en) * 2016-07-22 2016-12-07 福建省德化县华泰陶瓷有限公司 Environmental protection shell pearl glaze, the environmental protection shell pearl glaze ceramic and preparation method thereof prepared with it
CN107382066A (en) * 2017-08-24 2017-11-24 赣州艺佳兴陶瓷有限公司 A kind of special ceramet glaze of ceramics
CN108059348A (en) * 2017-12-31 2018-05-22 湖南省明丰达陶瓷琉璃瓦业有限公司 A kind of emerald green copper glaze
CN108545937A (en) * 2016-01-20 2018-09-18 福建省德化县鸿芳陶瓷有限公司 A kind of preparation process of Sapporo color ceramic
CN108640511A (en) * 2018-07-27 2018-10-12 醴陵千汇实业有限公司 A kind of iron oxide black orange peel glaze and preparation method thereof
CN109942189A (en) * 2019-04-16 2019-06-28 福建省德化问瓷阁陶瓷有限公司 A kind of dark metal glaze ceramics of environmental-friendly lead-free and its manufacture craft
CN111170635A (en) * 2020-01-14 2020-05-19 湖南泰鑫瓷业有限公司 Matt reaction glaze with metallic luster and preparation method thereof
CN111875366A (en) * 2020-07-20 2020-11-03 广东新润成陶瓷有限公司 Whole-body log texture ceramic tile and preparation method thereof
CN112028484A (en) * 2020-09-04 2020-12-04 福建省春秋陶瓷实业有限公司 Dark green transmutation glaze ceramic product and preparation method thereof
CN113666639A (en) * 2021-08-31 2021-11-19 佛山欧神诺陶瓷有限公司 Black rock plate and preparation method thereof

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104130030A (en) * 2014-08-11 2014-11-05 湖南省醴陵市楚华陶瓷实业有限公司 Preparation method of bright gold glaze
CN105330158A (en) * 2015-10-30 2016-02-17 广东家美陶瓷有限公司 Glaze of brunet ceramic and preparation method of glaze
CN105330158B (en) * 2015-10-30 2018-02-23 广东家美陶瓷有限公司 A kind of glaze of dark ceramics and preparation method thereof
CN108545937A (en) * 2016-01-20 2018-09-18 福建省德化县鸿芳陶瓷有限公司 A kind of preparation process of Sapporo color ceramic
CN106186700A (en) * 2016-07-22 2016-12-07 福建省德化县华泰陶瓷有限公司 Environmental protection shell pearl glaze, the environmental protection shell pearl glaze ceramic and preparation method thereof prepared with it
CN106186700B (en) * 2016-07-22 2019-01-15 福建省德化县华泰陶瓷有限公司 Environmentally friendly shell pearl glaze, environmental protection shell pearl glaze ceramic and preparation method thereof made from it
CN107382066A (en) * 2017-08-24 2017-11-24 赣州艺佳兴陶瓷有限公司 A kind of special ceramet glaze of ceramics
CN108059348A (en) * 2017-12-31 2018-05-22 湖南省明丰达陶瓷琉璃瓦业有限公司 A kind of emerald green copper glaze
CN108640511A (en) * 2018-07-27 2018-10-12 醴陵千汇实业有限公司 A kind of iron oxide black orange peel glaze and preparation method thereof
CN109942189A (en) * 2019-04-16 2019-06-28 福建省德化问瓷阁陶瓷有限公司 A kind of dark metal glaze ceramics of environmental-friendly lead-free and its manufacture craft
CN111170635A (en) * 2020-01-14 2020-05-19 湖南泰鑫瓷业有限公司 Matt reaction glaze with metallic luster and preparation method thereof
CN111875366A (en) * 2020-07-20 2020-11-03 广东新润成陶瓷有限公司 Whole-body log texture ceramic tile and preparation method thereof
CN112028484A (en) * 2020-09-04 2020-12-04 福建省春秋陶瓷实业有限公司 Dark green transmutation glaze ceramic product and preparation method thereof
CN113666639A (en) * 2021-08-31 2021-11-19 佛山欧神诺陶瓷有限公司 Black rock plate and preparation method thereof

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Application publication date: 20131225